Search results for "INVESTIGATION"

Photocatalytic oxidation of acetonitrile in gas–solid and liquid–solid regimes

2005

Il programma NON mi ha consentito di scaricare il PDF di questo articolo. Se lo volete ditemi come inviarlo ABSTRACT Photocatalytic degradation of acetonitrile was carried out in both gas–solid and liquid–solid regimes using two commercial TiO2 catalysts (Merck and Degussa P25). For the gas–solid regime, a continuous annular photoreactor was used. The influence on photodegradation kinetics of the gas flow rate and concentrations of acetonitrile, oxygen, and water was investigated. Acetonitrile degradation products detected in the gas phase included carbon dioxide and hydrogen cyanide. The same photoactivity was exhibited in the presence and in the absence of water vapour. The liquid–solid reg…

Analiza informacji: między kryminalistyką i prawem

2022

Analiza informacji jest pojęciem pojawiającym się szeroko we współ-czesnych realiach społecznych, gospodarczych, ekonomicznych czy prawnych. Nie omija ona również nauk prawnych czy nauk policyjnych, dając nowe możliwości rozwiązywania problemów kryminalnych, niejednokrotnie dostarczając również ciekawych i innowacyjnych narzędzi. Analiza informacji jako procedura myślowa, polegająca na działaniu zmierzającym do wskazania i zrozumienia związków między ludźmi, miejscami i zdarzeniami jest najistotniejszym, ale zarazem niewystarcza-jąco zbadanym obszarem współczesnej kryminalistyki. Celem tego arty-kułu jest przedstawienie Czytelnikowi istoty analizy informacji, określenie jej głównych cech, a…

Strengthening of Masonry Columns with BFRCM or with Steel Wires: An Experimental Study

2016

Nowadays, innovative materials are more frequently adopted for strengthening historical constructions and masonry structures. The target of these techniques is to improve the structural efficiency with retrofitting methods while having a reduced aesthetical impact. In particular, the use of basalt fiber together with a cementitious matrix emerges as a new technique. This kind of fiber is obtained by basalt rock without other components, and consequently it could be considered a natural material, compatible with masonry. Another innovative technique for strengthening masonry columns consists of applying steel wires in the correspondence of mortar joints. Both techniques have been recently pr…

Responsabilidad social universitaria: acción aplicada de valoración del bienestar psicológico en personas adultas mayores institucionalizadas

2012

La sociedad atraviesa una serie de transformaciones en sus relaciones entre instituciones y comunidad; en este marco la universidad, desde su misión académica centrada en la formación e investigación para el desarrollo de conocimientos, está promoviendo una mayor implicación hacia las necesidades de la sociedad, a lo que se denomina responsabilidad social universitaria (RSU). Este artículo presenta cómo, desde una perspectiva humanista, se constituye una comunidad social de investigación entre la Unidad de Investigación Enfoque Centrado en la Persona de la Universidad de Valencia –España-, el grupo Prisma de la Universidad Autónoma de Bucaramanga –Colombia- y la Fundación Albeiro Vargas (FA…

X-ray Computed Tomography for Capillary Collapse of Loose Unsaturated Sand

2016

Abstract The collapse of unsaturated soils consists of the reduction in volume upon wetting at constant total stress. Several studies at the macro scale outline the influence of initial void ratio, confining pressure and matric suction on the onset of collapse of standard laboratory specimens. Conversely, few observations at the micro scale are available in the literature, although the influence of the particles arrangement and intergranular bonding has been formerly supposed. The collapse of fine sand derived by a pyroclastic soil of Southern Italy is investigated in this paper at the microscale using the X-ray Computed Tomography. The experimental procedure, formerly tested on similar pyr…

NMR Study of the (Z)-Phenylhydrazones of 5-Alkyl- and 5-Aryl-3-benzoyl-1,2,4-oxadiazoles: Support for the Interpretation of Kinetic Results on the Re…

2005

An analysis of the 1H, 13C, and 15N NMR substituent chemical shifts (SCSs) of the title compounds in CDCl3 solution has been carried out by using the SCSs of other classes of compounds (arenes, methyl esters or amides), Hammett substituent constants or kinetic data. The results obtained provide information concerning the ground-state electronic distribution of the compounds examined. The results relevant to the carbon and nitrogen atoms of the 1,2,4-oxadiazole ring can be considered of special interest, as the effects of the substit- Introduction For several years our research group has been involved in the use of NMR spectroscopic data (1H, 13C, 15N, and 17O) to obtain information about th…

Determination of Plasma Lipid Hydroperoxides by an NADPH/NADP + Coupled Enzyme Reaction System. Evaluation of a Method

1998

Summary: Several techniques based on different principles have been proposed to measure lipid hydroperoxides. Enzymatic methods are sensitive and can be quite specific but they are subject to interference by inhibitors and not all are stoichiometric. The present work proposes some modifications of the Heath & Tappel (Anal Biochem 1976; 7:184—91) enzymatic method of determination of lipid hydroperoxides in order to standardize and automate it and to meet the analytical criteria required for a biological assay. The proposed new protocol and the automated assay give acceptable within-run and between-run precisions, with coefficients of variation of 3.34% and 5.80%, respectively, at the usual p…

Artifacts in Light Scattering Experiments Using Opaque Scattering Screens on the Example of Spinodal Decomposition

1996

π-Conjugated diimidazolium salts: rigid structure to obtain organized materials.

2015

Phenylene ethynylene based diimidazolium salts differing in the alkyl chain length borne on the imidazolium ion and anion nature were synthesized. Their properties were studied both in solution and in the solid state. Salts obtained were able to aggregate in organic solvent solution. Aggregate formation was studied by performing concentration dependent measurements using UV-vis, fluorescence and Resonance Light Scattering. Furthermore, features of the aggregates were also investigated in the solid state by means of fluorescence and Scanning Electron Microscopy measurements. Finally, Density Functional Theory calculations were performed to obtain insights into the interaction geometry in the…

Microscopic and nanoscopic EVA composite investigation: Electrical properties and effect of purification treatment

2004

This work presents preliminary results of an investigation aiming at characterization of nanocomposite insulating materials. Focus is made on size and technological process effects, i.e. dependence of electrical properties on filler size, on polymer-nanofiller interaction (e.g. intercalation or exfoliation) and, in particular, on chemical purification procedures. The materials under investigation are (EVA) copolymer filled by layered micro and nanosized silicates consisting of montmorillonite and fluorohectorite, that is, natural and synthetic clays. Microstructural characterization, using transmission electron microscopy, TEM, and wide-angle X-ray spectroscopy, WAXS, and electrical measure…