Search results for " layer"
showing 10 items of 1022 documents
Surface debris of canal walls after post space preparation in endodontically treated teeth: A scanning electron microscopic study
2004
Abstract Purpose To evaluate surface cleanliness of root canal walls along post space after endodontic treatment using 2 different irrigant regimens, obturation techniques, and post space preparation for adhesive bonding. Study design Forty teeth, divided into 4 groups, were instrumented, using Ni-Ti rotary files, irrigated with NaOCl or NaOCl + EDTA and obturated with cold lateral condensation (CLC) or warm vertical condensation (WVC) of gutta-percha. After post space preparation, etching, and washing procedure, canal walls were observed using a scanning electron microscope (SEM). Amount of debris, smear layer, sealer/gutta-percha remnants, and visibility of open tubules were rated. Result…
A numerical model of the cloud-topped planetary boundary-layer: influence of the physico-chemical properties of aerosol particles on the effective ra…
2000
The present investigation deals with the impact of different aeorosol types on the value of the effective radius of stratiform clouds. In several numerical sensitivity studies with the microphysical stratus model MISTRA, the aerosol composition was linearly changed from pure maritime to pure rural aerosol particles. Numerical results show that in environments with pure maritime aerosols, the effective radius is usually much larger than in continental regions. Values of the effective radius are also time-dependent with minima and maxima during day and night, respectively. In precipitating clouds, the effective radius might achieve values larger than 30 μm. In continental regions, the effecti…
The effect of hydration layers on the anodic growth and on the dielectric properties of Al2O3 for electrolytic capacitors
2014
Hydrous films were grown on high purity and cubicity Al foils for electrolytic capacitors in deionized water, ethylene glycol - deionized water and in glycerol - deionized water for different immersion times. According to the X-ray diffraction patterns the hydration treatment allowed to grow a pseudo boehmite layer on Al surface whose morphology is appreciably affected by the bath composition. Capacitance measurements and photoelectrochemical findings suggest that a more compact barrier layer forms during the immersion in alcohol containing solutions. The hydration in water allowed to save energy and to prepare more blocking oxide films. The beneficial effect of hydration in hot water on th…
Strongly-coupled PbS QD solids by doctor blading for IR photodetection
2016
Solution-processed QD solids are emerging as a novel concept for high-performance optoelectronic devices. In this work, doctor blading is proposed for the fabrication of strongly-coupled QD solids from a PbS nanoink for photodetection at telecom wavelengths. The key step of this procedure is the solid-state ligand exchange, which reduces the interparticle distance and increases the carrier mobility in the resulting strongly-coupled QD solid. This is accomplished by replacing the original long oleylamine molecules by shorter molecules like 3-mercaptopropionic acid, as confirmed by FTIR, TGA and XPS. Further, a detailed investigation with XPS confirms the air-stability of the QD solids and th…
Increased conductivity of a hole transport layer due to oxidation by a molecular nanomagnet
2008
Thin film transistors based on polyarylamine poly?N,N?-diphenyl-N,N ?bis?4-hexylphenyl?- ?1,1?biphenyl?-4,4?-diamine ?pTPD? were fabricated using spin coating in order to measure the mobility of pTPD upon oxidation. Partially oxidized pTPD with a molecular magnetic cluster showed an increase in mobility of over two orders of magnitude. A transition in the mobility of pTPD upon doping could also be observed by the presence of a maximum obtained for a given oxidant ratio and subsequent decrease for a higher ratio. Such result agrees well with a previously reported model based on the combined effect of dipolar broadening of the density of states and transport manifold filling. Peer Reviewed
A new neuraminic acid derivative and three types of glycopeptides isolated from the Cuvierian tubules of the sea cucumber Holothuria forskali
1973
The Cuvierian tubules of Holothuria forskali Della Chiaje, a sea cucumber found in the Adriatic Sea, were investigated with regard to their carbohydrate moieties. From a Pronase digest of these tubules three types of carbohydrate units were isolated and characterized. 1. A high-molecular-weight glycopeptide fraction was shown to contain sulphated polyfucose, galactosamine, a uronic acid and a previously unknown neuraminic acid derivative. The sulphate was shown by i.r. analysis to be present as an O-ester. The carbohydrate unit was linked O-glycosidically to threonine and serine residues in the polypeptide chain. The hitherto unknown neuraminic acid derivative (Hf-neuraminic acid) was resis…
Ovicide-induced serosa degeneration and its impact on embryonic development in Manduca sexta (Insecta: Lepidoptera)
2003
Abstract Eggs of Manduca sexta treated with the ovicide Ov. 165049 turn orange, and the embryos later die. The orange pigmentation is at first confined to the serosa, and is accompanied by pathological changes of serosal cells. Lipid vesicles aggregate and spindle-shaped electron-lucent vesicles—normally forming a single layer below the apical cell surface—greatly accumulate. The mitochondria swell considerably, and their matrices become electron-lucent. Subsequently, the serosal cells develop additional features of necrosis. They form many autophagic vacuoles which contain mostly degradating mitochondria, but also segregated rough endoplasmic reticulum (rER) and glycogen granules. The whol…
Finite element modelling of temperature distribution in the cutting zone in turning processes with differently coated tools
2005
Abstract The aim of this study is to check the applicability of various simulation models to obtain finite element solutions of cutting forces, specific cutting energy and adequate temperatures for a range of coated tool materials and defined cutting conditions. Commercial explicit finite element code Thirdwave AdvantEdge has been used in simulations of orthogonal cutting processes performed by means of uncoated carbide and coated tools. The latter were equipped with progressively increasing number of thin layers including TiC, TiN and Al 2 O 3 films deposited onto ISO P20 carbide substrates. Results showing the tool–chip interfacial friction influencing the temperature distribution fields,…
Experimental characterisation of the CIRA plasma wind tunnel SCIROCCO test section
2008
Abstract During the Validation Phase of the CIRA-PWT SCIROCCO Facility located at Capua (Italy), a test campaign has been carried out to verify the performances of the facility with the use of the two conical nozzle configurations “D” and “F” with exit diameters are, respectively of, 1150 and 1950 mm. For the first time the data results of the tests have been used to characterize the plasma flow in the test section of the facility. In particular, analytical relationships between the main thermo-fluid-dynamic parameters in the test section and the reservoir conditions of the facility have been found, and compared to the CFD prediction developed during the Design Phase of the facility. Very i…
PCM Thermal Energy Storage in Buildings: Experimental Study and Applications
2015
Abstract The study aims at analyzing the performance of Phase Change Materials (PCMs) in residential housing for different climates. This paper presents the results of an experiment performed in the Concordia University Solar Simulator and Environmental Chamber research facility (SSEC, Montreal, Canada). PCM boards were embedded on the back wall of a test hut placedin the climatic chamber. Several experiments were performed to explore the potential for verification of the proposed analysis and to produce enough data to perform model calibrations. Results show a strong increase in the apparent thermal inertia of the room allowing for a reduction in daily temperature fluctuations in the test …