Search results for "OXY"

showing 10 items of 11443 documents

Heart rate recovery after exercise and maximal oxygen uptake in sedentary patients with type 2 diabetes

2015

Aims: Heart rate recovery after exercise (HRR) is an estimate of autonomic modulation of the heart, and has been shown to be inversely associated with insulin resistance, metabolic syndrome, and type 2 diabetes [1]. Type 2 diabetes is associated with poor exercise tolerance and maximal aerobic capacity (VO2max) [2]. Aim of our study was to assess the relationship between HRR and VO2max in sedentary patients with type 2 diabetes. Methods: Maximal treadmill exercise testing using standard or modified Bruce protocol was performed in 16 (8 males and 8 females) sedentary patients with type 2 diabetes (T2D), and in 16 (9 males and 7 females) age-matched sedentary non-diabetic controls (ND). HRR (…

metabolism fat oxidation rate oxygen uptake exercise diabetes.Settore M-EDF/01 - Metodi E Didattiche Delle Attivita' MotorieHeart rate recovery Maximal oxygen uptake Type 2 diabetes
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Decomposition Process of Carboxylate MOF HKUST-1 Unveiled at the Atomic Scale Level

2016

HKUST-1 is a metal-organic framework (MOF) which plays a significant role both in applicative and basic fields of research, thanks to its outstanding properties of adsorption and catalysis but also because it is a reference material for the study of many general properties of MOFs. Its metallic group comprises a pair of Cu2+ ions chelated by four carboxylate bridges, forming a structure known as paddle-wheel unit, which is the heart of the material. However, previous studies have well established that the paddle-wheel is incline to hydrolysis. In fact, the prolonged exposure of the material to moisture promotes the hydrolysis of Cu-O bonds in the paddle-wheels, so breaking the crystalline n…

metal-organic-frameworks MOF electron paramagnetic resonance EPR ESR water structural stabilityInorganic chemistryFOS: Physical sciences02 engineering and technology010402 general chemistry01 natural sciencesAtomic unitslaw.inventionCatalysisMetalCrystalchemistry.chemical_compoundAdsorptionlawPhysics - Chemical PhysicsCarboxylatePhysical and Theoretical ChemistryElectron paramagnetic resonanceChemical Physics (physics.chem-ph)Condensed Matter - Materials ScienceChemistryMaterials Science (cond-mat.mtrl-sci)021001 nanoscience & nanotechnology0104 chemical sciencesSurfaces Coatings and FilmsElectronic Optical and Magnetic MaterialsGeneral EnergyChemical engineeringvisual_artvisual_art.visual_art_mediumMetal-organic framework0210 nano-technologyThe Journal of Physical Chemistry C
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Scanning Tunneling Spectroscope Use in Electrocatalysis Testing

2010

Published version of an article from the journal: Materials (1996-1944). Also available from publisher: http://dx.doi.org/10.3390/ma3063675 The relationship between the electrocatalytic properties of an electrode and its ability to transfer electrons between the electrode and a metallic tip in a scanning tunneling microscope (STM) is investigated. The alkaline oxygen evolution reaction (OER) was used as a test reaction with four different metallic glasses, Ni78Si8B14, Ni70Mo20Si5B5, Ni58Co20Si10B12, and Ni25Co50Si15B10, as electrodes. The electrocatalytic properties of the electrodes were determined. The electrode surfaces were then investigated with an STM. A clear relationship between the…

metallic glasses of Ni alloysAnalytical chemistryElectrochemistryElectrocatalystlcsh:TechnologyArticleCatalysislaw.inventionlawscanning tunneling microscopeGeneral Materials Sciencelcsh:MicroscopyQuantum tunnellinglcsh:QC120-168.85lcsh:QH201-278.5Chemistrylcsh:TVDP::Technology: 500::Chemical engineering: 560Oxygen evolutionElectrochemical scanning tunneling microscopeChemical engineeringoxygen evolution reactionlcsh:TA1-2040Electrodelcsh:Descriptive and experimental mechanicslcsh:Electrical engineering. Electronics. Nuclear engineeringScanning tunneling microscopelcsh:Engineering (General). Civil engineering (General)scanning tunneling microscope; oxygen evolution reaction; metallic glasses of Ni alloyslcsh:TK1-9971
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From 1D coordination polymers to Metal Organic Frameworks by the use of 2-pyridyl oximes.

2020

The synthesis and characterization of coordination polymers and metal&ndash

metal–organic frameworks (MOFs)MagnetismPolymersdetectioncarboxylatesmixed-ligand02 engineering and technology010402 general chemistry01 natural scienceslcsh:TechnologyArticleMetalchemistry.chemical_compoundPolymer chemistryGeneral Materials Sciencelcsh:Microscopylcsh:QC120-168.85chemistry.chemical_classificationMagnetismeFerric oxidelcsh:QH201-278.5Ligandlcsh:TMagnetismPolymer021001 nanoscience & nanotechnologyOximeMagnetic susceptibility0104 chemical sciencesPolímerscoordination polymerschemistrylcsh:TA1-2040magnetismvisual_artvisual_art.visual_art_mediumencapsulationMetal-organic frameworklcsh:Descriptive and experimental mechanicslcsh:Electrical engineering. Electronics. Nuclear engineeringÒxid de ferropyridyl oximes0210 nano-technologySelectivitylcsh:Engineering (General). Civil engineering (General)lcsh:TK1-9971iron(III)
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Amplicon-based high-throughput pooled sequencing identifies mutations in CYP7B1 and SPG7 in sporadic spastic paraplegia patients

2011

Hereditary spastic paraplegia (HSP) is a neurodegenerative disorder defined clinically by progressive lower limb spasticity and weakness. HSP is a genetically highly heterogeneous condition with at least 46 gene loci identified so far, involving X-linked, autosomal recessive (AR) and autosomal dominant inheritance. For correct diagnosis, molecular testing is essential because clinical parameters by themselves are not reliable to differentiate HSP forms. The purpose of this study was to establish amplicon-based high-throughput genotyping for AR-HSP. A sample of 187 index cases with apparently sporadic or recessive spastic paraplegia were analyzed by applying an array-based amplification stra…

methods [High-Throughput Nucleotide Sequencing]GenotypeHereditary spastic paraplegiaDNA Mutational AnalysisMolecular Sequence DataSPG7 protein humanCytochrome P450 Family 7diagnosis [Paraplegia]Biologymedicine.disease_causegenetics [Paraplegia]Cohort Studiesgenetics [Metalloendopeptidases]03 medical and health sciences0302 clinical medicineGenetic variationGenotypeGeneticsmedicineHumansddc:610Genetic TestingGenotypingGenetics (clinical)CYP7B1 protein human030304 developmental biologyGenetic testingParaplegiaGenetics0303 health sciencesMutationBase SequenceParapleginmedicine.diagnostic_testgenetics [Steroid Hydroxylases]Genetic VariationHigh-Throughput Nucleotide SequencingMetalloendopeptidasesmethods [DNA Mutational Analysis]Ampliconmedicine.diseasegenetics [Genetic Variation]3. Good healthMutationSteroid HydroxylasesATPases Associated with Diverse Cellular Activities030217 neurology & neurosurgeryClinical Genetics
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CCDC 2149627: Experimental Crystal Structure Determination

2022

Related Article: Adrian Laviós, Amparo Sanz-Marco, Carlos Vila, M. Carmen Muñoz, José R. Pedro, Gonzalo Blay|2022|Org.Lett.|24|2149|doi:10.1021/acs.orglett.2c00427

methyl (1R3S3aR8bR)-7-bromo-3-methoxy-3a-nitro-1-phenyl-233a8b-tetrahydro-1H-[1]benzofuro[23-c]pyrrole-1-carboxylateSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 985005: Experimental Crystal Structure Determination

2014

Related Article: Frank Bohland, Irina Erlin, Lukas Platte, Maike Schröder, Dieter Schollmeyer, Udo Nubbemeyer|2014|Eur.J.Org.Chem.|2014|6272|doi:10.1002/ejoc.201402720

methyl 1-benzyl-8-((t-butyl(dimethyl)silyl)oxy)-3-chloro-2-oxo-234789-hexahydro-1H-azonine-4-carboxylateSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1880603: Experimental Crystal Structure Determination

2018

Related Article: M.M. Abdou, M. Matziari, P.M. O'Neill, E. Amigues, R. Zhou, R. Wang, B.F. Ali|2018|IUCrData|3|x181662|doi:10.1107/S2414314618016620

methyl 3-(2-hydroxyphenyl)propanoateSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 993834: Experimental Crystal Structure Determination

2014

Related Article: Inguna Goba, Baiba Turovska, Sergey Belyakov, Edvards Liepinsh|2014|J.Mol.Struct.|1074|549|doi:10.1016/j.molstruc.2014.06.044

methyl 5-acetyl-26-dimethyl-4-phenyl-14-dihydropyridine-3-carboxylateSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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Synthesis and characterization of ferrocene-based Schiff base and ferrocenecarboxaldehyde oxime and their adsorptive removal of methyl blue from aque…

2018

Abstract The ferrocene-based Schiff base 3 was synthetized by reaction of ferrocenecarboxaldehyde 1 with 4-aminoantipyrine 2. However, the reaction of 1 with hydroxylamine affords ferrocenecarboxaldehyde oxime 4. Compounds 3 and 4 were fully characterized by IR, 1H, 13C and DEPT-135 NMR spectroscopy, elemental analyses and also by single crystal X-ray diffraction. Compounds 3 and 4 were used to remove anionic methyl blue dye from wastewater. The results established that both compounds have high adsorption capacity towards methyl blue. Langmuir adsorption capacity of compound 4 (464 mmol/g) is much higher than that of compound 3 (193 mmol/g) at 25 °C. The kinetics data was fitted well pseudo…

methyl blue dyeLangmuirMethyl blue02 engineering and technology010402 general chemistry01 natural sciencesBiochemistryInorganic Chemistrychemistry.chemical_compoundAdsorptionHydroxylamineMaterials ChemistryPhysical and Theoretical Chemistryferrocenecarboxaldehyde oximeta116single crystal X-ray diffractionAqueous solutionSchiff baseOrganic Chemistry021001 nanoscience & nanotechnologyOximeferrocene-based Schiff base0104 chemical sciencesFerrocenechemistryadsorption0210 nano-technologyNuclear chemistryJournal of Organometallic Chemistry
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