Search results for "Nitrile"

showing 10 items of 1539 documents

Synthesis of Isoxazole and 1,2,3-Triazole Isoindole Derivatives via Silver- and Copper-Catalyzed 1,3-Dipolar Cycloaddition Reaction.

2016

International audience; The CuI-or Ag 2 CO 3-catalyzed [3+2] cycloaddition of propargyl-substituted dihydroisoindolin-1-one (3) with arylnitrile oxides 1a-d (Ar = Ph, p-MeC 6 H 4 , p-MeOC 6 H 4 , p-ClC 6 H 4) produces in good yields novel 3,5-disubstituted isoxazoles 4 of the ethyl-2-benzyl-3-oxo-1-((3-arylisoxazol-5yl)methyl)-2,3-dihydro-1H-isoindole-1-carboxylate type. With aryl azides 2a-d (Ar = Ph, p-MeC 6 H 4 , p-OMeC 6 H 4 , p-ClC 6 H 4), a series of 1,4-disubstituted 1,2,3-triazoles 6 (ethyl-2-benzyl-3-oxo-1-((1-aryl-1H-1,2,3-triazol-4-yl)methyl)-2,3-dihydro-1H-isoindole-1-carboxylates) was obtained. The reactions proceed in a regioselective manner affording exclusively racemic adduc…

123-TriazoleMagnetic Resonance SpectroscopySilverSpectrophotometry Infrared12Pharmaceutical Science[3+2] dipolar cycloaddition; arylnitrile oxides; arylazides; isoxazole; 123-triazolesarylazidesIsoindoles010402 general chemistryCrystallography X-Ray01 natural sciencesMedicinal chemistryCatalysisArticleAnalytical Chemistrylcsh:QD241-441chemistry.chemical_compoundlcsh:Organic chemistryDrug DiscoveryOrganic chemistryPhysical and Theoretical ChemistryIsoxazoleCycloaddition Reaction010405 organic chemistryArylOrganic ChemistryisoxazoleRegioselectivityIsoxazolesarylnitrile oxidesTriazolesCycloaddition0104 chemical scienceschemistryChemistry (miscellaneous)13-Dipolar cycloaddition[3+2] dipolar cycloadditionMolecular Medicine123-triazoles3-triazolesIsoindoleSelectivity[PHYS.ASTR]Physics [physics]/Astrophysics [astro-ph]CopperMolecules (Basel, Switzerland)
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CCDC 241844: Experimental Crystal Structure Determination

2005

Related Article: J.Pinkas, J.Kubista, R.Gyepes, J.Cejka, P.Meunier, K.Mach|2005|J.Organomet.Chem.|690|731|doi:10.1016/j.jorganchem.2004.09.081

1-Isopropyl-456-trimethyl-7-(trimethylsilyl)bicyclo(2.2.1)hept-5-ene-2233-tetracarbonitrileSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 741667: Experimental Crystal Structure Determination

2009

Related Article: J.Zhao, V.Bohmer, M.Bolte|2009|Acta Crystallogr.,Sect.E:Struct.Rep.Online|65|o1658|doi:10.1107/S1600536809023344

22'-Dimethyl-22'-(m-phenylenedimethylene)propanedinitrileSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1421617: Experimental Crystal Structure Determination

2016

Related Article: Jakob Wudarczyk, George Papamokos, Vasilis Margaritis, Dieter Schollmeyer, Felix Hinkel, Martin Baumgarten, George Floudas, Klaus Müllen|2016|Angew.Chem.,Int.Ed.|55|3220|doi:10.1002/anie.201508249

22-Dimethyl-23-dihydro-1H-benzimidazole-4567-tetracarbonitrile tetrahydrofuran solvateSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1042088: Experimental Crystal Structure Determination

2015

Related Article: Kaisa Helttunen, Tiia-Riikka Tero, Maija Nissinen|2015|CrystEngComm|17|3667|doi:10.1039/C5CE00311C

2202632-tetramethoxy-24303639-tetramethyl-58111417-pentaoxahexacyclo[19.15.3.12529.13135.0438.01823]hentetraconta-1318202225(41)262831(40)323437-dodecaene-2834-diol acetonitrile solvateSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 718575: Experimental Crystal Structure Determination

2010

Related Article: K.Salorinne, M.Nissinen|2009|CrystEngComm|11|1572|doi:10.1039/b902718a

281420-Tetraethyl-4101622-tetrahydroxy-6121824-tetramethoxycalix(4)arene acetonitrile solvateSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1507211: Experimental Crystal Structure Determination

2017

Related Article: D.Ryvlin, O.Dumele, A.Linke, D.Fankhauser, W.B.Schweizer, F.Diederich, S.R.Waldvogel|2017|ChemPlusChem|82|493|doi:10.1002/cplu.201700077

281420-tetra-n-hexyl-5101520-tetrakis(35-bis(iodo)phenyl)-424:610:1216:1822-OO'- tetraethylenecalix[4]resorcinarene acetonitrile dichloromethane solvateSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 886448: Experimental Crystal Structure Determination

2012

Related Article: T.-R.Tero, K.Salorinne, M.Nissinen|2012|CrystEngComm|14|7360|doi:10.1039/c2ce25972a

281420-tetraethyl-4101622-tetrakis((4-bromobenzyl)oxy)-6121824-tetramethoxycalix[4]arene acetonitrile solvateSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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Mpro-SARS-CoV-2 Inhibitors and Various Chemical Reactivity of 1-Bromo- and 1-Chloro-4-vinylbenzene in [3 + 2] Cycloaddition Reactions

2021

The regioselectvity and the mechanism of the (32CA) cycloadditions reactions of 1-bromo-4-vinylbenzene 1 and 1-chloro-4-vinylbenzene 2 with benzonitrile oxide 3 were investigated under the molecular electron density theory (MEDT) at the B3LYP/6-311++G(d,p) computational level. Evaluation of the ELF reveals that these zwitterionic type (zw-type) 32CA reactions take place in a two-stage one-step mechanism. This MEDT study shows that the meta isoxazolines are kinetically and thermodynamically favored over the ortho ones, these 32CA reactions being completely regioselective, in agreement with experimental outcomes. In addition, the efficiency of isoxazolines against SARS-CoV-2 have been also in…

2019-20 coronavirus outbreakCoronavirus disease 2019 (COVID-19)010405 organic chemistryChemistrySARS-CoV-2Severe acute respiratory syndrome coronavirus 2 (SARS-CoV-2)OxideMEDTRegioselectivity010402 general chemistry01 natural sciencesMedicinal chemistryDFTCycloaddition3. Good health0104 chemical scienceschemistry.chemical_compoundBenzonitrileELFDocking (molecular)regioselectivity2-isoxazolineOrganics
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COVID-19 in Philadelphia-negative myeloproliferative disorders: a GIMEMA survey

2020

2019-20 coronavirus outbreakPediatricsmedicine.medical_specialtyCancer ResearchCoronavirus disease 2019 (COVID-19)EpidemiologySevere acute respiratory syndrome coronavirus 2 (SARS-CoV-2)Pneumonia ViralPhiladelphia chromosomeSeverity of Illness IndexMyeloproliferative diseaseBetacoronavirusMyeloproliferative DisordersLeukemia Myelogenous Chronic BCR-ABL PositiveCorrespondenceNitrilesmedicineHumansPhiladelphia ChromosomeBetacoronavirus COVID-19 Coronavirus Infections Cross-Sectional Studies Disease Progression Humans Italy Leukemia Myelogenous Chronic BCR-ABL Positive Philadelphia Chromosome Pneumonia Viral Pyrazoles SARS-CoV-2 Severity of Illness Index Survival Analysis PandemicsPandemicsPhiladelphia negativebusiness.industrySARS-CoV-2Disease progressionCOVID-19Hematologymedicine.diseaseSurvival AnalysisCross-Sectional StudiesPyrimidinesItalyOncologyDisease ProgressionPyrazolesbusinessCoronavirus InfectionsCoronavirus InfectionsLeukemia
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