Search results for " absorption spectroscopy"
showing 10 items of 293 documents
Characterization of a cylindrical plastic {\beta}-detector with Monte Carlo simulations of optical photons
2017
V. Guadilla et al. -- 5 pags., 8 figs., tab.
The role of yttrium and titanium during the development of ODS ferritic steels obtained through the STARS route: TEM and XAS study
2018
Abstract Oxide Dispersion Strengthened Ferritic Steels (ODS FS) are candidate materials for structural components in future fusion reactors. Their high strength and creep resistance at elevated temperatures and their good resistance to neutron radiation damage is obtained through extremely fine microstructures containing a high density of nanometric precipitates, generally yttrium and titanium oxides. This work shows transmission electron microscopy (TEM) and extended X-ray absorption fine structure (EXAFS) characterization of Fe-14Cr-2W-0.3Ti-0.24Y ODS FS obtained by the STARS route (Surface Treatment of gas Atomized powder followed by Reactive Synthesis), an alternative method to obtain O…
Total Absorption Spectroscopy
2018
Some advances in science come when a new technique is available. There are many examples in the history of science. The advances usually provide the opportunity to see what was hidden to the well-e...
Total absorption study of theβdecay of102,104,105Tc
2013
The $\ensuremath{\beta}$-feeding probabilities for three important contributors to the decay heat in nuclear reactors, namely ${}^{102,104,105}$Tc, have been measured using the total absorption spectroscopy technique. For the measurements, sources of very high isobaric purity have been obtained using a Penning trap (JYFLTRAP). A detailed description of the data analysis is given and the results are compared with high-resolution measurements and theoretical calculations.
Beta delayed alpha emission from the neutron deficient rare earth isotopes [sup 152]Tm and [sup 150]Ho
2011
The study of beta‐delayed proton emission is a well known method to aid the determination of the beta strength distribution in nuclei far from the stability line. At the neutron deficient side of the nuclear chart the process of proton or alpha emission from excited states is energetically allowed when one goes far enough from stability. However, beta‐delayed alphas have seldom been measured for nuclei heavier than A = 20. Here we present a study of the beta‐delayed alpha‐particle emission from 152Tm and 150Ho and their importance in the full B(GT) distribution. © 2011 American Institute of Physics
Determination of Boron in Fertilizers by Inductively Coupled Plasma-Atomic Emission Spectrometry: Studies of Some Spectral Interferences at Different…
1995
Abstract The most sensitive analytical wavelengths of boron cannot be used in the determination of boron in fertilizers by inductively coupled plasma-atomic emission spectrometry because of spectral interference by potassium, phosphorus, and iron. For the 4 wavelengths of boron investigated, it was noticed that, at the same wavelength, the pattern of spectral interference changes according to fertilizer composition. The spectral interference patterns at the 4 analytical boron wavelengths were studied by adding matrix elements typically found in fertilizers to real fertilizer samples. When levels of added matrix elements correlate less than 0.2 to each other, the effect of added matrix eleme…
Recent progress in high pressure X-ray absorption spectroscopy studies at the ODE beamline
2020
I.J. and A.K. are grateful to the Latvian Council of Science project no. lzp-2018/2-0353 for financial support. The research leading to these results has been partially supported by the project CALIPSOplus under the Grant Agreement No. 730872 from the EU Framework Programme for Research and Innovation HORIZON 2020.
X-ray absorption near edge spectroscopy of thermochromic phase transition in CuMoO4
2018
Thermochromic phase transition was studied in CuMoO4 using the Cu and Mo K-edge x-ray absorption spec-troscopy in the temperature range of 10-300 K. The hysteretic behavior has been evidenced from the tempera-ture dependence of the pre-edge shoulder intensity at the Mo K-edge, indicating that the transition from brown-ish-red γ-CuMoO4 to green α-CuMoO4 occurs in the temperature range of 230-280 K upon heating, whereas the α-to-γ transition occurs between 200 and 120 K upon cooling. Such behavior of the pre-edge shoulder at the Mo K-edge correlates with the change of molybdenum coordination between distorted tetrahedral in α-CuMoO4 and distorted octahedral in γ-CuMoO4. This result has been s…
Low temperature X-ray absorption spectroscopy study of $CuMoO_{4}$ and $CuMo_{0.90}W_{0.10}O_4$ using reverse Monte-Carlo method
2020
Radiation physics and chemistry 175, 108411 (2020). doi:10.1016/j.radphyschem.2019.108411
Direct determination of total mercury in phosphate rock using alkaline fusion digestion
2014
The aim of this work was to develop a new method to determine the mercury (Hg) concentrations in phosphate rock using a dedicated analytical instrument (the DMA80 Tricell by Milestone) that employs an integrated sequence of thermal decomposition followed by catalyst conversion, amalgamation and atomic absorption spectrophotometry. However, this instrument underestimates Hg concentrations when phosphorite and apatite rocks are investigated with a classic thermal decomposition treatment that complies with US EPA method 7473. Therefore, to improve the recovery of total Hg, we performed alkaline fusion digestion (AFD) directly inside the furnace of the instrument, using BCR(32) as a certified r…