Search results for "Microstructure"
showing 10 items of 707 documents
Hardening of Steel Perforated Tape by Nd:YAG Laser
2016
One of the directions of application of the perforated metal material is their use as cutting elements in the production of processing tools. In this case it is necessary to carry out hardening of cutting surfaces to increase their hardness. One of the methods of hardening metals could be laser treatment. Therefore, the present work is a study of the effect of Nd:YAG laser radiation on the microstructure and hardness of fragments formed from steel perforated tape. Different laser scan speeds (doses) were used in the experiments. The results have shown that the increase the microhardness of 30-40% after the laser treatment of steel perforated tape in the surface layer in a depth range up to …
Processing conditions, microstructure and mechanical properties of hetero-nanostructured ODS FeAl alloys produced by spark plasma sintering
2013
International audience; Spark plasma sintering (SPS) has been used to sinter a milled oxide dispersion-strengthened (ODS) FeAl powder in order to prepare dense nanostructured parts. The effect of processing conditions including sintering temperature, holding time and degassing treatments on the microstructure and mechanical properties of the as-sintered materials was investigated. A hetero-nanostructure that contains nano, ultrafine and micrometric grains was confirmed to be developed whatever the processing window, due to the large temperature difference generated during the SPS process itself. The grain size distribution can be tailored by selecting a combination of sintering temperature …
Peculiarities of Forming of Magnetic Hardening in Sintered Nd15Fe76.2Ti1.0Al0.8B7 Permanent Magnet by Ageing
1999
Variations of the intrinsic coercivity ( i H c ) with ageing (at 293 to 1173 K for 0.45 to 57.6 ks) of sintered Nd 15 Fe 76.2 Ti 1.0 Al 0.8 B 7 have been investigated. The tests indicated minimum and maximum of intrinsic coercivity ( i H min c and i H max c ) at temperatures 725 K and 1025 K, respectively. The observed behaviour of i H c has been compared with microhardness measurements and microstructure observations (SEM, EDAX, domain structure (DS) and room temperature Mossbauer spectroscopy). SEM and DS investigations gave hints to a change in microstructure. Fitting of the Mossbauer spectra of permanent magnets for different i H c has shown that the magnetic hyperfine field Bhf of 8j2 …
Scaling properties of magnetic domain walls in Pt/Co/Pt trilayers on MgO (111)
2002
Abstract We present a scaling analysis of the time evolution of domain walls in ultrathin magnetic films that are subject to different forms of uncorrelated and correlated disorder caused by the microstructure of the underlying template. The study is performed on ultrafine modulated Pt/Co/Pt trilayers grown on as-supplied and structured MgO (1 1 1) substrates employing polar Kerr microscopy for the imaging of the magnetic domains.
Effect of zinc concentration on the microstructure and relaxation frequency of Mn–Zn ferrites synthesized by solid state reaction
2013
Abstract Mn3Zn polycrystalline ferrites with Mn1−xZnxFe2O4 stoichiometry (x=0.59, 0.61, 0.65) were prepared by solid state reaction. These ferrites were heated at different temperatures. The cubic structure with space group Fd3m (Oh7) No. 227 was confirmed by the refinement of x-ray diffraction (XRD) powders through Rietveld´s method using fullprof. Scanning electron microscopy (SEM) results revealed for all compounds a non-homogeneous grain size and shape distribution, with a mean grain size of 9 μm. The Curie temperature Tc was found to decrease as the Zn concentration increases. The magnetic domain relaxation was investigated by inductance spectroscopy (IS). The relaxation frequency fr s…
Influence of the microstructure and laser shock processing (LSP) on the corrosion behaviour of the AA2050-T8 aluminium alloy
2011
International audience; The corrosion behaviour of AA2050-T8 was studied after polishing and after laser shock processing (LSP) treatment using the electrochemical microcell technique and the SVET. After polishing, pitting at constituent particles and intergranular corrosion were observed. By contrast, no intergranular corrosion developed after LSP. Microcell measurements revealed that LSP increases the pitting potential. SVET measurements revealed that local anodic currents are systematically lower on LSP-treated surfaces than on polished ones. The current density on the LSP-treated surface remains constant around 50 μA cm−2 up to 123 min after immersion, while on the polished surface it r…
Local electrochemical impedance spectroscopy study of the influence of ageing in air and laser shock processing on the micro-electrochemical behaviou…
2011
International audience; In the present paper, the micro-electrochemical behaviour of AA2050-T8 in 0.1 M NaCl was first studied after polishing by means of local electrochemical impedance spectroscopy and field-emission scanning electron microscopy/electron dispersive spectroscopy (FE-SEM/EDS). The influence of ageing in air and LSP was then investigated. Ageing in air for three months led to an increase in the charge transfer resistance. This was clearly observed in sites surrounding constituent particles where the charge transfer resistance was in the order of 1 MΩ cm2 (instead of 10-3 MΩ cm2 after polishing). Increased passivity around particles was confirmed from FE-SEM/EDS analysis. On …
Corrosion resistance of the FeAlC permanent magnet alloy
1998
Abstract The correlation between corrosion behaviour rate of hard magnetic FeAlC alloys and their microstructure and phase composition is presented. Potentiokinetic polarization curves of the tested material in acid (pH = 1 and 2) and neutral (pH = 7) sulphate solutions have been measured. For open-circuit condition, kinetic curves of etching of the samples in 0.5 M H2SO4 have been determined. The resistance of the tested magnets against atmospheric corrosion has been evaluated using a salt-spray test. The atmospheric corrosion rate is 1.5–2 times slower than that found for Nd-Fe-B type magnets. The FeAlC alloys show good corrosion resistance in neutral environments and corrode at rates…
Beta forging of Ti-6Al-4V: Microstructure evolution and mechanical properties
2013
Titanium alloys are finding an increasing use in the aeronautical field, due to their characteristics of high mechanical properties, lightness and corrosion resistance. Moreover these alloys are compatible with the carbon fibre reinforced plastics that are also finding a wide use in the aeronautical field. On the other hand the use of these alloys implies some drawbacks, for example titanium alloys are often considered more difficult to form and generally have less predictable forming characteristics than other metallic alloys such as steel and aluminum. In this paper was studied both the microstructure evolution and the mechanical properties of a Ti-6Al-4V rolled bar after hot forging. The…
TEM studies on La2−2xCa1+2xMn2O7 (x=0.5 and 0.25)
2003
The nominal compositions and structures of the compounds La2-2xCa1+2xMn2O7 (x=0.5 and 0.25) prepared by solid-state reaction have been studied by transmission electron microscopy and high-resolution electron microscopy. Besides the observation of the major phase of a two-layer structure in the nominal composition La1.0Ca2.0Mn2O7, the embedded n = 3, n = 4 Ruddlesden-Popper phases and La rich phase in the two-layer structure were observed as defects. No layered structure was observed in the nominal composition La1.5Ca1.5Mn2O7. Instead, a major phase of orthorhombically distorted perovskite, a minor phase of an ideal cubic perovskite, and a small fraction of calcium-oxide were observed in the…