Search results for "3-triazole"

showing 10 items of 42 documents

Cellulose‑copper as bio-supported recyclable catalyst for the clickable azide-alkyne [3 + 2] cycloaddition reaction in water.

2018

Abstract Naturally-occurring cellulose has been employed as a bio-support macromolecule for the immobilization of either copper(I) or copper(II) ions in order to click azide and alkyne derivatives in water. Under such a click regime, 1,4-disubstitued-1,2,3-triazoles were obtained regioselectively in excellent yields at room temperature. The reaction work-up is simple and the bio-heterogeneous catalyst that has been fully characterized by AAS, SEM, EDX and FT-IR can be easily separated and reused at least five times without any significant decrease in its activity and selectivity, particularly in the case of the very stable CuI-Cellulose.

Azides123-TriazoleAlkynechemistry.chemical_element010402 general chemistry01 natural sciencesBiochemistryCatalysisCatalysischemistry.chemical_compoundStructural BiologyPolymer chemistrySpectroscopy Fourier Transform InfraredCelluloseCelluloseMolecular Biologychemistry.chemical_classificationCycloaddition Reaction010405 organic chemistryChemistryWaterGeneral MedicineCopperCycloaddition0104 chemical sciencesAlkynesClick chemistrySolventsClick ChemistryAzideCopperInternational journal of biological macromolecules
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1,5-Disubstituted 1,2,3-Triazoles as Amide Bond Isosteres Yield Novel Tumor-Targeting Minigastrin Analogs.

2021

[Image: see text] 1,5-Disubstituted 1,2,3-triazoles (1,5-Tz) are considered bioisosteres of cis-amide bonds. However, their use for enhancing the pharmacological properties of peptides or proteins is not yet well established. Aiming to illustrate their utility, we chose the peptide conjugate [Nle(15)]MG11 (DOTA-dGlu-Ala-Tyr-Gly-Trp-Nle-Asp-Phe-NH(2)) as a model compound since it is known that the cholecystokinin-2 receptor (CCK2R) is able to accommodate turn conformations. Analogs of [Nle(15)]MG11 incorporating 1,5-Tz in the backbone were synthesized and radiolabeled with lutetium-177, and their pharmacological properties (cell internalization, receptor binding affinity and specificity, pla…

Biodistribution3-TriazolesStereochemistryPeptidomimeticmedia_common.quotation_subject1201 natural sciencesBiochemistryTurn (biochemistry)Drug Discovery[CHIM]Chemical SciencesPeptide bondInternalizationReceptorCancermedia_commonTumor Targeting[CHIM.ORGA]Chemical Sciences/Organic chemistry010405 organic chemistryChemistry123-Triazoles; Peptidomimetics; Structure−activity relationships; Radiopharmaceuticals; Tumor targeting; CancerStructure-Activity RelationshipsOrganic ChemistryBiological activity0104 chemical sciences010404 medicinal & biomolecular chemistryYield (chemistry)PeptidomimeticsRadiopharmaceuticalsACS medicinal chemistry letters
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CCDC 766325: Experimental Crystal Structure Determination

2010

Related Article: L.Kiss, E.Forro, R.Sillanpaa, F.Fulop|2010|Tetrahedron|66|3599|doi:10.1016/j.tet.2010.03.030

Ethyl 1-((1R*2R*3R*4R*)-3-((t-butoxycarbonyl)amino)-4-(ethoxycarbonyl)-2-hydroxycyclopentyl)-1H-123-triazole-4-carboxylateSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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Insight into non-nucleoside triazole-based systems as viral polymerases inhibitors

2023

Viruses have been recognized as the etiological agents responsible for many pathological conditions ranging from asymptomatic infections to serious diseases, even leading to death. For this reason, many efforts have been made to identify selective viral targets with the aim of developing efficient therapeutic strategies, devoid of drug-resistance issues. Considering their crucial role in the viral life cycle, polymerases are very attractive targets. Among the classes of compounds explored as viral polymerases inhibitors, here we present an overview of non-nucleoside triazole-based compounds identified in the last fifteen years. Furthermore, the structure-activity relationships (SAR) of the …

PharmacologyOrganic ChemistryDrug Discovery123-TriazolesNon-nucleosides antiviral agentsViral polymerasesGeneral MedicineAntiviral therapy124-TriazolesEuropean Journal of Medicinal Chemistry
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Copper(II)-dipicolinate-mediated clickable azide–alkyne cycloaddition in water as solvent

2018

Copper(II)-dipicolinate complex [CuIIL(H2O)2] (1) (H2L = dipicolinic acid (H2dipic)) was synthesized via oxidation of copper(I) iodide and pyridine-2,6-dicarboxylic acid in water and acetonitrile in the presence of glycine. Complex 1 was characterized by FT-IR and elemental analysis and its structure confirmed by single crystal X-ray analysis. This complex is an efficient precatalyst that mediates azide-alkyne cycloaddition reactions in water at room temperature either in the absence or presence of a reducing agent. Compound 1-mediated azide-alkyne cycloaddition affords alkyl/aryl substituted 1,2,3-triazole heterocycles in a regioselective manner and excellent yields under very mild reactio…

Reducing agent3-TriazolesIodide12Alkyne010402 general chemistry01 natural scienceschemistry.chemical_compoundPolymer chemistryMaterials Chemistry[CHIM.COOR]Chemical Sciences/Coordination chemistryPhysical and Theoretical ChemistryAcetonitrilechemistry.chemical_classification010405 organic chemistryChemistryClick chemistry[CHIM.ORGA]Chemical Sciences/Organic chemistryAryl[CHIM.CATA]Chemical Sciences/CatalysisAzide-alkyne cycloadditionCycloaddition0104 chemical sciencesDipicolinic acidClick chemistryAzideCopperHomogenous catalysis
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CCDC 2005162: Experimental Crystal Structure Determination

2021

Related Article: Argha Saha, Srimanta Guin, Wajid Ali, Trisha Bhattacharya, Sheuli Sasmal, Nupur Goswami, Gaurav Prakash, Soumya Kumar Sinha, Hediyala B. Chandrashekar, S. S. Anjana, Debabrata Maiti|2021|Cell Press: Chem|7|948|doi:10.1016/j.chempr.2021.01.003

Space GroupCrystallography(22'-bipyridine)-(1-methyl-1H-123-triazole)-silver hexafluorophosphateCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1522079: Experimental Crystal Structure Determination

2017

Related Article: Mikk Kaasik, Sandra Kaabel, Kadri Kriis, Ivar Järving, Riina Aav, Kari Rissanen, Tönis Kanger|2017|Chem.-Eur.J.|23|7337|doi:10.1002/chem.201700618

Space GroupCrystallography4-(35-bis(trifluoromethyl)phenyl)-5-iodo-1-(1-phenylethyl)-1H-123-triazoleCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1953273: Experimental Crystal Structure Determination

2020

Related Article: Jérôme Bayardon, Benjamin Rousselle, Yoann Rousselin, Quentin Bonnin, Raluca Malacea-Kabbara|2020|Eur.J.Org.Chem.|2020|4723|doi:10.1002/ejoc.202000723

Space GroupCrystallographyCrystal SystemCrystal Structure(4-{2-[(2-methoxyphenyl)(phenyl)phosphanyl]phenyl}-1-phenyl-1H-123-triazole)-allyl-palladium hexafluorophosphate dichloromethane solvateCell ParametersExperimental 3D Coordinates
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CCDC 786367: Experimental Crystal Structure Determination

2011

Related Article: P.Ramirez-Lopez, M.C.de la Torre, M.Asenjo, J.Ramirez-Castellanos, J.M.Gonzalez-Calbet, A.Rodriguez-Gimeno, C.R.de Arellano, M.A.Sierra|2011|Chem.Commun.|47|10281|doi:10.1039/c1cc13251b

Space GroupCrystallographyCrystal SystemCrystal Structure33'-(14-Phenylenebis(methylene-1H-123-triazole-14-diylmethyleneoxy))bisestra-135(10)-trien-17-ol chloroform solvateCell ParametersExperimental 3D Coordinates
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CCDC 2062093: Experimental Crystal Structure Determination

2021

Related Article: Jas S. Ward, Antonio Frontera, Kari Rissanen|2021|Inorg.Chem.|60|5383|doi:10.1021/acs.inorgchem.1c00409

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameters(44'-dimethyl-22'-bipyridine)-(1-methyl-1H-123-triazole)-silver hexafluorophosphate dichloromethane solvateExperimental 3D Coordinates
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