Search results for "Chemical Fractionation"

showing 4 items of 54 documents

Chemical speciation of polycyclic aromatic hydrocarbons in sediments: partitioning and extraction of humic substances.

2010

The primary objective of this study was to examine the chemical speciation of polycyclic aromatic hydrocarbons (PAHs) found in sediments endowed with different characteristics. To achieve this purpose and because the nature of the sediments influences the distribution of PAHs, we have analyzed four different types of sediments. To study the role of organic matter in the sequestration of PAHs, we fractionated humic substances into humic acids and humin–mineral fractions. After their separation and purification, the humic components were examined for their sorptive reactivity by extracting them with organic solvents; these extracts were subsequently subjected to GC/MS analysis. Our results sh…

chemistry.chemical_classificationPollutionPersistent organic pollutantGeologic Sedimentsmedia_common.quotation_subjectExtraction (chemistry)Solid Phase ExtractionSedimentFraction (chemistry)PAHsChemical speciationHumicSandy and muddy sedimentsAquatic ScienceChemical FractionationOceanographyPollutionSettore CHIM/12 - Chimica Dell'Ambiente E Dei Beni CulturaliGas Chromatography-Mass SpectrometrySpeciationHydrocarbonchemistryEnvironmental chemistryOrganic matterPolycyclic Aromatic HydrocarbonsHumic Substancesmedia_commonEnvironmental MonitoringMarine pollution bulletin
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Maturation of a Key Resource – The Germanium-68/Gallium-68 Generator: Development and New Insights

2011

(68)Ge/(68)Ga radionuclide generators have been investigated for almost fifty years, since the cyclotron-independent availability of positron emitting (68)Ga via the (68)Ge/(68)Ga system had always attracted researches working in basic nuclear chemistry as well as radiopharmaceutical chemistry. However, it took decades and generations of research (and researchers) to finally reach a level of (68)Ge/(68)Ga radionuclide generator designs adequate to the modern requirements of radiometal labelling chemistry. Nevertheless, most of the existing commercial generator systems address aspects of (68)Ge breakthrough and safe synthesis of (68)Ga radiopharmaceuticals by adopting eluate post-processing …

chemistry.chemical_elementGallium RadioisotopesGermaniumNanotechnologyChemical FractionationRadiology Nuclear Medicine and imagingCation Exchange ResinsProcess engineeringAnion Exchange ResinsEdetic AcidChelating AgentsRadioisotopesPharmacologyGenerator (computer programming)Gallium-68 generatorGermaniumbusiness.industryRadionuclide GeneratorsSolid Phase ExtractionChemical fractionationRadioactivitychemistryPositron-Emission TomographyRadiopharmaceuticalsRadionuclide GeneratorbusinessCurrent Radiopharmaceuticals
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Kaempferol as a dietary anti-inflammatory agent: current therapeutic standing

2020

Inflammation is a physiological response to different pathological, cellular or vascular damages due to physical, chemical or mechanical trauma. It is characterized by pain, redness, heat and swelling. Current natural drugs are carefully chosen as a novel therapeutic strategy for the management of inflammatory diseases. Different phytochemical constituents are present in natural products. These phytochemicals have high efficacy both in vivo and in vitro. Among them, flavonoids occur in many foods, vegetables and herbal medicines and are considered as the most active constituent, having the ability to attenuate inflammation. Kaempferol is a polyphenol that is richly found in fruits, vegetabl…

medicine.drug_classPhytochemicalsAnti-Inflammatory AgentsPharmaceutical ScienceBiological AvailabilityReviewChemical FractionationAnti-inflammatoryAnalytical Chemistrylcsh:QD241-441therapeutic utility03 medical and health scienceschemistry.chemical_compoundStructure-Activity Relationship0302 clinical medicinelcsh:Organic chemistryDrug DiscoveryToxicity TestsmedicineAnimalsHumansPhysical and Theoretical ChemistryKaempferols030304 developmental biologyTherapeutic strategyFlavonoids0303 health sciencesBiological ProductskaempferolPlants MedicinalTraditional medicineOrganic Chemistryfood and beveragesKaempferol Anti-Inflammatory TherapyBioavailabilityReview articlechemistryPhytochemicalChemistry (miscellaneous)Polyphenolinflammation030220 oncology & carcinogenesisDietary SupplementsMolecular MedicineKaempferol
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Increasing Yield and Antioxidative Performance of Litchi Pericarp Procyanidins in Baked Food by Ultrasound-Assisted Extraction Coupled with Enzymatic…

2018

Extraction with organic solvents is a traditional method to isolate bioactive compounds, which is energy-wasting and time-consuming. Therefore, enzyme and ultrasound treatments were combined to assist the extraction of oligomeric procyanidins from litchi pericarp (LPOPC), as an innovative approach to replace conventional extraction methods. Under optimum conditions (enzyme concentration 0.12 mg/mL, ultrasonic power 300 W, ultrasonic time 80 min, and liquid/solid ratio 10 mL/g), the yield of LPOPC could be improved up to 13.5%. HPLC analysis indicated that the oligomeric procyanidins (OPC) content of LPOPC from proposed extraction was up to 89.6%, mainly including (&minus

oligomeric procyanidinsPharmaceutical Sciencelitchi pericarpChemical FractionationHigh-performance liquid chromatographyPeroxideAntioxidantsArticleAnalytical Chemistrylcsh:QD241-441Lipid peroxidationchemistry.chemical_compound0404 agricultural biotechnologylcsh:Organic chemistryLitchiDrug DiscoveryRSM (Response Surface Methodology)Physical and Theoretical ChemistryChromatography High Pressure LiquidAnalysis of VarianceChromatographyMolecular StructurePlant ExtractsOrganic ChemistryExtraction (chemistry)04 agricultural and veterinary sciences040401 food sciencebaked foodMonomerProanthocyanidinchemistryUltrasonic WavesChemistry (miscellaneous)Yield (chemistry)Molecular MedicineHPLCProcyanidin A1Molecules
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