Search results for "MEA"
showing 10 items of 8532 documents
Information content of data and variables and types of weighting in least-squares regression methods
1990
Abstract Algorithms are given for evaluating the relative amount of useful information related to a particular parameter which is carried by individual data points and intervals of the variables. The algorithms provide an efficient means of using the information contained in a set of data. Applications to the optimization of weighting in regression methods are described. Several informational and combined informational-statistical types of weighting are studied as a means of improving the accuracy and precision of the parameters obtained by non-linear regression.
Steam sterilization processes affect the stability of clinical thermometers: Thermistor and prototypal FBG probe comparison
2020
Abstract Temperature is one of the most frequently measured physical quantities in clinical environment and a good biomarker of illness. The need for reusable probes, which have to be sterilized to prevent infections, requires the metrological qualification of thermometer probes in response to ageing effects induced by several sterilization processes. In this study, we investigated the effect of repeated sterilizations on both a commonly-used autoclavable thermistor probe and a prototypal Fiber Bragg Gratings (FBG) probe for temperature measurements. Findings highlighted a greater reliability of the proposed FBG probe than the commercial thermistor. Specifically, the FBG probe was able to w…
Determination of phosphorus by instrumental neutron activation and bremsstrahlung measurement in bone samples
1997
A non destructive method based on the31P(n,γ)32P reaction for the assay of phosphorus in bone samples is described. This method involves a thermal neutron irradiation of 2 minutes in a reactor followed by the measurement of the bremsstrahlung produced by the β− of32P in a Ge-detector surrounded by an anti-Compton shield. Accuracy and precision were tested by analysing the certified NIST 1486 Bone Meal reference material and tri-calcium phosphate (Ca3(PO4)2) samples. The value obtained for the reference material was in good agreement with the certified value and with relative standard deviation of 4.1% the precision was acceptable. The value obtained for Ca3(PO4)2 shows a deviation of −6% fr…
Comparison of in Situ Land Surface Temperatures Measured with Radiometers and Pyrgeometers: Consequences for Calibration and Validation of Thermal In…
2018
Land surface temperature (LST) is a key magnitude in many exchange processes between the surface and the atmosphere. LST measurement from satellites provides an efficient way to monitor its change across wide areas on Earth, an essential issue being LST validation using in situ measurements to assess its accuracy and precision. Presently, there are two widely used methodologies: temperature measurements made by wideband radiometers observing the land surface with a given viewing angle and a limited field of view, and measurements provided by total radiation pyrgeometers with a nearly hemispheric field of view. Although both measurements are correlated, they are not equivalent; thus, it is r…
3D reconstruction of hot metallic surfaces for industrial part characterization
2009
During industrial forging of big hot metallic shells, it is necessary to regularly measure the dimensions of the parts, especially the inner and outer diameters and the thickness of the walls, in order to decide when to stop the forging process. The inner and outer diameters of the shells range from 4 to 6 meters and to measure them a large ruler is placed horizontally at the end of the shell. Two blacksmiths standing on each side of the ruler at about ten meters from it visually reads the graduations on the ruler in order to determine the inner and outer diameters from which the thickness of the wall is determined. This operation is carried out several times during a forging process and it…
Sample Preparation Improvement in Polycyclic Aromatic Hydrocarbons Determination in Olive Oils by Gel Permeation Chromatography and Liquid Chromatogr…
2005
Abstract The determination of 15 polycyclic aromatic hydrocarbons (PAHs) in olive oil samples has been improved in order to obtain a fast methodology with a low limit of detection through the combination of liquid–liquid extraction with acetonitrile and preparative gel permeation chromatography (GPC) prior to the injection of purified extracts into a C18 column. Acetonitrile–water was used as the mobile phase with a gradient from 50 to 95%, w/w, acetonitrile in 30 min. The oven temperature was maintained at 15°C, and fluorometric detection was made at a fixed excitation wavelength of 264 nm and variable, optimal emission wavelength for each analyte ranging from 352 nm for 11-H-benzo(b)fluor…
Renewable polyol obtained by microwave-assisted alcoholysis of epoxidized soybean oil: Preparation, thermal properties and relaxation process
2019
[EN] The soybean oil polyol (SOP) use as feedstock in the polyurethane industry has been recently emphasized due to its excellent resistance to hydrolysis, which is also applicable in coatings and thermal insulation. In this article, the SOP was obtained by a very fast microwave-assisted alcoholysis of epoxidized soybean oil (ESO). The preparation method, thermal properties, and relaxation process were evaluated. High yields as opening and consumption epoxy group and selectivity of 99.8 mol%, 985 mol%, and 71.2 mol% were obtained. Through titrations, nuclear magnetic resonance and gel permeation chromatography were identified parameters as 0.32 mg KOH.g(-1) acid number, 190 mg KOH.g(-1) hyd…
Electronic properties of Co2MnSi thin films studied by hard x-ray photoelectron spectroscopy
2009
This work reports on the electronic properties of thin films of the Heusler compound Co2MnSi studied by means of hard x-ray photoelectron spectroscopy (HAXPES). The results of photoelectron spectroscopy from multilayered thin films excited by photons of 2?8?keV are presented. The measurements were performed on (substrate/buffer layer/Co2MnSi(z)/capping layer) multilayers with a thickness z ranging from 0 to 50?nm. It is shown that high energy spectroscopy is a valuable tool for non-destructive depth profiling. The experimentally determined values of the inelastic electron mean free path in Co2MnSi increase from about 19.5 to 67?? on increasing the kinetic energy from about 1.9 to 6.8?keV. T…
Hard x-ray photoelectron spectroscopy of buried Heusler compounds
2009
This work reports on high energy photoelectron spectroscopy from the valence band of buried Heusler thin films (Co2MnSi and Co2FeAl0.5Si0.5) excited by photons of about 6?keV energy. The measurements were performed on thin films covered by MgO and SiOx with different thicknesses from 1 to 20?nm of the insulating layer and additional AlOx or Ru protective layers. It is shown that the insulating layer does not affect the high energy spectra of the Heusler compound close to the Fermi energy. The high resolution measurements of the valence band close to the Fermi energy indicate a very large electron mean free path of the electrons through the insulating layer. The spectra of the buried thin fi…
Subjective ranking of concert halls substantiated through orthogonal objective parameters.
2015
[EN] This paper studies the global subjective assessment, obtained from mean values of the results of surveys addressed to members of the audience of live concerts in Spanish auditoriums, through the mean values of the three orthogonal objective parameters (Tmid, IACCE3, and LEV), expressed in just noticeable differences (JNDs), regarding the best-valued hall. Results show that a linear combination of the relative variations of orthogonal parameters can largely explain the overall perceived quality of the sample. However, the mean values of certain orthogonal parameters are not representative, which shows that an alternative approach to the problem is necessary. Various possibilities are pr…