Search results for "Calibration"
showing 10 items of 890 documents
On-line photochemical derivatization and flow-injection spectrophotometric determination of ergonovine maleate
1993
Abstract A flow-injection manifold is proposed for the on-line photochemical derivatization of ergonovine maleate with application to pharmaceutical formulations. The procedure is based on the reaction with p-dimethylaminobenzaldehyde in presence of iron(III) and sulphuric acid medium. The reaction rate is improved by irradiation of the solution with a mercury lamp (254.0 nm). The calibration graph is linear over the range 3–74 μg ml−1 ergonovine, with a mid-range R.S.D. of 1.7% and a sample throughput of 34 h−1. The influence of foreign compounds was tested.
Toward more realistic viscosity measurements of tyre rubber–bitumen blends
2014
AbstractThe measurement of rheological properties of the tyre rubber bitumen blends is often challenging due to presence of suspended tyre rubber’s crumbs. Furthermore, the phase separation during the course of measurements makes the viscosity of these non-homogeneous blends difficult to ascertain. In this study, a new dual helical impeller was designed and manufactured to be used with a rotational viscometer in order to have a real-time control of the viscosity while performing a laboratory mixing of the blends. Layer based manufacturing techniques showed to be a convenient method to produce complex shaped impeller prototypes before manufacturing the more expensive stainless steel assembly…
Assessment of Classifiers and Remote Sensing Features of Hyperspectral Imagery and Stereo-Photogrammetric Point Clouds for Recognition of Tree Specie…
2018
Recognition of tree species and geospatial information on tree species composition is essential for forest management. In this study, tree species recognition was examined using hyperspectral imagery from visible to near-infrared (VNIR) and short-wave infrared (SWIR) camera sensors in combination with a 3D photogrammetric canopy surface model based on RGB camera stereo-imagery. An arboretum with a diverse selection of 26 tree species from 14 genera was used as a test area. Aerial hyperspectral imagery and high spatial resolution photogrammetric color imagery were acquired from the test area using unmanned aerial vehicle (UAV) borne sensors. Hyperspectral imagery was processed to calibrated …
CiNetStrain - Wireless Strain Gauge Network - Calibration and Reliability Measurements
2013
Wireless sensor networks can be extended to include numerous different sensing devices. Strain gauges are the most common nondestructive sensing elements for measuring surface strain. This paper discusses the design, for the wireless CiNet network, of a strain gauge measurement system, which would make strain measurements more flexible while opening new targets of application in addition to those that traditional wired strain measuring systems can offer. The calibration and validation of the wireless strain measurements as well as energy consumption issues are also brought under observation.
Assessment of building energy modelling studies to meet the requirements of the new Energy Performance of Buildings Directive
2020
Abstract The cost optimal method (COM) as applied in the Energy Performance of Buildings Directive (EPBD) uses “non-calibrated deterministic reference buildings (RBs)”. Such RBs are defined with single envelope and equipment parameter values, for which calibration with actual building stock energy performance (EP) is not undertaken. Thus, it is not possible to visualise the effect of uncertainties or diversity in the input parameters on cost-optimal level benchmarks and to verify the choice of RBs. The paper proposes an update to the COM via use of “Probabilistic Bayesian calibrated RBs” to handle uncertainties and produce more realistic cost optimal levels to support policy makers in devis…
Chemical separation and MC-ICPMS analysis of U, Th, Pa and Ra isotope ratios of carbonates
2018
Diagenetic alteration of fossil reef corals may have severe effects on the reliability of 230Th/U-ages. The widely applied criteria introduced to test for the reliability of coral 230Th/U-ages are often not sufficient to identify all altered ages. The combination of 230Th/U- with 231Pa/U-dating has been suggested as a promising method to identify altered ages. Furthermore, 226Ra/230Th ratios can provide information about the diagenetic history during the last 10 000 years. Here we present a method to chemically separate U, Th, Pa and Ra from the same aliquot of a carbonate sample. The isotope ratios of our mixed U–Th–Pa–Ra spike are calibrated using a secular equilibrium material treated in…
On-line extraction coupled to liquid chromatographic analysis of hydrophobic organic compounds from complex solid samples-Application to the analysis…
2019
This work investigates the applicability of on-line extraction (OLE) directly coupled to liquid chromatography (LC) for the dynamic extraction of hydrophobic organic compounds from complex solid samples. The method operates within the existing apparatus of the LC by replacing the valve loop with an extraction vessel comprised of an empty guard column loaded with the sample. In this manner, extraction is accomplished by the mobile phase as it flows through the extraction vessel under high pressure without the need for additional apparatus other than those comprising the LC system or additional sample pretreatment steps. The experimental parameters affecting the extraction efficiency of the m…
Determination of the energetic value of fruit and milk-based beverages through partial-least-squares attenuated total reflectance-Fourier transform i…
2005
Abstract The estimation of important nutritional parameters, such as carbohydrates content and energetic value (calories) in commercially available fruit juice and flavour milk shakes has been made by attenuated total reflectance-Fourier transform infrared spectroscopy (ATR-FTIR) using a partial-least-square (PLS) calibration approach. A highly heterogeneous population of 65 samples obtained from the Spanish market, covering fruit juices, flavour milk shakes and milk-added fruit juices was used. The spectral range and the size of the calibration set for building the PLS model have been evaluated. Considering a calibration set comprised of 27 samples, selected via hierarchical cluster analys…
Response of GAFChromic® HD-V2 film dosimeter in 10-300 Gy dose range for radiation testing of electronic devices
2019
The study reported in this paper aimed to investigate the response of a GAFChromic? HD-V2 film dosimeter in the dose range between 10 and 300 Gy, normally used to perform irradiation tests on electronic devices with a 60Co gamma-ray irradiator. The well-defined linearity of response in terms of absorbance as a function of absorbed dose, easiness of handling and data analysis of irradiated dosimeters, reproducibility, stability, and insensitivity to visible light and most of the environmental parameters, make HD-V2 film a flexible, inexpensive and reliable dose measurement device. The study has shown a fogging effect of the dosimeter response since its value changes over time. Strategies and…
The repeatability and reproducibility of calibrating signals generated by Hsu-Nielsen method
2005
During the measurements of the acoustic emission signals taken both in the laboratory and industrial conditions it is necessary to carry out calibration of the measurement paths used. One of the basic calibration methods is the one invented by Hsu-Nielsen, which consists in generating an acoustic signal during breaking a scriber placed in a special head put on an automatic pencil. The paper presents the measurement results of acoustic signals taken at various structural parameters of calibrating heads, which was done to determine their influence on the repeatability of the results obtained. Moreover, the measurements were taken for ten identical, in relation to their geometrical measurement…