Polypropylene/polyhedral oligomeric silsesquioxane nanocomposites – study of free volumes, crystallinity degree and mass flow rate

6533b862fe1ef96bd12c7733

RESEARCH PRODUCT

Polypropylene/polyhedral oligomeric silsesquioxane nanocomposites – study of free volumes, crystallinity degree and mass flow rate

Arkadiusz Niemczyk Roman Szatanik Michał Dutkiewicz Mariusz Szołyga Krystyna Czaja Katarzyna Dziubek Bogdan Marciniec

subject

poliedryczne oligomeryczne silseskwioksany (POSS)Materials science Polymers and Plastics General Chemical Engineering 02 engineering and technology 010402 general chemistry 01 natural sciences Degree (temperature)chemistry.chemical_compound Crystallinity mass flow rate nanocomposites Materials Chemistry Mass flow rate Composite material nanokompozyty Polypropylene Nanocomposite positron annihilation lifetime spectroscopy (PALS)masowy wskaźnik szybkości płynięcia crystallinity degree stopień krystaliczności 021001 nanoscience & nanotechnology Silsesquioxane 0104 chemical sciences chemistry spektroskopia czasów życia pozytonów (PALS)polipropylen 0210 nano-technology polypropylene polyhedral oligomeric silsesquioxanes (POSS)

description

Nanokompozyty polipropylen/poliedryczne oligomeryczne silseskwioksany (PP/POSS) przygotowano metodą mieszania w stanie stopionym polimeru. Wpływ struktury oraz ilości zastosowanych nanonapełniaczy POSS na objętości swobodne w polipropylenie określono z zastosowaniem spektroskopii czasów życia pozytonów (PALS). Ustalono zależności pomiędzy parametrami PALS: czasem życia o-Ps (τ3) i natężeniem (I3) składowej o-Ps oraz wartościami stopnia krystaliczności (Xc ) i masowego wskaźnika szybkości płynięcia (MFR) badanych materiałów. Obecność nanonapełniaczy POSS wpłynęła na liczbę i rozmiary objętości swobodnych w polimerze, co spowodowało zmianę mikrostruktury osnowy polipropylenowej. Wraz ze zwiększaniem zawartości napełniaczy POSS zmniejszał się stopień krystaliczności kompozytów, zwiększało natężenie składowej o-Ps, a dodatkowo wzrastała wartość MFR – nanocząstki POSS pełniły w układzie rolę plastyfikatorów.

year	journal	country	edition	language
2016-09-01	Polimery

https://doi.org/10.14314/polimery.2016.610

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