Search results for "Alkanesulfonates"

showing 2 items of 2 documents

Supramolecular Aggregates in Vacuum: Positively Mono-Charged Sodium Alkanesulfonate Clusters

2010

The formation and structural features of positively mono-charged aggregates of sodium bis(2-ethylhexyl) sulfosuccinate (AOT) and sodium methane—(MetS), butane—(ButS) and octane—(OctS) sulfonate molecules in the gas phase have been investigated by electrospray ionization mass spectrometry, energy-resolved mass spectrometry and density functional theory (DFT) calculations. The experimental results show that the center-of-mass collision energy required to dissociate 50% of these mono-charged aggregates scantly depends on the length of the alkyl chain as well as on the aggregation number. This, together with the large predominance of mono-charged species in the mass spectra, was rationalized i…

AlkanesulfonatesSpectrometry Mass Electrospray IonizationAmphiphilic moleculeVacuumChemistryElectrospray ionizationSodiumSodiumSupramolecular chemistrychemistry.chemical_elementGeneral MedicineAtomic and Molecular Physics and Opticschemistry.chemical_compoundSulfonateTandem Mass SpectrometrySupramolecular aggregates amphiphilic molecules surfactants reversed micelles ESI MS ESI MS/MS energy resolved mass spectrometry DFT calculationsQuantum TheoryOrganic chemistrySpectroscopyEuropean Journal of Mass Spectrometry
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Characterization and quantitation of mixtures of alkyl ether sulfates and carboxylic acids by capillary electrophoresis with indirect photometric det…

2003

The separation, characterization, and determination of mixtures of alkyl ether sulfates (AES) and fatty acids (C10-C16) in background electrolytes (BGEs) containing acetonitrile (ACN)-water mixtures is addressed. Due to inhibition of the ionization of the carboxylate groups, the migration time and the resolution between the fatty acids decreased when the water content of the BGE was reduced, but efficiency and resolution between the AES oligomers improved. The migration times increased and resolution improved by substituting 5% ACN by an equivalent amount of dioxane. A complete separation of the two surfactant classes, up to the AES oligomers with 8 ethylene oxide units (EOs) with respect t…

Alkanesulfonateschemistry.chemical_classificationDetection limitMolar concentrationChromatographyEthylene oxideCalibration curveFatty AcidsClinical BiochemistryCarboxylic AcidsElectrophoresis CapillaryBiochemistryOligomerAnalytical ChemistryMolecular WeightSurface-Active Agentschemistry.chemical_compoundCapillary electrophoresischemistryCalibrationSolventsCarboxylateAlkylELECTROPHORESIS
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