Search results for "NOGEL"

showing 10 items of 121 documents

Nanohydrogel Formation within the Halloysite Lumen for Triggered and Sustained Release

2018

An easy strategy to obtain nanohydrogels within the halloysite nanotube (HNTs) lumen was investigated. Inorganic reverse micelles based on HNTs and hexadecyltrimethylammonium bromides were dispersed in chloroform, and the hydrophilic cavity was used as a nanoreactor to confine the gel formation based on alginate cross-linked by calcium ions. Spectroscopy and electron microscopy experiments proved the confinement of the polymer into the HNT lumen and the formation of calcium-mediated networks. Biological tests proved the biocompatibility of the hybrid hydrogel. The nanogel in HNTs was suitable for drug loading and sustained release with the opportunity of triggered burst release by chemical …

NanotubeMaterials scienceBiocompatibilityChlorine compound02 engineering and technologyNanoreactorHexadecyl trimethyl ammonium bromideengineering.materialHybrid hydrogel010402 general chemistry01 natural sciencesMicelleHalloysiteSustained release Drug deliveryAdsorptionKaoliniteHalloysite nanotube (HNTs)Chemical stimuliGeneral Materials ScienceControlled drug deliveryBiological testSettore CHIM/02 - Chimica Fisicachemistry.chemical_classificationTargeted drug deliveryCrosslinkingReverse micellePolymer021001 nanoscience & nanotechnology0104 chemical sciencesChemical engineeringchemistryYarn Biological applicationengineeringBiocompatibilityCalcium0210 nano-technologyMicelleNanogelACS Applied Materials & Interfaces
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Numerical simulations of the kinetics of pulsed electron beam induced synthesis of nanogels in dilute aqueous polymer solutions

2018

Nanogel can be produced by irradiation of dilute aqueous polymer solutions. The nanogels are formed primarily through intramolecular radical-radical crosslinking reactions between two polymer radical sites.

Numerical simulation electron beam nanogelsSettore CHIM/07 - Fondamenti Chimici Delle Tecnologie
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About entangled networks of worm-like micelles: a rejected hypothesis

1996

We report new results from small-angle neutron scattering on d(1 2)-cyclohexane/lecithin/water micellar solutions performed as a function of the water content (w(o)), temperature (T) and dispersed phase volume fraction (phi). The data from dilute samples are interpretable in terms of the existence of giant cylindrical reverse micelles and are well fit with a core-shell model (that provides the micelle structure and dimensions) with values of 28 and 45 Angstrom for the inner core and the outer shell radii, almost independent on temperature and concentration. Such a result could appear consistent with the current idea that worm-like micelles are living polymers. On the contrary, the appearanc…

ORGANOGELSPolymers and PlasticsSANSChemistryInner coreForm factor (quantum field theory)Concentration effectThermodynamicsMineralogyliving polymersNeutron scatteringgelsSmall-angle neutron scatteringMicelleLIGHT-SCATTERINGCondensed Matter::Soft Condensed MatterColloid and Surface ChemistryMICROEMULSIONSMicellar solutionsMaterials Chemistryreverse micellesPhysical and Theoretical ChemistryStructure factorLECITHIN REVERSE MICELLESColloid and Polymer Science
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Two components organogels as molecular recognition systems: properties, behavior and future applications

Organogels diimidazolium salts molecular recognition
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Diimidazolium-based organic salts as low molecular weight hydro- and organogelator

Organogels hydrogel self-assembly
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Synthesis of new fluorinated low molecular weight (LMW) gelators

2011

Oxadiazoles fluorinated compounds LMW gelators organogels hydrogelsSettore CHIM/06 - Chimica Organica
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On the nature of macroradicals formed upon radiolysis of aqueous poly(N-vinylpyrrolidone) solutions

2020

In this work we have explored the nature of macroradicals formed upon radiolysis of aqueous poly(N-vinylpyrrolidone) (PVP) solutions using pulse radiolysis, density functional theory (DFT) and literature data. On the basis of literature data on site-specific kinetics of hydrogen abstraction from simple amides and spectra corresponding to specific radical sites on the same amides we have assessed the distribution of H-atom abstraction by `OH radicals from different positions on the pyrrolidone ring and the polymer backbone. Pulse radiolysis experiments performed at different doses per pulse and different PVP concentrations demonstrate that the H-abstracting radiolysis products are not quanti…

PULSE-RADIOLYSISMaterials sciencePulse radiolysisCROSS-LINKINGNanogelsMICROGELSPOLY(ACRYLIC ACID) NANOGELSHYDROXYL RADICALSPhotochemistry01 natural sciences030218 nuclear medicine & medical imaging03 medical and health scienceschemistry.chemical_compoundDELIVERYNanogel0302 clinical medicine0103 physical sciencesMacroradicalRadiationAqueous solution010308 nuclear & particles physicsN-VinylpyrrolidonePulse (physics)ELECTRONSNETWORKSchemistryRadiolysispoly(N-vinyl pyrrolidone)Density functional theoryDensity functional theoryMacroradicalsSettore CHIM/07 - Fondamenti Chimici Delle TecnologiePOLYMERSRADIATION-INDUCED SYNTHESIS
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Oligonucleotide-decorated carboxyl-modified PVP nanogels: a new platform for diagnosis and gene-therapy.

2012

Nanogels, or nanoscalar chemically crosslinked polymer networks, were generated by simultaneous crosslinking of Poly(N-vinyl pyrrolidone) (PVP) and grafting of acrylic acid (AA) monomer through e-beam irradiation of their aqueous solutions. The yield of the process is very high and no separation or complex purification procedures are required since no recourse to surfactants or organic solvents is made. The administered irradiation dose (40 kGy) imparts also sterility to the obtained nanogels in the form of aqueous dispersions. Control of particle size and size-distribution can be achieved by proper selection of the irradiation conditions. In particular, we obtained nanogel variants with av…

PVP nanogels OligonucleotideSettore CHIM/07 - Fondamenti Chimici Delle Tecnologie
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Multi-Functional Nanogels for Tumor Targeting and Redox-Sensitive Drug and siRNA Delivery

2016

(1) Background: A new family of nanosystems able to discern between normal and tumor cells and to release a therapeutic agent in controlled way were synthetized by e-beam irradiation. This technique permits to obtain biocompatible, sterile, carboxyl-functionalized polyvinylpyrrolidone (PVP-co-acrylic acid) nanogels (NGs); (2) Methods: Here, we performed a targeting strategy based on the recognition of over-expressed proteins on tumor cells, like the folate receptor. The selective targeting was demonstrated by co-culture studies and flow cytometry analysis, using folate conjugated NGs. Moreover, nanoparticles were conjugated to a chemotherapeutic drug or to a pro-apoptotic siRNA through a gl…

PVPPharmaceutical ScienceNanogels02 engineering and technologyPharmacology01 natural sciencesAntioxidantsAnalytical Chemistryfolate-targetingPolyethylene GlycolsNanogelchemistry.chemical_compoundMiceRNA interferenceNeoplasmsDrug DiscoveryFluorescence microscopePolyethyleneimineRNA Small InterferingCytotoxicitymedicine.diagnostic_testPovidone021001 nanoscience & nanotechnologyControlled releaseCell biologyChemistry (miscellaneous)Folate receptorMolecular Medicinee-beamGSH-responsive release0210 nano-technologyOxidation-Reduction010402 general chemistrydoxorubicinArticleFlow cytometryFolic AcidCell Line TumormedicineAnimalsHumansPhysical and Theoretical ChemistryParticle SizeOrganic ChemistryGlutathione0104 chemical scienceschemistryPVP; nanogels; e-beam; folate-targeting; doxorubicin; siRNA; GSH-responsive releasesiRNACancer cellNIH 3T3 CellsNanoparticlesSettore CHIM/07 - Fondamenti Chimici Delle TecnologieFolic Acid TransportersHeLa CellsMolecules
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E-Beam Crosslinked Polymeric and Bio-Hybrid Nanocarriers for Drug Delivery and Bioimaging

2014

PVPnanogeldrug deliverybioimaging.Settore CHIM/07 - Fondamenti Chimici Delle Tecnologie
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