Search results for "Extraction"

Synthesis of a technetium-99m labelledL-tyrosine derivative with thefac-99mTc(I)(CO)3-core using a simple kit-procedure

2004

Summary The synthesis of a novel technetium-99m labelled derivative of l-tyrosine as a potential tumour imaging agent for nuclear medicine diagnosis is reported. The synthesis involved the labelling precursor fac-[ 99m Tc(OH2)(CO)3] + which was synthesized using the commercially available Isolink 1 -labelling kit and the tyrosine derivative O-(N,Nbis(carboxymethyl)aminoethyl)-l-tyrosine trifluoroacetate. The labelled compound O( 99m Tc(I)-tricarbonyl-N,N-bis(carboxymethyl)aminoethyl)-l-tyrosine was obtained in a radiochemical yield of 70–80% within 60 min with a radiochemical purity greater than 98% without any HPLC purification step. Purification was achieved merely by solid phase extracti…

A density functional theory study of uranium(VI) nitrate monoamide complexes.

2011

Density functional theory calculations were performed on uranyl complexed with nitrate and monoamide ligands (L) [UO(2)(NO(3))(2)·2L]. The obtained results show that the complex stability is mainly governed by two factors: (i) the maximization of the polarizability of the coordinating ligand and (ii) the minimization of the steric hindrance effects. Furthermore, the electrostatic interaction between ligands and uranium(vi) was found to be a crucial parameter for the complex stability. These results pave the way to the definition of (quantitative) property/structure relationships for the in silico screening of monoamide ligands with improved extraction efficiency of uranium(vi) in nitrate ac…

Selective Extraction of Biocompounds from Stevia rebaudiana Bertoni Leaves Using Electrotechnologies

2016

Current and New Insights in the Sustainable and Green Recovery of Nutritionally Valuable Compounds from Stevia rebaudiana Bertoni.

2015

International audience; The South American plant Stevia rebaudiana Bertoni is a great source of noncaloric sweeteners (steviol glycosides), mainly concentrated in its leaves, but also has important antioxidant compounds (vitamin C, polyphenols, chlorophylls, and carotenoids) and other important macro- and micronutrients such as folic acid and all of the essential amino acids except tryptophan. Traditionally, conventional methods have been used to recover nutritionally valuable compounds from plant food matrices. However, nowadays, the need for obtaining greener, sustainable, and viable processes has led both food industries and food scientists to develop new processes in full correspondence…

Motor learning and body size within an insect brain computational model

2014

Nowadays modeling insect brains is also an important source of inspiration to develop learning architectures and control algorithms for applications on autonomous walking robots. Within the insect brain two important neuropiles received a lot of attention: the mushroom bodies (MBs) and the central complex (CX). Recent research activities considered the MBs as a unique architecture where different behavioural functions can be found. MBs are well known in bees and flies for their role in performing associative learning and memory in odor conditioning experiments [4]. They are also involved in the processing of multiple sensory modalities including visual tasks [3], different forms of learning…

Presence and characterisation of verotoxin producing E. coli in fresh Italian pork sausages, and preparation and use of an antibiotic-resistant strai…

2005

One hundred and twenty six samples of fresh pork sausages were analysed-for the presence of verocytotoxigenic Escherichia coli (VTEC). Selective enrichment followed by DNA extraction and PCR amplification of the stx1 and stx2 genes highlighted the occurrence of the above mentioned genes in 20 out of 126 samples screened. From the stx positive enriched cultures, isolation was performed on CT-SMAC agar plates after immuno-magnetic separation of E. coli O157. Fifty three non-sorbitol fermenting isolates were obtained and further characterised, along with the reference strain E. coli ATCC 35150(T). All the isolates were characterised by PCR assays, assessing the presence of stx1, stx2, rfbE(O15…

Purification of recovered phosphoric acid by extracting aluminium with di-2-ethylhexyl phosphoric acid

2021

AbstractThe extraction of aluminium from dilute phosphoric acid with di-2-ethylhexyl phosphoric acid (DEHPA) was optimized using response surface methodology. The optimization was based on the experimental three-level central composite face-centred design (CCF) and was conducted on real-life samples. The three variables included were pH, extractant concentration and aqueous to organic phase ratio (AO). Under the optimized conditions (pH 2.5, 0.6 M DEHPA and AO ratio 1:2), extraction efficiency of 99% for aluminium in four extraction stages is achieved. The purified phosphoric acid solution can then be utilized by the fertilizing industry. Stripping tests for organic phase loaded with alumin…

Knowledge Extraction from Healthcare Data Using User-Adaptable Keywords-Based Query Language

2020

Nowadays, the volume of the information gathered by any organization increases more and more rapidly. It is essential to be able to use this information efficiently for it to benefit the operation of the organization. There is no point of gathering the information if it is not converted into knowledge. The knowledge extraction process becomes the backbone of any successful organization. Moreover, the extraction of the knowledge must be quick and efficient, so that the newly-obtained knowledge can be put in use at once. The problem addressed in this paper is how to allow the domain expert to extract the knowledge from their information systems themselves without involving the third party in …

Visualization in comparative music research

2007

Computational analysis of large musical corpora provides an approach that overcomes some of the limitations of manual analysis related to small sample sizes and subjectivity. The present paper aims to provide an overview of the computational approach to music research. It discusses the issues of music representation, musical feature extraction, digital music collections, and data mining techniques. Moreover, it provides examples of visualization of large musical collections.

Experimental analysis of the water retention behaviour of shales

2014

Shales are among the most commonly considered geomaterials in current energy-related geomechanical investigations, as they are involved in engineering applications such as the unconventional extraction of natural gas, CO2 sequestration and nuclear waste geological storage. A deep understanding of their behaviour with regard to variations in the degree of saturation is of primary significance for such applications. With the aim to establish a sound protocol for shale retention behaviour analysis, this paper presents an advanced experimental methodology that takes into account the specificities of shales such as small pore size dimensions and the large variations in water potential to be appl…