Search results for "EDX"
showing 10 items of 33 documents
New results in ancient Maya rituals researches: The study of human painted bones fragments from Calakmul archaeological site (Mexico)
2020
Abstract The funeral chambers of the ancient city of Calakmul (Mexico) and the individuals who were buried in them have brought in recent decades new knowledge about the beliefs and funeral customs of the pre-Hispanic Maya. Tombs and bodies were prepared as part of the rituals that should favor the return of ch'ulel to the Underworld, known as Xibalba by the ancient Maya. The ch'ulel is one of the two anemic entities that inhabit the individual, equivalent to our concept of the soul. Bodies preparation included coloured scented body ointments application, with a deep symbolic connotation and probably also a conservative purpose. The aim of this research was to characterize pigments and bind…
Obsidian in the Upper Palaeolithic of Iberia
2021
Submitted by André Pereira (andrepereira@letras.ulisboa.pt) on 2021-07-28T13:04:08Z No. of bitstreams: 1 obsidian-in-the-upper-palaeolithic-of-iberia.pdf: 35662679 bytes, checksum: 4c261781e3211c52c02d47cc36e26d98 (MD5) Approved for entry into archive by Manuel Botelheiro Moreno (manuelmoreno@campus.ul.pt) on 2021-07-28T16:31:42Z (GMT) No. of bitstreams: 1 obsidian-in-the-upper-palaeolithic-of-iberia.pdf: 35662679 bytes, checksum: 4c261781e3211c52c02d47cc36e26d98 (MD5) Made available in DSpace on 2021-07-28T16:32:40Z (GMT). No. of bitstreams: 1 obsidian-in-the-upper-palaeolithic-of-iberia.pdf: 35662679 bytes, checksum: 4c261781e3211c52c02d47cc36e26d98 (MD5) Previous issue date: 2021 info:eu…
Un disco-coraza de hierro de la Bastida de les Alcusses (moixent, valencia)
2017
Se presenta un disco-coraza de hierro procedente del oppidum ibérico de la Bastida de les Alcusses documentado con motivo de la revisión completa de los hallazgos de las excavaciones realizadas entre 1928 y 1931. La pieza es una lámina seudocircular en cuyo perímetro se distribuyen unos pequeños remaches para suspender el disco a las correas de sujeción, realizadas probablemente en cuero. Después de presentar el disco y los resultados de las analíticas EDXRF que permiten identificar los metales utilizados en la producción del disco (hierro) y los remaches (plata y cobre), se analiza su contexto de hallazgo, se encuadra históricamente esta categoría de armamento defensivo. Finalmente, se int…
Electrochemical Fingerprint of Archeological Lead Silicate Glasses Using the Voltammetry of Microparticles Approach
2016
9 págs.; 14 figs.; 1 tab.
Life after death: a physicochemical study of materials used by the ancient Maya in human bone ointments
2021
Ancient Maya believed in life after death. They used to prepare dead bodies during burial ceremonies whose purpose was to celebrate the dead and to help them passing through the way from earthly life to the beyond one. Bodies preparation included coloured scented body ointment application, with a deep symbolic connotation and probably also a conservative purpose. The aim of this research was to characterize pigments and binders used by ancient Maya in the preparation of body oint ments used to paint human bones. Emblematic painted bone samples from Xcambó (Maya archaeological site located in the municipality of Dzemul, in the Mexican state of Yucatán) were investigated through a non-destruc…
Nature-Inspired Effects of Naturally Occurring Trace Element-Doped Hydroxyapatite Combined with Surface Interactions of Mineral-Apatite Single Crysta…
2022
Innovative engineering design for biologically active hydroxyapatites requires enhancing both mechanical and physical properties, along with biocompatibility, by doping with appropriate chemical elements. Herein, the purpose of this investigation was to evaluate and elucidate the model of naturally occurring hydroxyapatite and the effects of doped trace elements on the function of normal human fibroblasts, representing the main cells of connective tissues. The substrates applied (geological apatites with hexagonal prismatic crystal habit originated from Slyudyanka, Lake Baikal, Russia (GAp) and from Imilchil, The Atlas Mountains, Morocco (YAp)) were prepared from mineral natural apatite wit…
Comparative Study of PM10 Concentrations and Their Elemental Composition Using Two Different Techniques during Winter–Spring Field Observation …
2022
The aims of this study were to determine the concentrations and elemental composition of PM10 in the village of Kotórz Mały (Poland), to analyse their seasonal variability, to determine the sources of pollutant emissions and to compare the consistency of the results obtained using different methods. Sampling and weather condition measurements were carried out in the winter (January–February) and spring (April) of 2019. Two combinations of different techniques were used to examine PM10 concentrations and their chemical composition: gravimetric method + atomic absorption spectrometry (GM+AAS) and continuous particle monitor + energy dispersive X-ray fluorescence (CPM+EDXRF).…
Portable non invasive analyses for Cultural Heritage
2014
The requirements that the scientific analyses for Cultural Heritage must have are: nondestructive and noninvasive, multielemental, sensitive, reliable and sufficiently rapid, able to carry out measurements in situ on objects of all types, and to deduce information practically on-line. Among the techniques that fulfill these requirements we find: multispectral imaging, portable EDXRF, Raman and UV-VIS-NIR spectrometry. In this paper we are going to show some cases in which it will appear clear the necessity of the correct order with which applying the non invasive techniques and what data of each of them it is necessary to understand in situ to obtain the maximum of the subsequent scientific…
Microchemical surface analysis of historic copper-based coins by the combined use of FIB-FESEM-EDX, OM, FTIR spectroscopy and solid-state electrochem…
2019
[EN] A multi-technique strategy, including microscopy, spectroscopic and electrochemical techniques, is proposed to study thin corrosion layers that form on the surface of historic copper-based coins. An accurate characterisation of this external corrosion layer is important for selecting a suitable conservation and/or restoration treatment. For this purpose, a series of copper-based coins from different historical periods and provenances, which mainly exhibited atmospheric corrosion, was analysed. The morphology of the corrosion layer and the upper core of coins was studied in trenches done on coin surfaces with a focused ion beam gun, coupled to a field emission scanning electron microsco…
Low-Q peak in X-ray patterns of choline-phenylalanine and homophenylalanine: a combined effect of chain and stacking
2016
Abstract In this contribution we report for the first time the X-ray patterns of choline-phenylalanine and choline-homophenylalanine ionic liquids. The presence of a low Q peak in both systems is another evidence that a long alkyl chain is not always needed to establish a nanodomain segregation in the liquid sufficient to be revealed by the diffraction experiment. These new data are compared with the diffraction patterns and the theoretical calculations of other choline-aminoacid ionic liquids recently reported. A significant role might be played by the stacking interactions between aromatic rings.