6533b86efe1ef96bd12cc003

RESEARCH PRODUCT

Determination of triazines and organophosphorus pesticides in water samples using solid-phase extraction.

Jordi MañesGuillermina FontYolanda PicoJuan Carlos MoltóHouda Berrada

subject

ChromatographyChromatography GasChemistryTriazinesOrganic ChemistryExtraction (chemistry)Ethyl acetateGeneral MedicineBiochemistryAnalytical Chemistrylaw.inventionchemistry.chemical_compoundAdsorptionOrganophosphorus CompoundslawFlame ionization detectorGas chromatographySolid phase extractionPesticidesDimethoateWater Pollutants ChemicalTriazine

description

Abstract Octadecyl (C 18 )-bonded porous silica was evaluated for the extraction of triazine and organophosphorus pesticides from natural water. The extraction results showed an effective performance when 1 l of water was passed through small glass columns containing 500 mg of 50–100-μm C 18 bonded porous silica. The absorbed compounds were removed with ethyl acetate, evaporated to 200 μl and determined by gas chromatography. The overall average recoveries were greater than 85% except for dimethoate and trichlorfon. Application of this procedure to the analysis of natural water samples gave results that agree well with those obtained by solvent extraction methods.

10.1016/s0021-9673(01)87173-9https://pubmed.ncbi.nlm.nih.gov/1783623