Search results for " Sam"
showing 10 items of 1096 documents
Selection of Large Sub-Samples from the Continuous Sample of Working Lives Representative of the Benefits Provided by the Spanish Public Pension Syst…
2016
The Continuous Sample of Working Lives (CSWL) is a set of anonymized microdata with information about individuals taken from Spanish Social Security records. It provides very valuable information, which is used in many studies on labor economics and in the analysis of the Spanish public pension system. This article presents two major contributions: The first is an analysis of how representative CSWL is of the population of pensioners for the period 2005-2013. It is concluded that the CSWL does not follow the same distribution as the population with respect to some types of benefits, and that this happens in most waves. One of the reasons is that it is obtained by simple random sampling, so …
Dataset of the COVID-19 lockdown survey conducted by GIPEyOP in Spain
2022
This article introduces a dataset that captures relevant in- formation about the living conditions, feelings, and habits of residents in Spain during ninety nine days of home confinement. This and other measures, imposed by the Government of Spain to mitigate the impact of the pandemic on the population, have brought with them important economic, labor, and social changes, which have been accompanied by various modifications (some only temporary) in Spaniards habits and behaviours. Data collection was carried out through the implementation of a questionnaire with 33 questions, which was sent by email to the collaborators of GIPEyOP (Elections and Public Opinion Research Group from the Unive…
Sociodemographic Characteristics and Interests of FeverApp Users
2021
The FeverApp Registry is a model registry focusing on pediatric fever using a mobile app to collect data and present recommendations. The recorded interactions can clarify the relationship between user documentation and user information. This initial evaluation regarding features of participants and usage intensity of educational video, information library, and documentation of fever events covers the runtime of FeverApp for the first 14 months. Of the 1592 users, the educational opening video was viewed by 41.5%, the Info Library was viewed by 37.5%, and fever events were documented by 55.5%. In the current sample, the role of a mother (p <
Electronic paramagnetic resonance power saturation of wooden samples
2009
The deterioration of wood used for artifacts of artistic interest involves the production of different free radicals from the macromolecules of the wooden matrix (cellulose, lignin, and hemicellulose). Among the techniques able to provide information about these free radicals, the contribution of electronic paramagnetic resonance (EPR) can be very valuable. In this paper, the study of EPR signals (with g 2) of both modern and ancient wooden taxa was undertaken in order to analyze some features of the free radicals in natural wood. In particular, we have studied the microwave power saturation behaviors of seasoned wooden samples from ten species, and we have found remarkable differences betw…
Manual packing and soil reuse effects on determination of saturated hydraulic conductivity of a loam soil
2022
Abstract Performing laboratory measurement of saturated hydraulic conductivity, Ks, of sieved soil is important for many scientific purposes such as testing theories and methods to determine Ks. A given soil mass can be used only once or it can be reused after a previous use. Little is known on the dependence of the Ks measurements on both the applied packing method and the reuse of the same soil mass. This lack of knowledge makes comparisons among different investigations more or less uncertain. Four packing methods were tested on an initially dry loam soil by measuring Ks with the simplified falling head (SFH) technique. The four methods differed by the used compacting procedure (dropping…
Determination of benzomercaptans in environmental complex samples by combining zeolitic imidazolate framework-8-based solid-phase extraction and high…
2020
[EN] In this work, the synthesis of zeolitic imidazolate framework-8 (ZIF-8) crystals and their subsequent application as effective sorbents for extraction and preconcentration of several benzomercaptans from environmental complex samples is described. These materials were prepared by solvothermal approach varying the concentration of n-butylamine modulator to modify the surface of the metal-organic framework. The resulting materials were characterized by scanning and transmission electron microscopy, powder X-ray diffraction and Fourier transform infrared spectroscopy. The ZIF-8 material that gave the best features was selected as extractive phase and the influence of various parameters (s…
Determination of phenolic compounds in surface waters using high-performance liquid chromatography and molecularly imprinted solid-phase extraction
2021
An effective and reliable analytical method based on molecularly imprinted solid-phase extraction (MI-SPE) and high-performance liquid chromatography with photodiode array detector was developed to simultaneously determine four phenolic compounds: bisphenol A, 2-phenylphenol, tert-octylphenol and nonylphenol. A molecularly imprinted polymer that can selectively recognize bisphenol A and alkylphenols was developed. A bulk polymerization method using bisphenol A as a template, acrylamide as functional monomer, ethylene glycol dimethacrylate as the cross-linking agent, acetonitrile as porogenic solvent and 1,1’-azobis(cyclohexanecarbonitrile) as initiator was applied. This polymer was applied …
Selection of sampling adsorbents and optimisation and validation of a GC-MS/MS method for airborne pesticides
2017
ABSTRACTA methodology for the sampling and determination of airborne pesticides has been developed. The trapping efficiency of three adsorbents, namely XAD-2,XAD-4 and a sandwich sorbent (PUF-XAD2-PUF), was tested for 34 pesticides and the latter was selected because it presented the highest retention capacity without breakthrough. Pesticides were determined by gas chromatography coupled to an ion trap mass spectrometer in tandem. The method showed recoveries ranging from 70% to 120% with limits of quantification in the range of 16.1–322.6 pg m−3 when 155 m3 were sampled. This analytical strategy was applied to 10 indoor air samples collected in dwellings from the Valencian Region. Six pest…
Determination of macrolide antibiotics in meat and fish using pressurized liquid extraction and liquid chromatography–mass spectrometry
2008
We developed a method for determining the quantities of seven macrolide antibiotics in meat and fish by using pressurized liquid extraction (PLE) and liquid chromatography-mass spectrometry with electrospray ionization (LC-(ESI)MS). The PLE was optimized with regard to solvents, temperature, pressure, extraction time and number of cycles. The optimum conditions were: methanol as the extraction solvent; a temperature of 80 degrees C; a pressure of 1500psi; an extraction time of 15min; 2 cycles; a flush volume of 150% and a purge time of 300s. All recoveries for macrolide antibiotics were over 77% at 200mug/kg, except for erythromycin, which was 58%. The repeatability and reproducibility on d…
Conditions of dust sampling in pneumatic conveying through the horizontal pipeline
2007
Abstract The paper presents the results of examinations on the reciprocal relation between the isokinetic coefficient H of sampling, the quantity of measured mass concentration and the measuring usefulness of a dust sample aspired from the stream of solgas conveyed pneumatically in the horizontal pipeline. In gravimetric measurements of two-phase flows, the conditions under which aspiration is carried out, are extremely important. Available theoretical considerations and practical experiments usually concern aspiration in the vertical channels, where the manner of making measurements is universally known and it does not express any reservations. However, it is often necessary to conduct tes…