Search results for "Curing"
showing 10 items of 102 documents
Epoxy resin-thermoplastic blends cured by ionising radiation. Structure/properties relationships
2009
Radiation curing of an epoxy resin based blend is carried out in order to produce polymer matrices for high-performance composites. A suitable choice of both curing process and formulation parameters allows to irradiate at about 60°C. Moreover hydrothermal ageing is performed on cured materials and their properties have been evaluated
Novel method for functionalising and patterning textile composites:Liquid resin print
2016
Abstract The paper reports a novel method of integrating resin into continuous textile reinforcement. The method presents a print of liquid reactive resin into textile preforms. A series of targeted injections forms a patch which upon consolidation and curing transforms into a stiff region continuously spanning through preform thickness. Enhancing the injected resin with conductive phase allows creating a pattern of patches with controlled dimensions and added functionalities. Patterned composites reveal features which are not typical for conventional composites such as fibre bridged interfaces, regular thickness variation, and gradient matrix properties. The presented study explores the ro…
Radiation curing of diacrylate glycerolate of bisphenol-A in the presence of an organically modified montmorillonite for the production of flame-resi…
2006
Polymerization of an acrylate derivative of bisphenol-A by ionizing radiation in the presence of an organically modified montmorillonite was carried out in order to produce a flame-retardant composite. The measurement of the thermal effect during irradiation indicates that radiation curing of pure resin and resin-clay mixtures occurred in both cases. Moreover, differential scanning calorimetry and dynamic mechanical thermal analysis showed that a curing completion can be obtained by thermal curing after irradiation with a significant increase of the glass transition temperature. The morphology was investigated by X-ray diffraction and transmission electron microscopy. These have indicated t…
Sepiolite-reinforced epoxy nanocomposites: Thermal, mechanical, and morphological behavior
2010
A bisphenol A-based epoxy resin was modified with pristine sepiolite and an organically surface-modified sepiolite and thermally cured using two different curing agents: an aliphatic and a cycloaromatic diamine. The nanocomposites were characterized by dynamic mechanical analysis (DMA), rheology, thermogravimetric analysis (TGA), and electron microscopy. The initial sepiolite–epoxy mixtures show a better dispersion for the sepiolite-modified system that forms a percolation network structure. Mechanical properties have also been determined. The flexural modulus of the epoxy matrix slightly increases by the incorporation of the organophilic sepiolite. The flexural strength of the sepiolite-mo…
Minimal exposure time of different LED-curing devices
2007
Abstract Objectives The purpose of the study was to investigate the shortest possible exposure time of different LED-curing devices for five different resin composites in a clinically relevant in vitro-model, where a 7 mm distance from the light guide tip to the bottom side of the cavity was compiled. Methods Resin composite samples (Tetric EvoCeram A3, Filtek Supreme XT A3B, Premise A3, CeramX Mono M5, QuiXfil) were filled in three increments of 2 mm thickness each in stainless steel moulds (O = 5 mm, h = 6 mm, n = 9). The samples were incrementally exposed to different blue LED-curing devices (Bluephase, Bluephase C8, Bluephase 16i/Ivoclar Vivadent, L.E.Demetron II/sds Kerr, Elipar Free…
Application of non-invasive technologies in dry-cured ham: An overview
2019
Background: Dry-cured ham is one of the most valued food products by Mediterranean consumers. In this sense, the appropriate development of its different production stages is essential to ensure the quality requirements. For this reason, non-invasive technologies have gained popularity and have been reported as useful not only to ensure the food safety of different products, but also to monitor fundamental stages in the production process, such as the salting stage, to analyze the content of different compounds without sample losses, and to correct possible defects in the final product. Scope and approach: This work has been focused on summarizing the studies that describe and have successf…
Interlaminar fracture toughness behavior of electron-beam cured carbon-fiber reinforced epoxy-resin composites
2013
The work describes the preparation and physical-mechanical characterization of unidirectional CFRP panels manufactured by an electron beam curing technique. Delamination fracture toughness in Mode I and II is investigated in order to evaluate the influence of fiber–matrix adhesion strength, matrix toughness and matrix crosslinking density as determined by the radiation curing process. A matrix system comprising a DGEBA epoxy monomer and an initiator of cationic polymerization have been used, with one batch of resin mixed with a PES monomer in order to enhance matrix toughness. Curing was achieved with a pulsed 10 MeV Electron Beam accelerator. Thermally cured composite systems have also bee…
Antibacterial performance of solvent cast polycaprolactone (PCL) films containing essential oils
2013
Abstract The increase of consumer demand for higher quality and longer shelf-life in foods, while reducing the use of non-compostable packaging materials, has encouraged research on biopolymers incorporating natural antimicrobial compounds. Cinnamaldehyde (CNMA) and allyl isothiocyanate (AITC) were incorporated into polycaprolactone (PCL) films by solvent casting. The release study was carried out by means of ATR and transmission FTIR spectroscopy and showed high volatility of the essential oils during the film forming process. While only negligible quantities of AITC were retained in the polymer matrix after film curing, the release of CNMA was prolonged for at least 50 h at room temperatu…
Prediction of the curing time of Spanish hams using peptide profiles established by capillary zone electrophoresis
2009
Abstract A capillary zone electrophoresis procedure for the prediction of curing time of Spanish hams using peptide profiles has been developed. Excellent resolution between the seven peptide peaks was achieved within 30 min analysis time with a BGE containing 60 mM MgSO 4 and 50 mM phosphate at pH 2.5. Using hams with curing times of 6, 8 and 12 months, both linear discriminant analysis (LDA) and multiple linear regression (MLR) models were constructed. In both cases, two different normalisation procedures of the peak areas were compared. Using LDA, all the ham samples corresponding to the three categories were correctly classified. Using MLR, the ham curing time could be predicted with av…
Epoxy resins as a matrix material in advanced fiber-reinforced polymer (FRP) composites
2013
Abstract: This chapter discusses the epoxy resins which, thanks to their good and versatile properties, can be considered nowadays the most important class of thermosetting polymers. In particular the chapter first reviews both the epoxy resins commonly available on the market, including a new class of bio-derived epoxy resins, and the most-used curing agents. it then describes the principal characteristics of the epoxy resins and how it is possible to enhance them by adding several fillers to the epoxy system. Finally, the chapter analyzes the main engineering fields in which epoxy resins find application today and their possible future utilization.