Search results for "Cyclodecane"

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Über Phosphor‐haltige Heterocyclen I. Kristallstruktur von trans ‐1,6‐Diphenyl‐1λ 5 ,6λ 5 ‐diphosphacyclodecan‐1,6‐dion‐Dihydrat

1974

Die Struktur der Titelsubstanz (2) wurde rontgenographisch bestimmt und bis zu einem konventionellen R von 0.039 verfeinert. 2 ist zentrosymmetrisch. Der 10-Ring besitzt die bei Cyclodecan-Derivaten (3) ubliche Konformation niedrigster Spannungsenergie. 2 und 3 haben vergleichbare Pitzer- und Baeyer-Spannung, die transannularen Wechselwirkungen sind jedoch in 2 verringert. Die geminalen Phenyl- und Oxo-Substituenten stehen beide extra-annular (Phenyl trans-pseudoaxial, Oxo trans-pseudoaquatorial). Mittlerer CP-Abstand 1.804(3) A, PO-Abstand 1.502(3) A. Die Struktur besteht aus uber PO…HOH…OP-Wasserstoffbrucken verbundenen 2-Molekulen. On Heterocyclic Systems Containing Phosphorus, I. Crysta…

Inorganic Chemistrychemistry.chemical_compoundchemistryGeminalHydrogen bondStereochemistryMoleculeCrystal structureRing (chemistry)Medicinal chemistryCyclodecaneChemische Berichte

researchProduct

CCDC 260264: Experimental Crystal Structure Determination

2007

Related Article: J.Hovinen, R.Sillanpaa|2005|Tetrahedron Lett.|46|4387|doi:10.1016/j.tetlet.2005.04.078

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameters147-tris(2-Nitrophenylsulfonyl)-9-triphenylmethoxymethyl-147-triazacyclodecane chloroform solvateExperimental 3D Coordinates

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