Search results for " mill"

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A sustainable phenolic compound extraction system from olive oil mill wastewater

2017

Abstract The reduction of environmental impact and the achievement of economic advantages based on by-product recovery is the aim of applying methodologies for phenolic compounds extraction from Olive Oil Mill Wastewater. Volume reduction of Olive Oil Mill Wastewater could generate important advantages in terms of waste disposal cost abatement and, in addition, reuse in the production of foods with health properties could lead to economic benefits. Despite the fact that literature shows that several techniques have been developed, few economic approaches have been presented. This paper assesses the economic feasibility of a system based on membrane filtration and reverse osmosis processes f…

Correlation between milling parameters and microstructure characteristics of nanocrystalline copper powder prepared via a high energy planetary ball …

2007

The microstructure evolution of Cu-nanostructured powders versus the ball milling conditions was investigated by whole peak profile powder pattern modeling method. This method allows defining in some approach the characteristics of as-milled Cu powder microstructure in terms of crystallite size, type and density of dislocations and twin faults density. It is shown that the change of microstructure characteristics of as-milled Cu powder versus the ball milling conditions (under constant time of the ball milling) depend on only some energy parameters of the milling, for example, average size of crystallite is uniquely defined by energy of the shock, whereas the portion of edge and screw compo…

Local structure of ball-milled LaNi5 hydrogen storage material by Ni K-edge EXAFS

2010

Abstract Local structure of the nanostructured LaNi5 hydrogen storage alloys, prepared by ball-milling, has been studied using Ni K-edge extended X-ray absorption fine structure spectroscopy. Results indicate that the ball-milling up to 100 h results in the production of nanoparticles characterized by large atomic disorder and slightly reduced unit-cell volume, compared to the bulk LaNi5. High temperature annealing appears to help in partial recovery of atomic order in the ball-milled samples; however, long-time ball-milled samples retain large disorder even after the high temperature annealing. The results suggest that the large disorder and the reduced unit-cell volume might be causing a …

Effect of Ni content on the structure and hydrogenation property of mechanically alloyed TiMgNix ternary alloys

2017

Abstract In this study, TiMgNix samples (x = 0.2, 0.4, 0.6, 0.8, 1) have been prepared by mechanical alloying using a planetary high-energy ball mill. The structural transformations were characterized by XRD and indicated that all the as-milled TiMgNix alloys consist of mixtures of crystalline Mg and amorphous Ti-Ni-(Mg) phase. TEM analyses also show that nanocrystallites and amorphous phases coexist in the as-milled TiMgNi alloy. Electrochemical test shows that the TiMgNi composition yields the highest discharge capacity. The discharge capacities and activation properties of TiMgNix alloys linearly increase with increasing Ni content. The MgTiNi0.8 composition boasts the best cycling prope…

Influence of the high energy ball milling on structure and reactivity of the Ni+Al powder mixture

2013

Abstract Investigation of the micro- and atomic structures for the planetary ball-milled Ni + Al mixtures has revealed existence of intermediate nano-crystalline and amorphous phases, which are not detectable by XRD analysis, but can be observed by means of HRTEM. Annealing of the milled mixtures at moderate temperature, 205–280 °C, transforms the nano-phases into crystal state and makes them XRD-detectable. These nano-scale structures may serve as nucleus for the intermetallic phases produced via reaction between Ni and Al and, therefore, decrease the activation energy of this reaction and diminish the temperature of the reaction initiation. Apparently, the active nano-phases are formed du…

The Grinding Resistance of the Wheat Grain Related to the Grinding Degree For The First Break In The Wheat Milling

2011

Breakage of wheat grain during first break roller milling depends on the characteristics of the wheat (including the distributions of kernel size, hardness and moisture content) and on the design and operation of the roller mill (including roll speeds and differential, roll disposition, fluting profile, number of flutes, fluting spiral, roll gap, the degree of roll wear and the feed rate). The effects of these factors are manifest in the particle size distribution exiting first break, the compositional distribution of those particles (as large particles tend to be richer in bran, while small particles are pure endosperm), the power required to mill the wheat and the rate of roll wear. For t…

Influence of mechanical activation on the physical stability of salbutamol sulphate.

2003

Abstract In order to obtain the optimal particle size distribution for pharmaceutical powders in dry powder inhalers the particles have to be micronised. In most cases the process of micronisation is connected with a high input of energy which induces disorder and defects on the surface of the drug particles and as a result changes in the crystallinity. Consequently, changes in the physical stability of the powders may occur. To investigate changes on the physical stability of the powder, different analytical methods are used in the present investigation: laser diffraction, Differential Scanning Calorimetry (DSC), isothermal microcalorimetry and DVS-method. Air-jet-milling is one of the mos…

Enhancement of self-sustaining reaction Cu3Si phase formation starting from mechanically activated powders

2000

Mechanical high-energy ball milling of an 3Cu Si elemental powders mixture was used to activate a self-sustaining combustion reaction or so-called self-sustaining high-temperature synthesis (SHS) to form the copper silicide phase, a reaction for which the thermodynamic criterion proposed by Munir for self-propagation reaction is not favorable. A complete characterization of the end-products was performed with X-ray diffraction analysis and scanning electron microscopy. Thermal and structural information describing the combustion front initiated by heating up a sample to 180°C in a Cu:Si system is communicated. This paper clearly shows that the mechanically activated self-sustaining high-tem…