6533b872fe1ef96bd12d2f20

RESEARCH PRODUCT

Isolation, dynamic NMR study and X-ray characterisation of a bis sulfonium zirconocene-ate dimer.

Philippe MeunierBruno DonnadieuEsteban OrtegaNadine Pirio

subject

SulfoniumStereochemistryDimerMetals and AlloysX-rayGeneral ChemistryNuclear magnetic resonance spectroscopyCatalysisSurfaces Coatings and FilmsElectronic Optical and Magnetic Materialschemistry.chemical_compoundchemistryMaterials ChemistryCeramics and Composites

description

The novel dimer [Cp(2)Zr[upper bond start]([minus sign in circle])S([plus sign in circle])CH(Ph)CH[double bond]C[upper bond end]PPh(2)](2), the first example of a structurally characterised sulfur-bridged binuclear zirconathiolane complex, was prepared, characterised by NMR spectroscopy and X-ray crystallography, and some aspects of its solution behaviour were studied.

10.1039/b312954chttps://pubmed.ncbi.nlm.nih.gov/15010777