Search results for "Indentation"

KNOWN RESIDUAL STRESS SPECIMENS USING OPPOSED INDENTATION

2009

In order to test new theories for residual stress measurement or to test the effects of residual stress on fatigue, fracture, and stress corrosion cracking, a known stress test specimen was designed and then fabricated, modeled, and experimentally validated. To provide a unique biaxial stress state, a 60 mm diameter 10 mm thick disk of 316L stainless steel was plastically compressed through the thickness with an opposing 15 mm diameter hard steel indenters in the center of the disk. For validation, the stresses in the specimen were first mapped using time-of-flight neutron diffraction and Rietveld full pattern analysis. Next, the hoop stresses were mapped on a cross section of two disks usi…

Graphene coating obtained in a cold-wall CVD process on the Co-Cr Alloy (L-605) for medical applications

2021

Graphene coating on the cobalt-chromium alloy was optimized and successfully carried out by a cold-wall chemical vapor deposition (CW-CVD) method. A uniform layer of graphene for a large area of the Co-Cr alloy (discs of 10 mm diameter) was confirmed by Raman mapping coated area and analyzing specific G and 2D bands

Micro and macro mechanical characterization of friction stir welded Ti–6Al–4V lap joints through experiments and numerical simulation

2013

Abstract Lap joints of Ti–6Al–4V were produced and the effect of the main process parameters was studied through macro and micro investigations highlighting mechanical resistance, microhardness profiles, grain size and phase distributions. A dedicated numerical model was used to link the input process parameters to temperature and strain distributions and to the final microstructure in the welded joint. It is found that the strain produced in the stir zone by proper combination of process parameters plays a fundamental role in the final microstructure and mechanical properties of the joints.

Experimental and Numerical Analysis of Microstructure Evolution during Linear Friction Welding of Ti6Al4V

2015

Abstract Linear Friction Welding (LFW) is a solid state welding process used to joint bulk components. In the paper, an experimental and numerical study on LFW of Ti6Al4V titanium alloy is presented. A laboratory designed LFW machine has been used to weld the specimens with different contact pressure and oscillation frequency. The joint microstructure has been experimentally observed with SEM and EDS. A dedicated numerical model, able to predict temperature, strain and strain rate distribution as well as the phase volume fraction evolution, has been utilized to predict the final microstructure in the welded parts. It was found that complete transformation of the alpha phase into beta phase …

Friction Stir Processing: thermo-mechanical loads and consequent effects on the local material characteristics

2008

The present article is focused on the correlation between the applied thermal and mechanical loads and the consequent effects on the material in friction stir processing (FSP) operations. On one hand, the actions exerted in FSP are split compared to the results obtained with a tool without the pin at its end to a traditional one with a cylindrical pin. In this way, the thermal flux determined by the frictional forces at the tool—shoulder—workpiece interface is secluded from the mechanical stirring action made by the tool pin. On the other hand, the processed specimens are analysed in terms of residual stress state, microhardness, and average grain size values. An in-process heat treatment …

Characterization of Fusion Lines Obtained with Laser Welding on Ductile Iron Plates

2016

This paper studies the ductile iron (DI) weldability using laser welding. For performing an Yb:YAG continuous laser was used, with a maximum power of 6 kW. The parametrical window power (P) - welding speed (S) was explored by carrying out the fusion lines on ductile iron plates without preheating, to determinate areas of weldability (complete penetration, correct geometry) to allow further characterization. The criteria for selection of focus areas were the geometry of the fusion lines and the absence of the welding defects. The unsatisfactory domains were characterized by: collapse of the melted metal, incomplete penetration, low fusion lines quality (geometry, compactness). In present stu…

2019

Atomic force microscopy (AFM) is today an established tool in imaging and determination of mechanical properties of biomaterials. Due to their complex organization, those materials show intricate properties such as viscoelasticity. Therefore, one has to consider that the loading rate at which the sample is probed will lead to different mechanical response (properties). In this work, we studied the dependence of the mechanical properties of endothelial cells on the loading rate using AFM in force spectroscopy mode. We employed a sharp, four-sided pyramidal indenter and loading rates ranging from 0.5 to 20 μm/s. In addition, by variation of the load (applied forces from 100 to 10,000 pN), the…

Obtaining of nanostructured ZnO coatings using mechanoactivated oxidation

2007

The concept to use nanostructured state of metal at the instant of destruction in air environment was used to obtain nanostructured Zn-ZnO coatings on glass and quartz by mechanical method. Subsequent annealing in the ambient atmosphere, annealing in vacuum and irradiation with 532-nm YAG:Nd laser were used to obtain completely oxidized, transparent ZnO coatings. The saturated with oxygen nanostructured coatings were transformed into nanostructured ZnO coatings after annealing above 773K or irradiation with laser (allowing to reach 673K) in ambient atmosphere. AFM and SEM images show that after annealing ZnO coatings have multi-shaped structure. The formation of ZnO need-like whiskers (d = …

Microhardness of demineralized enamel following home bleaching and laser-assisted in office bleaching

2015

Background There is little data regarding the effect of tooth whitening on microhardness of white spot lesions. This study was conducted to investigate the effect of home-bleaching and laser-assisted in-office bleaching on microhardness of demineralized enamel. Material and Methods Forty bovine incisors were selected and immersed in a demineralizing solution for 12 weeks to induce white spot lesions. Enamel blocks were prepared and randomly assigned to two groups of 20 each. The first group underwent home bleaching with 15% carbamide peroxide which was applied for 8 hours a day over a period of 15 days. In the second group, in-office bleaching was performed by 40% hydrogen peroxide and powe…

Mechanical Characterization of Polymers on a Nanometer Scale through Nanoindentation. A Study on Pile-up and Viscoelasticity

2007

The analysis of nanoindentation force curves collected on polymers through the common Oliver and Pharr procedure does not lead to a correct evaluation of Young’s modulus. In particular, the estimated elastic modulus is several times larger than the correct one, thus compromising the possibility of a nanomechanical characterization of polymers. Pile-up or viscoelasticity is usually blamed for this failure, and a deep analysis of their influences is attempted in this work. Piling-up can be minimized by indenting on a true nanometer scale, i.e., at penetration depth smaller than 200 nm. On the other side, it is common knowledge that fast indentations minimize the effect of viscoelasticity. How…