KMR spektroskopijas pielietojums fluorbenzoskābju un fluorbenzamīdu kristalizācijas pētījumos

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RESEARCH PRODUCT

KMR spektroskopijas pielietojums fluorbenzoskābju un fluorbenzamīdu kristalizācijas pētījumos

subject

π-π MIJIEDARBĪBAS FLUORBENZAMĪDI ŪDEŅRAŽA SAIŠU DIMĒRI PAŠASOCIĀCIJA Ķīmija FLUORBENZOSKĀBES

description

Kresse I. Darba vadītājs Dr. Chem. Bobrovs R. Maģistra darbs, 53 lapaspuse, 34 attēli, 10 tabulas, 37 literatūras avoti. Latviešu valodā. Darba literatūras apskatā aplūkotas fluorbenzoskābju un fluorbenzamīdu kristāliskās struktūras, starpmolekulārie mijiedarbību veidi, kur īpaša uzmanība pievērsta ūdeņraža saitēm un π-π mijiedarbībām, uzskaitītas kodolu magnētiskās rezonanses metodes, kuras tiek izmantotas pašasociācijas pētījumos un aprakstīts kristalizācijas process. Eksperimentālajā daļā uzņemti protonu, oglekļa un fluora kodolmagnētiskās rezonanses spektri dažādu koncentrāciju etanola-d6, dioksāna-d8, acetona-d6 un DMSO-d6 šķīdumiem visām izmantotajām fluorbenzoskābēm un fluorbenzamīdiem, kā arī – toluolam un etiķskābei. Iegūtie dati analizēti, izdarot secinājumus par molekulu pašasociāciju šķīdumos. Šķīdumiem uzņemti relaksācijas laika T1 mērījumi, kas papildina informāciju par iespējamajām asociātu izmēru izmaiņām.

year	journal	country	edition	language
2019-01-01

https://dspace.lu.lv/dspace/handle/7/46748

PEPhysical Sciences and Engineering
- PE2Fundamental Constituents of Matter
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