Search results for "Extraction"
showing 10 items of 2072 documents
A preliminary study on the distribution of morphine and its glucuronides in the subcompartments of blood.
1998
[Abstract ] The distribution of morphine, morphine-3-glucuronide (M3G), and morphine-6-glucuronide (M6G) in whole blood, plasma, and packed erythrocytes was studied. Parameters investigated were the hematocrit values (10, 42, 44, and 71%) and the water content of the samples. The blood-to-plasma ratio of morphine concentrations was unaffected by variations in hematocrit and water content, whereas the corresponding ratios for M3G and M6G were strongly influenced. Ratios were 0.53 to 0.65 and 0.52 to 0.62 in specimens with average hematocrit values (42 and 44%, respectively), and the ratios were 0.81 or 0.89 (hematocrit 10%) and 0.27 or 0.28 (hemalocrit 71%) in blood samples with different he…
Can Signaling Theory Help Agency and Resource Scarcity Theories Explain Franchisee Failure? Predicting SBA-Backed Loan Defaults
2010
This study examines the use of analytic techniques to develop a model that predicts the potential default of Small Business Administration (SBA) backed loans issued to American franchisees. Data collected by World Franchising (WF) in their 2008 survey and by SBA from 2000-2008, covering 271 diverse US franchise chains, on the reported failure rates and charge off percentages of SBA backed loans was used to explore associations between franchisor characteristics and franchisee loan performances. The predictive capability of the derived model was assessed using a data mining technique in which the original data set is split into two different subsets: one for estimation and one for validation…
Hunting for valuables from landfills and assessing their market opportunities A case study with Kudjape landfill in Estonia
2017
Landfill mining is an alternative technology that merges the ideas of material recycling and sustainable waste management. This paper reports a case study to estimate the value of landfilled materials and their respective market opportunities, based on a full-scale landfill mining project in Estonia. During the project, a dump site (Kudjape, Estonia) was excavated with the main objectives of extracting soil-like final cover material with the function of methane degradation. In total, about 57,777 m3 of waste was processed, particularly the uppermost 10-year layer of waste. Manual sorting was performed in four test pits to determine the detailed composition of wastes. 11,610 kg of waste was…
Optimization of microwave-assisted extraction of polyphenols from Quercus bark
2015
Abstract Box–Behnken response surface methodology was used to investigate and optimize microwave assisted extraction (MAE) (treatment power and time) of antioxidant compounds, especially polyphenols, from bark extracts. Moreover, the effects of solvent composition (methanol and ethanol) particle size, and pH conditions were evaluated and optimized. In addition, the effects of MAE were compared to conventional solvent extraction at room temperature and reflux extraction (at 100 °C). The results indicated that all process variables had a significant effect on polyphenol and antioxidant recovery, except for methanol (p > 0.05). For instance, TPC and antioxidant activity were increased when hig…
Preparation and characterization of dummy-template molecularly imprinted polymers as potential sorbents for the recognition of selected polybrominate…
2018
The main aim of this work was to conduct the preliminary/basic research concerning the preparation process of a new dummy molecularly imprinted polymer (DMIP) materials. Developed DMIPs were proposed as a sorption material in solid-phase extraction (SPE) technique for recognition of selected low mass polybrominated diphenyl ethers (PBDEs) – PBDE-47 and PBDE-99. Four new DMIPs were synthesized employing bulky polymerization technique by application of structural analogue of low mass PBDEs - 4,4′-Dihydroxydiphenyl ether, as a dummy template. The DMIPs and corresponding non-imprinted polymers were prepared using different functional monomers: methacrylic acid; methyl methacrylate and different…
Data Mining Algorithms for Knowledge Extraction
2020
In this paper, we study the methods, techniques, and algorithms used in data mining, and from the studied algorithms, we emphasized the clustering algorithms, more precisely on the K-means algorithm. This algorithm was first studied using the Euclidean distance, then modifying the distance between the clusters using the distances Mahalanobis and Canberra. After implementing the algorithms in C/C++, we compared the clustering of the three algorithms, after which we modified them and studied the distance between the clusters.
Recombinant, activated factor VII for surgery in factor VII deficiency: a prospective evaluation - the surgical STER
2010
Excessive bleeding represents a major complication of surgical interventions and its control is especially relevant in patients with Congenital Bleeding Disorders (CBD). In factor VII (FVII) deficiency, scanty data on surgery is available to guide treatment strategies. The STER (Seven Treatment Evaluation Registry) is a multi-centre, prospective, observational, web-based study protocol providing the frame for a structured and detailed data collection. Inhibitor occurrence was checked in a centralized fashion. Forty-one surgical operations (24 'major' and 17 'minor') were performed in 34 subjects with a carefully characterized FVII deficiency under the coverage of recombinant activated Facto…
An integrated strategy between food chemistry, biology, nutrition, pharmacology, and statistics in the development of functional foods: A proposal
2017
Abstract Background Much research has been conducted to attest that different food and herbal extracts display functional properties in humans when consumed regularly as part of a balanced diet. However, most studies only relate one or some in vitro and/or in vivo functionalities of these extracts, without performing clinical trials to attest the alleged functionality. For instance, while some studies focus on the existence of statistical correlation between antioxidant activity and antidiabetic properties and the phenolic composition of a certain herb, others aim to assess the effects of different extraction methods ( i.e., pulsed electric fields, ultrasound, and supercritical fluid extrac…
Studies of polyamines transport through liquid membranes with D2EHPA as a carrier.
2008
The transport of polyamines through the liquid membranes with di‐2‐ethylhexyl phosphoric acid (D2EHPA) was investigated. The study was performed in three main steps: liquid–liquid extraction (LLE), bulk liquid membrane (BLM) extraction, and supported liquid membrane (SLM) extraction. Equilibrium distribution experiments allowed determining the extraction constants and stoichiometric coefficients for each polyamine. It turned out that one amino group binds two molecules of carrier (one D2EHPA dimer) and the extractability of polyamine rises with the increase in number of function groups in the molecule. The BLM and SLM experiments showed that despite considerable differences in distribution …
Biomethylation of thallium by bacteria and first determination of biogenic dimethylthallium in the ocean
2000
To investigate a possible biomethylation of thallium, incubation experiments were carried out under aerobic conditions with a sewage sludge and with a mixed bacterial culture isolated from a sewage sludge, as well as under anaerobic conditions with a fresh-water lake sediment, by adding Tl(I) nitrate to these systems. Only in the case of the anaerobic sediment was a significant production of dimethylthallium observed (after three-weeks). Analysing different surface seawater samples and those from a single depth profile down to 4000 m, dimethylthallium was determined above the detection limit of 0.4 ng L−1 in about 20% of all samples, ranging from 0.5 to 3.2 ng l−1. The proportion of dimethy…