Search results for "Metal complex"

showing 7 items of 67 documents

The interaction of novel transition metal complexes and ligands with biomolecular targets: kinetic, thermodynamic and computational investigations.

metal complexesDNA
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Structure ofD-ribonic acid-dimethyltin(IV) in coordinating solvents: an experimental and DFT119Sn NMR study

2006

We have investigated a newly synthesized complex of D-ribonic acid with dimethyltin(IV). The structure of the complex in solution has been characterized by means of 1 H, 13 C, and 119 Sn NMR and by DFT calculations. The comparison of experimental and computational results allowed the determination of the stable conformation in solution as well as the detection of a dimerization process. Moreover, evidence is given of active coordination of the metal by the solvent.

organotin compounds; ribonic acid; carbohydrate-metal complexes; 119Sn NMR; DFT calculationsChemistryOrganic Chemistrycarbohydratestin compoundstin-119carbohydrates; tin compounds; tin-119; NMR spectroscopy; computational chemistrycomputational chemistryMetalSolventNMR spectroscopyComputational chemistryvisual_art119Sn NMR Carbohydrate-metal complexes DFT calculations Organotin compounds Ribonic acidvisual_art.visual_art_mediumOrganic chemistryPhysical and Theoretical ChemistryJournal of Physical Organic Chemistry
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Complex species formation of Cu and Cd metal ions with polyacrylate, polymethacrylate and alginate ligands. Potentiometric investigation by ISE-H+ an…

2008

potentiometrySettore CHIM/01 - Chimica Analiticametal complexespolyelectrolyte
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Progression of Diiminopyridines: From Single Application to Catalytic Versatility

2015

Diiminopyridyl metal complexes, first characterized several decades ago, found practical application in 1998 when they were used as precatalysts in coordinative ethylene polymerization. This discovery contributed to the so-called postmetallocene revolution and triggered the large-scale experimental and theoretical research aimed at understanding diversified diiminopyridine chemistry. The results of this quest, some of which were intriguing and difficult to anticipate, are discussed and summarized in the current Review.

redox reactiontransition metal complexChemistrySingle applicationTheoretical researchNanotechnologyGeneral ChemistryCatalysisdiiminopyridinechemistry.chemical_compoundaluminum alkylEthylene polymerizationcooperative effectsOrganic chemistryOlefin polymerizationAluminum alkylolefin polymerizationDiiminopyridineACS Catalysis
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A Theoretical and Experimental Investigation of the Spectroscopic Properties of a DNA-Intercalator Salphen-Type ZnIIComplex

2014

The photophysical and DNA-binding properties of the cationic zinc(II) complex of 5-triethylammonium methyl salicylidene ortho-phenylenediiminato (ZnL 2 + ) were investi- gated by a combination of experimental and theoretical methods. DFT calculations were performed on both the ground and the first excited states of ZnL 2 + and on its possi- ble mono- and dioxidation products, both in vacuo and in selected solvents mimicked by the polarizable continuum model. Comparison of the calculated absorption and fluores- cence transitions with the corresponding experimental data led to the conclusion that visible light induces a two-elec- tron photooxidation process located on the phenylenediimi- nato…

spectroscopyNO ligandStereochemistryIntercalation (chemistry)Ionic bondingmetal complex Fluorescence spectroscopy DNA recognition metal complexes organometallics complex formation DNA binding drugs fluorescence spectroscopy equilibrium constants reaction mechanisms nucleic acids affinity binding mode thermodynamics speciationmetal complexesbinding modePhenylenediaminesPolarizable continuum modelCatalysisdrugsmetal complexthermodynamicsintercalationcomplex formationOrganometallic CompoundsA-DNADNA bindingFluorescence spectroscopyDNA recognitionphotochemistryLigandChemistrySpectrum AnalysisphotooxidationOrganic ChemistryCationic polymerizationequilibrium constantsGeneral Chemistrydensity functional calculationFluorescenceZincCrystallographyreaction mechanismsnucleic acidsspeciationSettore CHIM/03 - Chimica Generale E InorganicaExcited stateaffinityfluorescenceorganometallics
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Role of Vibrational Dynamics in Electronic Relaxation of Cr(acac)3

2015

Ultrafast energy relaxation of Cr(acac)3 dissolved in tetrachloroethylene (TCE) is studied by time-resolved infrared (TRIR) spectroscopy by using electronic and vibrational excitation. After electronic excitation at 400 or 345 nm, the ground state recovers in two time scales: 15 ps (major pathway) and 800 ps (minor pathway), corresponding to fast electronic transition to the ground state and intermediate trapping on the long-lived (2)E state followed by intersystem crossing (ISC) to the ground state. The quantum yield for the fast recovery of the ground state depends on the excitation wavelength, being higher for 345 nm. Vibrational cooling (VC) occurs on the electronic excited states with …

ta114ChemistryRelaxation (NMR)kinetic modelsQuantum yieldMolecular physicsMolecular electronic transitiontransition metal complexesvibrationsIntersystem crossingComputational chemistryExcited statePhysical and Theoretical ChemistryGround stateSpectroscopyta116ExcitationThe Journal of Physical Chemistry A
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Sintesi di complessi metallici e studio della loro interazione con acido desossiribonucleico.

2011

transition metal complexes; deoxyribonucleic acid.transition metal complexeSettore CHIM/03 - Chimica Generale E Inorganicadeoxyribonucleic acid.
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