Search results for "Microstructure"
showing 10 items of 707 documents
Temperature control during Spark Plasma Sintering and application to up-scaling and complex shaping
2013
International audience; The determination and the homogeneity of the sample temperature during consolidation of powders by Spark Plasma Sintering (SPS) are addressed. Densifications were carried out in three different facilities differing by their constructors and their size. A structural transformation activated in a TiAl alloy was used as a marker of the sample temperature and finite element modeling were performed to evaluate the temperature at each point of the set-up. A good agreement between experimental and simulated data is exhibited. Alloys with identical microstructures were sintered and the homogeneity of the microstructure was better in the largest machines or when the sample wa…
Influence of external stretching on hydrogen electromigration in Pd and PdCu, PdAg alloys
2005
Influence of external stretching of Pd and Pd77Cu23 and Pd77Ag23 alloys on hydrogen electromigration in these systems was investigated. The electro-resistivity method was applied in the investigations. It was found that in order to furnish a full description of the kinetics and dynamics transport of hydrogen in the externally applied electric field to samples in the state of elastic and plastic stretching, it is not sufficient to provide a functional dependence of two commonly used parameters (diffusion coefficient D and effective valence Zeff) on degree of deformation. To describe the electromigration in these conditions a mathematical model was applied, which assumes the existence of two …
Electropolishing of CuZn brasses and 316L stainless steels: Influence of alloy composition or preparation process (ALM vs. standard method)
2016
International audience; In the present paper, electropolishing behavior of different brass alloys (CuZn39Pb2, CuZn42) in phosphoric acid is studied to observe the impact of alloying elements on polishing quality. In the same way, the influence of the manufacturing process is also evaluated through the comparison of a “standard” stainless steel and a stainless steel prepared by Additive Laser Manufacturing (ALM). An electrochemical study was first performed to determine the best treatment conditions for each material/electrolyte pair and to study the electropolishing mechanism and its kinetic dependence on diffusion. Metallic samples are fully characterized before and after electropolishing …
Comparative X-ray diffraction study of the crystalline microstructure of tetragonal and monoclinic vanadium–zirconium dioxide solid solutions produce…
2009
The microstructural characteristics of solid solutions, prepared by heating dried gel precursors with nominal compositions VxZr1−xO2(0 ≤x≤ 0.1) at 723 and 1573 K, were determined from X-ray diffraction patterns. The crystalline microstructure of the resulting specimens, characterized by a prevalent crystallite shape, a volume-weighted crystallite size distribution and a second-order lattice strain distribution, was found to depend on the vanadium content. A characteristic feature of all size distributions was their bimodality, explained as a result of transformations between tetragonal and monoclinic phases during thermal treatment. A comparative study of the microstructure of both zirconia…
Microstructure-oxidation resistance relationship in Ti3AlC2 MAX phase
2020
International audience; Spark Plasma Sintering and Hot Isostatic Pressing were used to synthesize coarse-grained and fine-grained Ti3AlC2 specimens. Moreover, Spark Plasma Sintering processing parameters were modified in order to vary the TiC, Al2O3 and TixAly impurity and the porosity contents in the fine-grained samples. The influence of the Ti3AlC2 microstructure on the oxidation resistance was assesed. It is demonstrated that the grain size can drastically modify the oxidation resistance. The higher density of grain boundaries, in fine-grained specimens, increases the number of Al diffusion paths and leads to the formation of a protective alumina scale. In coarse-grained sample, Al diff…
Room-Temperature Micropillar Growth of Lithium-Titanate-Carbon Composite Structures by Self-Biased Direct Current Magnetron Sputtering for Lithium Io…
2019
Here, an unidentified type of micropillar growth is described at room temperature during conventional direct-current magnetron sputtering (DC-MS) deposition from a Li4Ti5O12+graphite sputter target under negative substrate bias and high operating pressure. These fabricated carbon-Li2O-TiO2 microstructures consisting of various Li4Ti5O12/Li2TiO3/LixTiO2 crystalline phases are demonstrated as an anode material in Li-ion microbatteries. The described micropillar fabrication method is a low-cost, substrate independent, single-step, room-temperature vacuum process utilizing a mature industrial complementary metal-oxide-semiconductor (CMOS)-compatible technology. Furthermore, tentative considerat…
Tuning four-wave mixing through temperature in ethanol-filled photonic crystal fiber
2016
In this paper, continuous tuning of four-wave mixing bands in an ethanol-filled photonic crystal fiber is investigated. A wide tuning range of the parametric bands, from 745 nm to 920 nm (signal) and from 1260 nm to 1710 nm (idler), is achieved through the thermo-optic effect. This corresponds to a frequency tuning range higher than 2000 cm−1; such wide range can be particularly useful in applications that require broadband wavelength conversion, e.g., CARS microscopy. Numerical calculations are in good agreement with experimental measurements.
Experimental investigation of effect of printing direction and surface roughness on the mechanical properties of AlSi10Mg-alloy produced by selective…
2021
The additive manufacturing has initially gained popularity for production of non-loadbearing parts and components or in the fields where the material strength and ductility are less important such as modelling and rapid prototyping. But as the technology develops, availability of metal additive manufacturing naturally dictates the desire to use the produced components in load-bearing parts. This requires not-only a thorough documentation on the mechanical properties but also additional and independent research to learn the expected level of variation of the mechanical properties and what factors affect them. The presented paper investigates strength, ductility, hardness, and microstructure …
Experimental Characterization of FSW T-Joints of Light Alloys
2007
Welding is playing a growing role in transport industry due to relevant advantages it allows. Friction Stir Welding is considered one of the most promising joining technologies, especially when it is applied to light alloys. Focusing attention on FSW of T-joints, several parameters have to be considered, and due to thermo-mechanical features of process, T joints need a dedicated approach. A set of previously developed experiments has shown that the tilt angle plays a relevant role in the joint strength. Furthermore it should be observed that T-joints are very often utilized in aerospace industries since the produced structures are composed of joined skins and stingers. Numerous data are rep…
Material flow in fsw of aa7075-t6 butt joints: continuous dynamic recrystallization phenomena
2006
In the paper the continuous dynamic recrystallization (CDRX) phenomena occurring in the FSW of AA7075-T6 butt joints is investigated at the varying of the most relevant technological and geometrical parameters. In particular, both experiments and numerical simulations obtained utilizing a 3D Lagrangian implicit, coupled, rigid-viscoplastic model have been developed on FSW butt joints. The resulting microstructure at the core of the weldings is correlated to the material flow occurring during the FSW process.