Search results for "Heptachlor"
showing 5 items of 5 documents
Gas chromatographic determination of organochlorine pesticides in cow milk.
2004
A gas chromatographic method of use in determining the following organochlorine pesticides in cow milk has been adapted and validated: alpha-hexachlorocyclohexane (alpha-HCH), beta-HCH, lindane, delta-HCH, hexachlorobenzene, aldrin, heptachlor, heptachlor epoxide, mirex, 2,4-dichlorodiphenyltrichloroethane (2,4-DDT), 4,4-DDT, 2,4-dichlorodiphenyldichloroethane (2,4-DDD), 4,4-DDD, 2,4-dichlorodiphenylethane (2,4-DDE) and 4,4-DDE. The method studied consists of three steps: the extraction of fat by centrifugation, mixing with anhydrous sodium sulfate, and transfer to a glass column and elution with hexane; purification of the extract via concentrated sulfuric acid treatment; and determination…
Organochlorinated pesticides in sediments from the Lake Albufera of Valencia (Spain).
2005
Bottom sediment samples from 121 sites of the Lake Albufera of Valencia were analyzed. Dieldrin, endrin, heptachlor and op'-DDT were not detected (0.01 ng g(-1)) in 88-93% of the sites. Aldrin and HCB concentration ranges were between0.01 and 0.1 ng g(-1) in 86% and 94% of the sites, respectively. Heptachlor-epoxide and lindane 95% confidence intervals were 0.2-0.5 and 0.06-0.12, respectively. The greatest average concentration corresponds to pp'-DDE, pp'-DDD and pp'-DDT. The sum of six isomers and derivatives of the DDT average concentration reaches 2.1 ng g(-1), as opposed to 2.7 ng g(-1) for the sum of 13 pesticides considered. In the site with a major contamination, 27.0 ng g(-1) of pp'…
Levels and Potential Health Hazards of Chlorinated Pesticidesin Surface Water Samples of Charsadda Area of Pakistan Using SPME-GC-ECD Technique
2021
In the present study, we determined the levels of chlorinated pesticide residues in surface water samples collected from the Charsadda district (KPK, Pakistan). SPME-GC-ECD with COMBI PAL CTC autosampler was used for extraction and analysis of 20 organochlorine pesticides in the collected water samples. For maximum efficiency of the SPME procedure, several parameters were studied, including the extraction and desorption time of the fiber, solution pH, agitation of samples, and stirring speed, etc. This method showed good liner response, with R2 values in the range of 0.9887 to 0.9999 for all pesticides. This method also provided good percent recoveries at 1 µg L−1 (87.5 to 106.0%) and at 2 …
CCDC 743660: Experimental Crystal Structure Determination
2010
Related Article: B.Therrien, Trieu-Tien Thai, J.Freudenreich, G.Suss-Fink, S.S.Shapovalov, A.A.Pasynskii, L.Plasseraud|2010|J.Organomet.Chem.|695|409|doi:10.1016/j.jorganchem.2009.10.033
CCDC 743659: Experimental Crystal Structure Determination
2010
Related Article: B.Therrien, Trieu-Tien Thai, J.Freudenreich, G.Suss-Fink, S.S.Shapovalov, A.A.Pasynskii, L.Plasseraud|2010|J.Organomet.Chem.|695|409|doi:10.1016/j.jorganchem.2009.10.033