Search results for "Microstructure"

High temperature alloy chloridation at 850°C. Part I: Comparison of Ni-based and Fe-based alloy behaviour

2007

Eight alloys were tested under Ar/Cl 2 atmosphere at 850 °C for 15 min and 1 h. Their gross and net weights were evaluated together with the base metal consumption. Macroscopic and microscopic micrographs, associated with chemical analyses and X-ray diffraction gave the composition and microstructure of the corrosion products. Huge differences were observed if one compared the nickel based alloy behaviour to that of the iron based alloy. Molybdenum and tungsten could also play a role, but it was not clearly defined until now. A tentative evaluation of the best candidates will be given, according the experimental conditions of this work and the chosen criteria. A corrosion index was establis…

Electrochemical behavior of nanocrystalline iron aluminide obtained by mechanically activated field activated pressure assisted synthesis

2004

Abstract The corrosion behavior of nanocrystalline iron aluminide obtained by mechanically activated field—activated pressure—assisted synthesis was investigated in sulphuric acid media using potentiodynamic curves. The effect of microstructure on the electrochemical corrosion resistance was investigated by examining samples which were heat treated to effect a change in crystallite size and microdistorsion.

Tool Path Design in Friction Stir Spot Welding of AA6082-T6 Aluminum Alloys

2007

In the paper, a variation of the Friction Stir Spot Welding (FSSW) process has been considered. In particular, a particular tool path is given after the sinking phase nearby the initial penetration site. The process mechanics was highlighted and the joint strength was considered at the varying of the most relevant process parameters. Furthermore macro and micro analyses were developed in order to highlight the process mechanics and the local material microstructure evolution. The investigated technology appears a promising joining technique in order to develop effective spot joints.

Sintered (Nd, Tb)–(Fe, Ti)–B+C permanent magnets

2001

Abstract This paper undertakes a study of the effect of carbon addition on the magnetic properties, the microstructure and corrosion resistance of Nd14.60Tb0.20Fe77.56Ti1.24B6.40+C sintered permanent magnets. It is shown that a 0.12 wt.% C addition increase the remanence and the maximum energy product and reduces (slightly) the intrinsic coercivity. The corrosion resistance in atmospheric environment is also significantly improved by this element.

Mechanical and microstructural characterization of friction stir welded skin and stringer joints

2013

A microstructural and mechanical investigation on lap joints welded by friction stir welding and made out of a 7075-T6 stringer and a 2024-T4 skin is presented. In particular, the metallurgical and mechanical properties of joints have been studied at different tool feed rates (V = 35, 50, 100 mm/min) and constant rotation speed (R = 500 r/min). Temperature distributions have been monitored during the process. It is found that in the welded area, the recrystallized zone (nugget) has an average grain size of about 3 µm and exhibits coarsened MgZn2 particles on grain boundaries. The maximum values of microhardness in the welded skin increase with the process temperature, while they just sligh…

Texture Effects on Zircaloy Oxidation : Experiment and Simulation

2002

Mechanical properties and corrosion behaviour of low carbon martensitic stainless steel after machining

2014

The influence of different combinations of cutting conditions on the mechanical behaviour (microhardness), the microstructure and the corrosion behaviour in NaCl solution (using the electrochemical microcell technique and pulse potentiodynamic testing) of a low carbon martensitic stainless steel (grade X4CrNiMo16.5.1 stainless steel) after tempering treatment was studied. Microhardness was increased on the machined surface. In addition, the electrochemical experiments have shown that the machined materials have a heterogeneous electrochemical behaviour. Significant effect of machining on pitting corrosion was noticed. The pitting potential was found to decrease as the microhardness increase…

Influence of sintering temperature on microstructure of Na0.5Bi0.5TiO3 ceramics

2021

Abstract Na0.5Bi0.5TiO3 (NBT)-based compositions are among the most promising lead-free ferroelectrics. Although studies of modification of NBT-based compositions’ properties are a hot topic, there has been very little attention paid to their characterization from the standpoint of ceramics and the process of producing them. Here, we report on comprehensive analysis of the influence of sintering temperature across a wide temperature range (1020–1240 °C) on the complete microstructure and chemical content of NBT ceramics produced by solid state sintering, which is dominating in producing of NBT ceramics. Thorough attention is paid to the grain size distribution, porosity, and inhomogeneity. …

Layered-structural monoclinic–orthorhombic perovskite La2Ti2O7 to orthorhombic LaTiO3 phase transition and their microstructure characterization

2014

The layered-structural ceramics, such as lanthanum titanate (La{sub 2}Ti{sub 2}O{sub 7}), have been known for their good temperature and low dielectric loss at microwave frequencies that make them good candidate materials for high frequency applications. However, few studies have been conducted on the synthesis optimization by sol gel reaction, in particular by acrylamide polymerization route. The interest in La{sub 2}Ti{sub 2}O{sub 7} ceramic has been greatly increased recently due to the effect of oriented grains. This anisotropy of the microstructure leads to anisotropy in dielectric, electrical and mechanical properties. In this study, grain oriented lanthanum titanate was produced by t…

Local analysis of the mechanical behaviour of inclusions-containing stainless steels under straining conditions

2003

Abstract A numerical method is described for determining the surface stress distribution under straining conditions from the real microstructure of materials containing local heterogeneities. The method is applied to resulfurized steels with a high density of MnS and oxide inclusions. The results are compared to those obtained from surface observations.