Search results for "Diffractometer"
showing 4 items of 14 documents
Crystal Data for Metal Cimetidine Isotiocionates: M(CM)2(NCS)2 (M = Co(II), Ni(II), Cu(II))
1992
AbstractMetal cimetidine isothiocyanates, M(C10H16SN6)2(NCS)2, where M = Co(II), Ni(II) and Cu(II), have been investigated by means of X-ray powder diffraction. Unit cell dimensions were determined from powder diffractometer data. Refined cell parameters (monoclinic with a primitive cell), powder data, calculated densities and Z value are presented.
Crystal Data for Complexes of Co(II) and Ni(II) Perchlorates with Mepirizole
1992
AbstractMetal mepirizole perchlorates, M(C11H14N4O2)3 (C104)2 where M = Co(II) and Ni(II) have been investigated by means of X-ray powder diffraction. Unit cell dimensions were determined by indexing programs from diffractometer data. Refined cell parameters (monoclinic with a C-centered cell), calculated density and Z values are presented.
X-ray powder diffraction study of monoclinic V4+-ZrO2 solid solutions obtained from gels
2003
Abstract Rietveld refinement of six monoclinic V x Zr 1− x O 2 solid solutions, with x =0, 0.01, 0.02, 0.05, 0.075 and 0.1, prepared by heating dried gel precursors at 1300°C in air atmosphere, has been characterized using X-ray powder diffractometer data. The present results confirm that crystal structure of these solid solutions contain V 4+ (Zr 4+ ) cations surrounded by seven oxygens, four at a distance between 2.13 and 2.28 A (referred as to O(2) in the tetrahedrally coordinated oxygens) and other three at a distance between 2.03 and 2.20 A (denoted as O(1) in the triangularly coordinated oxygens). The trends in the lattice parameter variation of V x Zr 1− x O 2 solid solutions specime…
Preparation and x-ray pole-figure characterization of DC-sputtered Bi-2201, Bi-2212 and Bi-2223 thin films
1997
Thin films of the three members of the superconducting series , n = 1,2,3, were prepared by diode sputtering. X-ray characterization shows that all the films are single phase and c-axis oriented and in addition they are epitaxially grown. The latter is found by x-ray pole-figure measurements taken with a four-circle diffractometer. These are emphasized in this work. AC susceptibility measurements show that, while the 2201 films are not superconducting until 4 K, the transition temperatures of the 2212 films are 82 K - 90 K and of the 2223 films 84 K - 89 K.