Search results for "Characterization"
showing 10 items of 1054 documents
Nature of activating effect of two‐step polymerization of propylene
1999
The prepolymerization effect on propylene polymerization in the presence of a TiCl3‐based catalyst, modified by di‐n‐buthyl ether, was studied. The influence of prepolymerization on the electron spin resonance spectra and morphology of the catalyst, as well as the properties and the morphology of both prepolymer and regular polymerization products, was investigated. The polymer morphology was evaluated through scanning electron microscopy, polymer bulk density, and particle size distribution. Some evidence of the enhancement effect of prepolymerization on the catalyst activity and stereospecificity was obtained. No influence from prepolymerization was observed on molecular weight and its di…
Purification and partial characterization of aminopeptidase from barley (Hordeum vulgare L.) seeds.
2013
Aminopeptidases (EC 3.4.11) are proteolytic enzymes, which hydrolyze one amino acid from N-terminus of peptidic substrates. Inhibitors of plant aminopeptidases can find an application in agriculture as herbicides. Isolation and partial characterization of aminopeptidase from barley (Hordeum vulgare L.) seeds has been described. The enzyme was purified to molecular homogeneity using a six-step purification procedure (precipitation with (NH4)2SO4, followed by chromatography on Sephadex G-25, DEAE-Sepharose, Sephacryl HR 300, Macro-Prep Q and Phenyl-Sepharose HP columns). The enzyme was purified 365-fold with recovery above 18%. The molecular weight of the purified enzyme was determined by SDS…
Expressive character identity of teen lesbian characters on 'Glee' & 'Pretty Little Liars'
2017
Seksuaalivähemmistöjen asema heteronormatiivisessa yhteiskunnassa on puhututtanut ahkerasti muutaman viime vuosikymmenen aikana. Globaalisti seksuaalivähemmistöjä laajalle yleisölle ovat tehneet tutuiksi populaarikulttuuriset valtavirtasisällöt kuten amerikkalaiset elokuvat ja televisiosarjat. Monet nuoret, jotka vasta rakentavat omaa seksuaali-identiteettiään, ammentavat vaikutteita näistä sisällöistä, erityisesti heidän ikäryhmilleen kohdistetuista tuotannoista kuten nuorten sarjoista. Siten on tarpeellista tutkia seksuaalivähemmistöjä edustavien fiktiivisten hahmojen kokonaisvaltaisia representaatioita suosittujen amerikkalaisten nuorten sarjojen kontekstissa ja päivittää tutkimus 1990-l…
Restoration of a XVII Century’s predella reliquary: From Physico-Chemical Characterization to the Conservation Process
2021
We report on the restoration of a XVII century’s predella reliquary, which is a part of a larger setup that includes a wall reliquary and a wooden crucified Christ, both belonging to the church of “Madre Maria SS. Assunta”, in Polizzi Generosa, Sicily, Italy. The historical/artistic and paleographic research was flanked successfully by the scientific objective characterization of the materials. The scientific approach was relevant in the definition of the steps for the restoration of the artefact. The optical microscopy was used for the identification of the wood species. Electron microscopy and elemental mapping by energy-dispersive X-ray (EDX) was successful in the identification of the l…
Production d’hamburger de filet de dorade (Sparus aurata) d’élevage: caractérisation nutritionnelle et sensorielle au cours du shelf-life
2016
Within the framework of the Work Package 5 «Valorisation de l'image des produits aquacoles» and the activity 5.3 «Innovation en vue de valoriser les produits aquacoles» of SecurAqua project, we have assessed the possibility of diversification of Sicilian farmed fish, through the production of processed products, among which seabream fillets hamburgers. In order to verify the feasibility of the process, we have performed a preliminary study of global quality characteristics of the product, including both the nutritional and sensory aspects correlated to the security and sustainability of the product. Results showed that, in terms of nutritional requirements, the hamburger samples maintained …
Monitoring WWTP performance using size-exclusion chromatography with simultaneous UV and fluorescence detection to track recalcitrant wastewater frac…
2018
A trial monitoring of a typical full-scale municipal WWTP in Central Finland was aimed to explore applicability of high performance liquid chromatography – size exclusion chromatography (HPSEC) with simultaneous UV and fluorescence detection as a tool for advanced routine monitoring of wastewater treatment. High, intermediate, and low molecular weight (MW) fractions of untreated wastewater (influent) and treated wastewater (secondary effluent) were characterized in terms of UV absorbance at 254 nm (UVA254) and specific fluorescence representing tyrosine-like, tryptophan-like, and humic/fulvic-like compounds. The activated sludge treatment removed 97 ± 1% of BOD, 93 ± 2% of COD, 71 ± 7% of D…
Characterization of IP-Based Communication for Smart Grid Using Software-Defined Networking
2018
The smart grid (SG) approach is based on a strong interaction between the network communication infrastructure and the power grid. Usually the management of the infrastructure is done by the distribution system operators (DSOs) that are worried about the increasing managing complexity due to the presence of increasing number of distributed energy resources and electrical vehicles. The use of software-defined networking (SDN) may simplify the network configuration and management for DSO, as highlighted from previous research works. The objective of this paper is to introduce and characterize an internet protocol (IP)-based communication architecture with specialized SDN bridges operating als…
Fabrication and Characterization of Dye-Sensitized Solar Cells
2014
Among the next-generation solar cells, a predominant role is played by Dye sensitized solar cells (DSSC) based on ruthenium complexes as sensitizers. They take advantage of a photoelectrochemical system to transform solar radiation into electric energy. In fact, DSSCs represent a cost-effective alternative to traditional silicon-based photovoltaic devices and they do not require expensive and sophisticated apparatus for their fabrication. In this work, we have produced and tested ruthenium DSSCs. In particular, we have measured the main parameters of these cells, such as the electrical and power performances and the efficiency levels, at different irradiance levels and at different incident…
Photoelectric valuation of highly efficient Dye-Sensitized Solar Cells
2015
Nowadays, a growing demand for free and clean energy requires the study and the development of new low-cost solar photovoltaic (PV) cells. Among them, Dye Sensitized Solar Cells (DSSCs) based on ruthenium complexes as sensitizers are assuming a great importance. The DSSCs under study are composed placing in succession a transparent conductive glass on which is screen-printed a mesoporous TiO2 thin film sensitized by a ruthenium based dye (N719) , an electrolytic solution containing a redox couple (I-/I3-) and another conductive glass covered by a thin transparent catalyst platinum film. In this work, we have measured the main photoelectrochemical parameters of the above mentioned DSSCs at d…
Light Soaking measurements on Ruthenium-based Dye Sensitized Solar Cells
2016
An interesting phenomenon occurring in Dye Sensitized Solar Cells (DSSCs) when exposed to an uninterrupted period of illumination is the so-called light soaking effect, which consists in the increase of the main electrical parameters of the cell, such as the photocurrent and the efficiency. Studying such an effect has noteworthy practical implications, ranging from the optimization of the manufacturing process to stability tests of DSSCs. In this paper, we present an experimental investigation on the performance variation, due to light soaking, of Ruthenium-based DSSCs.