Search results for "Direct method"
showing 10 items of 51 documents
Comparison of electron diffraction data from non-linear optically active organic DMABC crystals obtained at 100 and 300 kV
2000
During the recent past, we have synthesized a new class of molecules with intramolecular two-dimensional charge transfer upon excitation. The present report presents such a molecule, 2,6-bis(4-dimethylamino-benzylidene)-cyclohexanone (DMABC), with an unusually high value of the second-order non-linear optical (NLO) coefficients. In order to optimize the macroscopic NLO properties of the compounds, it is necessary to relate their first hyperpolarizability tensors at a molecular level to those at a crystal bulk level. This requires a complete structure determination and refinement. However, the growth of sufficiently large single crystals, which are needed for structural analysis and refineme…
The beta-delayed proton and gamma decay of 27P for nuclear astrophysics
2013
The creation site of 26Al is still under debate. It is thought to be produced in hydrogen burning and in explosive helium burning in novae and supernovae, and possibly also in the H-burning in outer shells of red giant stars. Also, the reactions for its creation or destruction are not completely known. When 26Al is created in novae, the reaction chain is: 24Mg(p, γ) 25Al(β +ν) 25Mg(p, γ) 26Al, but this chain can be by-passed by another chain, 25Al(p, γ) 26Si(p, γ) 27P and it can also be destroyed directly. The reaction 26mAl(p, γ) 27Si∗ is another avenue to bypass the production of 26Al and it is dominated by resonant capture. We find and study these resonances by an indirect method, throug…
Reference interval by the indirect approach of serum thyrotropin (TSH) in a Mediterranean adult population and the association with age and gender.
2019
Abstract Background The serum concentration of thyrotropin (TSH) represents a first-line test in diagnostic algorithms. The estimation of TSH reference intervals (RIs) is still a matter of debate due to the high prevalence of subclinical disease making difficult the definition of truly healthy subjects. The aim of this study was to estimate TSH RIs in healthy subjects and to evaluate the effect of age and gender on TSH concentration. Methods Forty-four thousand one hundred and fifty-six TSH data were collected between July 2012 and April 2018 at the Department of Laboratory Medicine, University-Hospital, Palermo. Common and sex-specific RIs were estimated by Arzideh’s indirect method after …
Direct method for calculating temperature-dependent transport properties
2015
We show how temperature-induced disorder can be combined in a direct way with first-principles scattering theory to study diffusive transport in real materials. Excellent (good) agreement with experiment is found for the resistivity of Cu, Pd, Pt (and Fe) when lattice (and spin) disorder are calculated from first principles. For Fe, the agreement with experiment is limited by how well the magnetization (of itinerant ferromagnets) can be calculated as a function of temperature. By introducing a simple Debye-like model of spin disorder parameterized to reproduce the experimental magnetization, the temperature dependence of the average resistivity, the anisotropic magnetoresistance and the spi…
Evaluation of a digital radiography to estimate working length
1997
The working lengths obtained with different methods in single-rooted teeth were compared. An endodontic rule in millimeters and calipers was used as a direct method of measurement (on endodontic files). As indirect methods, measurements were taken from conventional x-rays with calipers and with a digital radiological measurement system. No statistically significant differences were obtained between the direct and indirect methods. Three vertical angulations were taken for the indirect methods (0 degree, 15 degrees, and 30 degrees). No significant differences were found between results for the two indirect methods versus the standard method except for the 30 degrees angulation, which resulte…
La traducció en l'ensenyament de llengües : un recurs exclòs de les aules del mètode directe?
2022
Tradicionalment s'ha pensat que la traducció com a eina a l'aula de llengües estrangeres va quedar desaconsellada en el mètode directe. Així, des de llavors, molts docents han defensat la idea que la traducció és un recurs nociu per ensenyar idiomes, encara que, segons Cook (2010), no hi ha evidències que ho hagin provat científicament. Abans de continuar acceptant aquesta creença heretada del mètode directe, pensem que és necessari revaluar si la traducció va ser rebutjada per tots els seus exponents i si va ser realment possible excloure-la de les aules del moment. Per tant, l'objectiu d'aquest article és dur a terme una revisió teòrica sobre què va ser, quan i per què va sorgir el mètode…
Le manuel Corso di Lingua francese a base intuitiva de Romeo Lovera
2020
We analyze the three volumes of Romeo Lovera’s manual, Corso di Lingua francese a base intuitiva, which were intended for teaching French in secondary schools. The manual was first published in 1902 in Venice by Libreria editrice del Bollettino di Filologia Moderna, and there will be many reissues. Romeo Lovera is Italy's biggest supporter of methodological reform in the teaching of foreign languages ; it discloses, through the Bollettino di Filologia Moderna, new theories, scientific methods and their didactic applications. In their manuals, from the first lesson, through the direct and indirect intuition of the foreign language, the student learns to speak the French language by studying …
Exact extension of the DIRECT algorithm to multiple objectives
2019
The direct algorithm has been recognized as an efficient global optimization method which has few requirements of regularity and has proven to be globally convergent in general cases. direct has been an inspiration or has been used as a component for many multiobjective optimization algorithms. We propose an exact and as genuine as possible extension of the direct method for multiple objectives, providing a proof of global convergence (i.e., a guarantee that in an infinite time the algorithm becomes everywhere dense). We test the efficiency of the algorithm on a nonlinear and nonconvex vector function. peerReviewed
Comparison of Numerical Methods in the Contrast Imaging Problem in NMR
2013
International audience; In this article, the contrast imaging problem in nuclear magnetic resonance is modeled as a Mayer problem in optimal control. A first synthesis of locally optimal solutions is given in the single-input case using geometric methods based on Pontryagin's maximum principle. We then compare these results using direct methods and a moment-based approach, and make a first step towards global optimality. Finally, some preliminary results are given in the bi-input case.
Direct determination of Mancozeb by photoacoustic spectrometry
2006
Abstract A solvent free, fast and environmentally friendly photoacoustic-infrared-based methodology (PAS-FTIR) was developed for the determination of Mancozeb in agrochemicals. This methodology was based on the direct measurement of the transmittance spectra of solid samples and a multivariate calibration model to determine the active ingredient concentration. The proposed partial least squares (PLS) model was made using nine standards prepared by mixing different amounts of kaolin and Mancozeb, with concentrations between 5.43 and 88.10% (w/w). A hierarchical cluster analysis was made in order to classify the samples in terms of similarity in the PAS-FTIR spectra. From their spectra differ…