Search results for "Laboratory scale"

showing 8 items of 18 documents

Extraction of Phenolic Compounds from Fresh Apple Pomace by Different Non-Conventional Techniques

2021

Red Delicious apple pomace was produced at laboratory scale with a domestic blender and different non-conventional extraction techniques were performed to isolate phenolic compounds, such as ultrasound-assisted extraction (UAE), ultraturrax extraction (UTE), accelerated solvent extraction (ASE) and pulsed electric field (PEF) extraction pre-treatment. Total phenolic content (TPC) was determined by Folin–Ciocalteu assay. Phloridzin, the main phenolic compound in apples, was determined by chromatographic analysis Q-TOF-LC/MS. The results obtained with these techniques were compared in order to identify the most efficient method to recover polyphenols. The highest value of TPC (1062.92 ± 59.80…

Pharmaceutical SciencephloridzinLaboratory scale01 natural sciencesArticleAntioxidantsMass SpectrometryASEQ-TOF-LC/MSAnalytical ChemistryQD241-4410404 agricultural biotechnologyNutraceuticalPhenolsFunctional foodDrug DiscoveryFood sciencenon-conventional extractionsPhysical and Theoretical ChemistryChromatography High Pressure LiquidpolyphenolsFlavonoidsEthanolPlant ExtractsChemistry010401 analytical chemistryOrganic ChemistryExtraction (chemistry)Pomace04 agricultural and veterinary sciencesPEF040401 food science0104 chemical sciencesAccelerated solvent extractionUAEChemistry (miscellaneous)PolyphenolMalusapple pomaceMolecular MedicineUTEMolecules
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Water-insoluble β-cyclodextrin–epichlorohydrin polymers for removal of pollutants from aqueous solutions by sorption processes using batch studies: A…

2017

This review is dedicated to Giangiacomo Torri (Istituto di Chimica e Biochimica G. Ronzoni, Milan, Italy) in celebration of his retirement.; International audience; Although water-insoluble cyclodextrin-epichlorohydrin polymers have been known for half a century, these materials are of continued interest to the scientific community, in particular for their interesting environmental applications as sorbents in liquid-solid sorption processes. However, in spite of the abundance of literature and conclusive results obtained at the laboratory scale, interpreting the mechanisms of pollutant elimination remains an interesting source of debate and sometimes of contradiction. This review summarizes…

PollutantsPolymers and Plastics02 engineering and technologyWater insolubleLaboratory scale010402 general chemistry01 natural scienceschemistry.chemical_compoundMechanismsMaterials ChemistryCyclodextrinOrganic chemistryEpichlorohydrinPolymerComputingMilieux_MISCELLANEOUSPollutantchemistry.chemical_classificationAqueous solutionCyclodextrinOrganic ChemistrySorptionSurfaces and InterfacesPolymer021001 nanoscience & nanotechnology0104 chemical sciences[ CHIM.POLY ] Chemical Sciences/Polymers[CHIM.POLY]Chemical Sciences/PolymerschemistryChemical engineeringCeramics and CompositesEpichlorohydrin0210 nano-technologyCross-linking
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Can crumb rubber modifier effectively replace the use of polymer- modified bitumen in asphalt mixture?

2021

Laboratory scale mechanical performances on six plant produced mixtures; three semi-dense surface courses and three dense binder courses modified with engineered crumb rubber (ECR) using the dry process are presented. The two types of mixtures produced and investigated fulfilled for the most part, the requirements of the Swiss and/or US standards regarding volumetric properties, water sensitivity and rutting. In advanced testing where no requirements exist, the dense ECR mixtures performed similar to the reference polymer modified mixtures and slightly worse for semi-dense mixtures in high temperature tests, where the binder becomes viscous in the rubber-binder composite and its ability to …

Polymer modifiedMaterials scienceCrumb rubber modified asphalt dry process performance plant productionAsphaltPlant productionGeography Planning and DevelopmentSettore ICAR/04 - Strade Ferrovie Ed AeroportiCrumb rubberBuilding and ConstructionLaboratory scaleComposite materialSafety Risk Reliability and QualityCivil and Structural Engineering
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CFD simulations of early- to fully-turbulent conditions in unbaffled and baffled vessels stirred by a Rushton turbine

2021

Abstract Laboratory scale unbaffled tanks provided with a top cover and a baffled tank both stirred by a Rushton turbine were simulated by carrying out RANS simulations. Three different turbulence models were adopted (k- ω SST, k- e and the SSG Reynolds stress model) to predict the flow field and the relevant performance parameters (power and pumping numbers) of the tank operated from early to fully turbulent conditions. CFD results were compared with literature experimental data and DNS simulation results to validate and properly compare the models. In the range of Reynolds numbers investigated, results showed that, for the unbaffled tank, the SSG model based on Reynolds stresses is a bett…

Settore ING-IND/26 - Teoria Dello Sviluppo Dei Processi Chimicibusiness.industryTurbulenceGeneral Chemical EngineeringSettore ING-IND/25 - Impianti ChimiciReynolds number02 engineering and technologyGeneral ChemistryReynolds stressMechanicsComputational fluid dynamicsLaboratory scale021001 nanoscience & nanotechnologyFlow fieldRushton turbinesymbols.namesake020401 chemical engineeringCFD SSG Stirred tank Turbulence model Unbaffled vesselsymbols0204 chemical engineering0210 nano-technologybusinessReynolds-averaged Navier–Stokes equationsSettore ING-IND/19 - Impianti NucleariMathematics
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Comparison of laboratory-scale thermophilic biofilm and activated sludge processes integrated with a mesophilic activated sludge process

2003

A combined thermophilic-mesophilic wastewater treatment was studied using a laboratory-scale thermophilic activated sludge process (ASP) followed by mesophilic ASP or a thermophilic suspended carrier biofilm process (SCBP) followed by mesophilic ASP, both systems treating diluted molasses (dilution factor 1:500 corresponding GF/A-filtered COD (COD(filt)) of 1900+/-190 mgl(-1)). With hydraulic retention times (HRTs) of 12-18 h the thermophilic ASP and thermophilic SCBP removed 60+/-13% and 62+/-7% of COD(filt), respectively, with HRT of 8 h the removals were 48+/-1% and 69+/-4%. The sludge volume index (SVI) was notably lower in the thermophilic SCBP (measured from suspended sludge) than in …

Suspended solidsEnvironmental EngineeringSewageWaste managementRenewable Energy Sustainability and the EnvironmentChemistryThermophileTemperatureBiofilmBioengineeringGeneral MedicineLaboratory scalePulp and paper industryWaste Disposal FluidAerobiosisBiodegradation EnvironmentalActivated sludgeBiofilmsSewage treatmentWater MicrobiologyWaste Management and DisposalEffluentMesophileBioresource Technology
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Investigation of flashing phenomena in MSF chambers

2007

The MSF process has covered in the last years more than 50% of world production of desalinated water from the sea. Although this process has been used for several decades, the large energy requirements force to search for new and feasible ways to improve the overall thermal efficiency. Few studies have bee carried out in lab-scale, pilot and industrial MSF units, underlining the complexity of flashing phenomena and the importance of operating parameters settings for optimal performance. In the present work a study on fundamental phenomena occurring inside MSF chambers has been carried out, focusing on the dependence of flashing efficiency on operating parameters and the effects of flashing …

Thermal efficiencyEngineeringSettore ING-IND/26 - Teoria Dello Sviluppo Dei Processi Chimicibusiness.industryMechanical EngineeringGeneral Chemical EngineeringFLOWEnvironmental engineeringProcess (computing)NONEQUILIBRIUMEVAPORATORSGeneral ChemistryLaboratory scaleFlashingEnergy requirementENERGYDESALINATIONGeneral Materials ScienceProcess engineeringbusinessWater Science and Technology
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ChemInform Abstract: Elemental Bromine Production by TiO2Photocatalysis and/or Ozonation.

2016

Significant production of elemental bromine (Br2 ) was observed for the first time when treating bromide containing solutions at acidic pH, with TiO2 photocatalyst, ozone, or a combination thereof. Br2 selectivities up to approximately 85 % were obtained and the corresponding bromine mass balance values satisfied. The process is general and may be applied at a laboratory scale for green bromination reactions, or industrially as a cheap, safe, and environmentally sustainable alternative to the currently applied bromine production methods.

chemistry.chemical_compoundOzoneBrominechemistryBromideInorganic chemistryPhotocatalysisHalogenationchemistry.chemical_elementTio2 photocatalystGeneral MedicineLaboratory scaleChemInform
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Co-treatment of landfill leachate in laboratory-scale sequencing batch reactors: analysis of system performance and biomass activity by means of resp…

2014

Aged or mature leachate, produced by old landfills, can be very refractory; for this reason mature leachate is difficult to treat alone, but it can be co-treated with sewage or domestic wastewater. The aim of the study was to investigate the feasibility of leachate co-treatment with synthetic wastewater, in terms of process performance and biomass activity, by means of respirometric techniques. Two sequencing batch reactors (SBRs), named SBR1 and SBR2, were fed with synthetic wastewater and two different percentages of landfill leachate (respectively 10% and 50% v v−1 in SBR1 and SBR2). The results showed good chemical oxygen demand (COD) removal efficiency for both reactors, with average C…

education.field_of_studyEnvironmental EngineeringSettore ICAR/03 - Ingegneria Sanitaria-Ambientalebusiness.industryCell RespirationChemical oxygen demandPopulationHeterotrophBiomassSewageLaboratory scaleBioreactorsbiological treatment leachate respirometric techniques SBR systemWastewaterEnvironmental chemistryAmmonium CompoundsEnvironmental scienceBiomassLeachateOrganic ChemicalsbusinesseducationWater Pollutants ChemicalWater Science and Technology
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