Search results for " diffraction"
showing 10 items of 896 documents
XRMA analysis and X-ray diffraction analysis of dental enamel from human permanent teeth exposed to hydrogen peroxide of varying pH
2019
Background This in vitroinvestigation shows how 3.3% H2O2, at different pH-values affects the enamel. Material and Methods A number of fifteen human premolars were used. The enamel of the coronal half in six of the teeth, were exposed by H2O2. Nine teeth were prepared to enamel powder. The enamel was exposed to 3.3% H2O2, at six different pH-values (pH range 4.5 - 7.0). Analyses of the topography of enamel performed by scanning electron microscope (SEM) and the chemical composition of enamel by X-ray microanalysis (XRMA). X-ray powder diffraction (XRD) analysed the crystallinity in enamel powder. Results The exposure to H2O2 at pH5.5 resulted in a decrease of O in the exposed enamel, and ch…
Studies on atomic layer deposition of IRMOF-8 thin films
2015
Deposition of IRMOF-8 thin films by atomic layer deposition was studied at 260–320 C. Zinc acetate and 2,6-naphthalenedicarboxylic acid were used as the precursors. The as-deposited amorphous films were crystallized in 70% relative humidity at room temperature resulting in an unknown phase with a large unit cell. An autoclave with dimethylformamide as the solvent was used to recrystallize the films into IRMOF-8 as confirmed by grazing incidence x-ray diffraction. The films were further characterized by high temperature x-ray diffraction (HTXRD), field emission scanning electron microscopy, Fourier transform infrared spectroscopy (FTIR), time-of-flight elastic recoil detection analysis (TOF-…
Understanding seismic path biases and magmatic activity at Mount St Helens volcano before its 2004 eruption
2020
SUMMARY In volcanoes, topography, shallow heterogeneity and even shallow morphology can substantially modify seismic coda signals. Coda waves are an essential tool to monitor eruption dynamics and model volcanic structures jointly and independently from velocity anomalies: it is thus fundamental to test their spatial sensitivity to seismic path effects. Here, we apply the Multiple Lapse Time Window Analysis (MLTWA) to measure the relative importance of scattering attenuation vs absorption at Mount St Helens volcano before its 2004 eruption. The results show the characteristic dominance of scattering attenuation in volcanoes at lower frequencies (3–6 Hz), while absorption is the primary atte…
Heptane adsorption in silicalite-1 : molecular dynamics simulation.
2009
Molecular dynamics (MD) simulations have been used to study the adsorption process of n-heptane molecules in silicalite-1 at 300 K. MD simulated results were compared to experimental neutron diffraction (ND) and experimental self-diffusion coefficients. The analysis of MD data indicated a packing of the adsorbed molecules around 4 mol./u.c., which is not the consequence of an enthalpic effect but of an entropic effect. The role of the n-heptane chain flexibility (cis–trans conformation) in relation with the silicalite-1 channel type (straight versus sinusoidal) was outlined and enabled to understand the mobility change arising at 4 mol./u.c., according to previous experimental results. The …
Acidic Monosaccharides become Incorporated into Calcite Single Crystals*.
2020
Streptococcus suis is an encapsulated bacterium and one of the most important swine pathogens and a zoonotic agent for which no effective vaccine exists. Bacterial capsular polysaccharides (CPSs) are poorly immunogenic, but anti-CPS antibodies are essential to the host defense against encapsulated bacteria. In addition to the previously known serotypes 2 and 14, that are non-immunogenic, we have recently purified and described the CPS structures for serotypes 1, 1/2, 3, 7, 8, and 9. Here, we aimed to elucidate how these new structurally diverse CPSs interact with the immune system to generate anti-CPS antibody responses. CPS-stimulated dendritic cells produced significant levels of C–C moti…
Nickel(II) 3,4;9,10-perylenediimide bis-phosphonate pentahydrate: A metal-organic ferromagnetic dye
2012
The new metal organic compound nickel(II) 3,4;9,10-perylenediimide bis-phosphonate pentahydrate, i.e. Ni-2[(PDI-BP)-(H2O)(2)]center dot 3H(2)O (1), has been synthesized and its structural and magnetic properties have been studied. Reaction of 3,4;9,10-perylenediimide bisphosphonate (PDI-BP, hereafter) ligand and nickel chloride in water resulted in the precipitation of a red and poorly crystalline solid (1). As the solid shows a poor crystalline organization of aggregates, the energy dispersive X-ray diffraction analysis (EDXD) technique has been used to obtain short-range order structural information of the single nanoaggregates by radial distribution function analysis. The overall structu…
Marble and stone revetment and pavements: Context and provenance
2022
Earlier excavations and survey at Vagnari furnished hardly any evidence for the use of marble at the site, and so the vicus was considered to be a low status settlement, with only a few rooms having been elegant enough to decorate them with marble floors or revetment. The fragments recovered were not analysed scientifically to determine the location of the quarries from which the marbles came. Of particular interest, however, were two small fragments of inscriptions on white marble retrieved from the rubble fill dumped in the 4th century AD in the reservoir. These originally may have been attached, when intact, to votive or funerary monuments, suggesting that the occasional commemorative mo…
Space-variant simultaneous detection of several objects by the use of multiple anamorphic fractional-Fourier-transform filters.
2010
A fractional correlator that is based on the anamorphic fractional Fourier transform is defined. This new, to our knowledge, correlator has been extended to work with multiple filters. The novelty introduced by the suggested system is the possibility of the simultaneous detection of several objects in different parts of the input scene (when anamorphic optics are dealt with), thereby permitting an independent degree of space invariance in two perpendicular directions. Computer experiments as well as experimental optical implementation are presented.
Radon–Wigner display: a compact optical implementation with a single varifocal lens
2008
A new optical implementation of the Radon‐Wigner display for one-dimensional objects is presented, making use of the fractional Fourier transform approach. The proposed setup makes use of only two conventional refractive elements: a cylindrical lens and a varifocal lens. Although the exact magnifications cannot be achieved simultaneously for all the fractional transforms, an optimum design can be obtained through balancing the conflicting magnification requirements. Experimental results are obtained with a commercially available progressive addition lens. For comparison, computer simulations are also provided. © 1997 Optical Society of America
Depth-of-Field Enhancement in Integral Imaging by Selective Depth-Deconvolution
2014
One of the major drawbacks of the integral imaging technique is its limited depth of field. Such limitation is imposed by the numerical aperture of the microlenses. In this paper, we propose a method to extend the depth of field of integral imaging systems in the reconstruction stage. The method is based on the combination of deconvolution tools and depth filtering of each elemental image using disparity map information. We demonstrate our proposal presenting digital reconstructions of a 3-D scene focused at different depths with extended depth of field.