Search results for "Brushite"

showing 4 items of 4 documents

Galvanic deposition and characterization of brushite/hydroxyapatite coatings on 316L stainless steel

2016

In this work, brushite and brushite/hydroxyapatite (BS, CaHPO4·H2O; HA, Ca10(PO4)6(OH)2) coatings were deposited on 316L stainless steel (316LSS) from a solution containing Ca(NO3)2·4H2O and NH4H2PO4 by a displacement reaction based on a galvanic contact, where zinc acts as sacrificial anode. Driving force for the cementation reaction arises from the difference in the electrochemical standard potentials of two different metallic materials (316LSS and Zn) immersed in an electrolyte, so forming a galvanic contact leading to the deposition of BS/HA on nobler metal. We found that temperature and deposition time affect coating features (morphology, structure, and composition). Deposits were char…

Calcium PhosphatesMaterials scienceGalvanic anodeScanning electron microscopeMaterials ScienceEnergy-dispersive X-ray spectroscopyBioengineering02 engineering and technologyCondensed Matter Physicengineering.material010402 general chemistry01 natural sciencesCorrosionHydroxyapatiteBiomaterialssymbols.namesakeCoatingGalvanic cellBrushiteMechanical EngineeringMetallurgyBiomedical applicationElectrochemical Techniques021001 nanoscience & nanotechnologyStainless Steel0104 chemical sciencesGalvanic depositionDurapatiteSettore ING-IND/23 - Chimica Fisica ApplicataChemical engineeringMechanics of Materialsengineeringsymbols316LSSBrushite0210 nano-technologyRaman spectroscopy
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Calcium phosphate/polyvinyl acetate coatings on SS304 via galvanic co-deposition for orthopedic implant applications

2021

Abstract In this work, the galvanic deposition method is used to deposit coatings of brushite/hydroxyapatite/polyvinyl acetate on 304 stainless steel. Coatings are obtained at different temperatures and with different sacrificial anodes, consisting of a mixture of brushite and hydroxyapatite. Samples are aged in a simulated body fluid (SBF), where a complete conversion of brushite into hydroxyapatite with a simultaneous change in morphology and wettability occurred. The corrosion tests show that, compared with bare 304, the coating shifts Ecorr to anodic values and reduces icorr Ecorr, and icorr has different values at different aging times due to chemical interactions at the solid/liquid i…

Materials scienceGalvanic anodeCytotoxicitySimulated body fluidPolyvinyl acetate02 engineering and technologyengineering.material010402 general chemistry01 natural sciencesHydroxyapatiteCorrosionchemistry.chemical_compoundCoatingMaterials ChemistryGalvanic cellBrushiteOrthopedic implantsSettore ING-IND/24 - Principi Di Ingegneria ChimicaPolyvinyl acetateSettore ING-IND/34 - Bioingegneria IndustrialeSurfaces and InterfacesGeneral Chemistry021001 nanoscience & nanotechnologyCondensed Matter Physics0104 chemical sciencesSurfaces Coatings and FilmsAnodeCorrosionGalvanic depositionSettore ING-IND/23 - Chimica Fisica ApplicataChemical engineeringchemistryengineering0210 nano-technologySurface and Coatings Technology
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Brushite/Hydroxyapatite Coatings obtained by galvanic deposition on 316L Stainless Steel

2016

Hydroxyapatite (HA, Ca10(PO4)6(OH)2) is a basic calcium phosphate mineral with chemical composition similar to that of bones and teeth. Owing to this peculiarity HA is a biocompatible material of high medical interest. Unfortunately, it possesses poor mechanical properties, because is brittle, has a low fracture resistance and a poor wear resistance. For these reasons, in the last years the research was been focused on the use of HA as a coating of another biomaterial that acts as support. The best choice is that to use a substrate that must be bionert and mechanically stable, such as 316L stainless steel (316LSS). This is useful for biomedical implants, because of its excellent biocompatib…

Settore ING-IND/23 - Chimica Fisica ApplicataBrushite/Hydroxyapatite Coatings galvanic deposition 316L Stainless Steel
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In vitro corrosion and biocompatibility of brushite/hydroxyapatite coatings obtained by galvanic deposition on 316LSS

2018

Corrosion behavior and cytotoxicity was reported for mixed brushite (BS)/hydroxyapatite (HA) coatings deposited on 316LSS substrate through a displacement reaction. Corrosion tests, carried out in a simulated body fluid, showed that in comparison with bare 316L, coating shifts Ecorrto anodic values and reduces icorreven if oscillations were observed, which were explained in terms of the chemical interactions at the solid/liquid interface. Cell biocompatibility of the coating was investigated through osteoblastic cell line MC3T3-E1, evidencing the absence of any cytotoxicity Taken together, the results show that galvanic deposition is a simple and cost-effective method for producing bioactiv…

Solid-state chemistryMaterials scienceBiocompatibilitySurfaces Coatings and Film02 engineering and technology010402 general chemistryElectrochemistry01 natural sciencesCorrosionGalvanic depositionElectrochemistryMaterials ChemistryBrushiteOrthopedic devicesSettore ING-IND/24 - Principi Di Ingegneria ChimicaRenewable Energy Sustainability and the EnvironmentMetals and Alloys021001 nanoscience & nanotechnologyCondensed Matter Physics0104 chemical sciencesSurfaces Coatings and FilmsElectronic Optical and Magnetic MaterialsCorrosionSettore ING-IND/23 - Chimica Fisica ApplicataChemical engineeringHydroxyapatite coatingBiocompatibility0210 nano-technologyOrthopedic device
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