Search results for " 4"
showing 10 items of 3131 documents
PEG 400/Cerium Ammonium Nitrate Combined with Microwave-Assisted Synthesis for Rapid Access to Beta-Amino Ketones. An Easy-to-Use Protocol for Discov…
2018
Compound libraries are important requirement in target-based drug discovery. In the present work, a small focused compound library based on β-aminoketone scaffold has been prepared combining microwave-assisted organic synthesis (MAOS) with polymer-assisted solution phase synthesis (PASPS) and replacing reaction workup standard purification procedures with solid phase extraction (SPE). Specifically, the effects of solvent, such as dioxane, dimethylformamide (DMF), polyethylene glycol 400 (PEG 400), temperature, irradiation time, stoichiometric ratio of reagents, and catalysts (HCl, acetic acid, cerium ammonium nitrate (CAN)) were investigated to maximize both conversion and yield. The optimi…
Isometric embeddings of snowflakes into finite-dimensional Banach spaces
2016
We consider a general notion of snowflake of a metric space by composing the distance by a nontrivial concave function. We prove that a snowflake of a metric space $X$ isometrically embeds into some finite-dimensional normed space if and only if $X$ is finite. In the case of power functions we give a uniform bound on the cardinality of $X$ depending only on the power exponent and the dimension of the vector space.
Entre l’État et la chefferie simple : le complexe aristocratique de Vix/le mont Lassois
2021
International audience
CCDC 777752: Experimental Crystal Structure Determination
2011
Related Article: Yuhui Kou, Hongqi Tao, Derong Cao, Zhiyong Fu, D.Schollmeyer, H.Meier|2010|Eur.J.Org.Chem.|2010|6464|doi:10.1002/ejoc.201000718
Ionic liquid crystals based on viologen dimers: tuning the mesomorphism by varying the conformational freedom of the ionic layer
2016
ABSTRACTWe investigated the liquid crystal behaviour of newly synthesised bistriflimide salts of symmetric viologen dimers. A smectic A phase was observed for intermediate spacer lengths and for relatively long lateral alkyl chains. The systems were characterised by thermal analysis, polarised optical microscopy, X-ray scattering and solid-state NMR. An intermediate ordered smectic phase was also exhibited by the compounds (except for systems with very short lateral chains) consisting of molten layers of alkyl chains and partially ordered ionic layers. These results, relating to the mesomorphic behaviour of viologen salts, are qualitatively compared to those of the more common imidazolium s…
CCDC 1849905: Experimental Crystal Structure Determination
2018
Related Article: A. Piontek, D. Siodłak, B. Zarychta|2018|IUCrData|3|x180889|doi:10.1107/S2414314618008891
Isoxazolo[5,4-e]isoindole a new ring system with potent antitumor activity
2011
Better numerical approximation by Durrmeyer type operators
2018
The main object of this paper is to construct new Durrmeyer type operators which have better features than the classical one. Some results concerning the rate of convergence and asymptotic formulas of the new operator are given. Finally, the theoretical results are analyzed by numerical examples.
Estimates for the differences of positive linear operators and their derivatives
2019
The present paper deals with the estimate of the differences of certain positive linear operators and their derivatives. Oxur approach involves operators defined on bounded intervals, as Bernstein operators, Kantorovich operators, genuine Bernstein-Durrmeyer operators, and Durrmeyer operators with Jacobi weights. The estimates in quantitative form are given in terms of the first modulus of continuity. In order to analyze the theoretical results in the last section, we consider some numerical examples.
Better approximation of functions by genuine Bernstein-Durrmeyer type operators
2018
The main object of this paper is to construct a new genuine Bernstein-Durrmeyer type operators which have better features than the classical one. Some direct estimates for the modified genuine Bernstein-Durrmeyer operator by means of the first and second modulus of continuity are given. An asymptotic formula for the new operator is proved. Finally, some numerical examples with illustrative graphics have been added to validate the theoretical results and also compare the rate of convergence.