Search results for "PreP"
showing 10 items of 1334 documents
Searching the most appropriate sample pretreatment for the elemental analysis of wines by inductively coupled plasma-based techniques.
2008
Different sample preparation methods were evaluated for the simultaneous multielement analysis of wine samples by inductively coupled plasma optical emission spectrometry (ICP-OES) and inductively coupled plasma mass spectrometry (ICP-MS). Microwave-assisted digestion in closed vessel, thermal digestion in open reactor, and direct sample dilution were considered for the determination of Li, Be, Na, Mg, Al, K, Ca, Sc, Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Zn, As, Se, Sr, Y, Mo, Cd, Ba, La, Ce, Pr, Nd, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu, Tl, Pb, and Bi in 12 samples of red wine from Valencia and Utiel-Requena protected designation of origin. ICP-MS allows the determination of 17 elements in most…
A Promising New Method to Estimate Drug-Polymer Solubility at Room Temperature
2016
The established methods to predict drug-polymer solubility at room temperature either rely on extrapolation over a long temperature range or are limited by the availability of a liquid analogue of the polymer. To overcome these issues, this work investigated a new methodology where the drug-polymer solubility is estimated from the solubility of the drug in a solution of the polymer at room temperature using the shake-flask method. Thus, the new polymer in solution method does not rely on temperature extrapolations and only requires the polymer and a solvent, in which the polymer is soluble, that does not affect the molecular structure of the drug and polymer relative to that in the solid st…
Mammalian cell metabolomics: Experimental design and sample preparation
2013
Metabolomics represents the global assessment of metabolites in a biological sample and reports the closest information to the phenotype of the biological system under study. Mammalian cell metabolomics has emerged as a promising tool with potential applications in many biotechnology and research areas. Metabolomics workflow includes experimental design, sampling, sample processing, metabolite analysis, and data processing. Given their influence on metabolite content and biological interpretation of data, a good experimental design and the appropriate choice of a sample processing method are prerequisites for success in any metabolomic study. The use of mammalian cells in the metabolomics f…
Reclaimed asphalt test specimen preparation assisted by image analysis
2015
This paper presents a laboratory investigation aimed at establishing a protocol for the production of homogeneous asphalt mixtures test specimens, incorporating reclaimed asphalt by using a gyratory compactor with coring and trimming works. Stone mastic asphalt specimens were compacted at the previously identified target densities with the final aim of obtaining specimens with a fixed and homogeneous air void distribution. A microstructural study was conducted to characterize the homogeneity in the air void distribution using X-ray computed tomography (CT) combined with image analysis techniques. The study concluded that the gyratory compactor is suitable for producing homogeneous test spec…
The effect of hyperthyroidisation on the plumage of carnivorous birds
1931
Izvilkums no: Acta Zoologica, Stockholms högskola, Bd.11, 1930.
Zāļu gatavošana aptiekā
2016
Zāļu gatavošana aptiekās sastapās ar problēmām jau 20. gadsimta 20. un 30. gados, jo rūpnieciski gatavotās zāles lielā daudzumā nāca no ārzemēm un aptieku gatavotajām zālēm bija grūti ar to konkurēt. Šobrīd aptiekās zāles tiek gatavotas arvien mazāk. Gadu gaitā daudzi aptiekā gatavotie preparāti ir kļuvuši komerciāli pieejami. Piemēram fentanila sūkājamās tabletes, 4-Aminopiridīna kapsulas (fampridine), nistatīna sūkājamās tabletes, tetrakaīna-adrenalīns-kokaīna šķīdums. Bakalaura darba mērķis: izvētrēt Līvānu centra aptiekā gatavoto zāļu apriti no 2015. gada janvāra līdz 2015. gada decembrim. Izmantojot aptiekā pieejamās ekstemporālās receptes, apkopotas un izanalizētas 399 receptes. Secin…
Palladium coupling catalysts for pharmaceutical applications
2007
International audience; This review discusses recent advances made in the area of palladium-catalyzed coupling reactions and describes a selection of the catalytic systems that are useful in the preparation of valuable compounds for the pharmaceutical industry. Most of these types of syntheses have used either simple palladium salts or palladium precursors associated with electron-rich mono- or bidentate phosphine ligands as catalysts. For some reactions, ligands such as triphenyl phosphine, 1,1'-bis(diphenylphosphino)ferrocene, a carbene or a bipyridine have also been employed. Several new procedures for the Suzuki cross-coupling reaction, the activation of aryl chlorides, the functionaliz…
Preprocessing of region of interest localization based on local surface curvature analysis for three-dimensional reconstruction with multiresolution
2009
We present an approach to integrate a preprocessing step of the region of interest ROI localization into 3-D scanners laser or ste- reoscopic. The definite objective is to make the 3-D scanner intelligent enough to localize rapidly in the scene, during the preprocessing phase, the regions with high surface curvature, so that precise scanning will be done only in these regions instead of in the whole scene. In this way, the scanning time can be largely reduced, and the results contain only per- tinent data. To test its feasibility and efficiency, we simulated the prepro- cessing process under an active stereoscopic system composed of two cameras and a video projector. The ROI localization is…
Manufacturing and characterization of single cell intermediate-temperature solid oxide fuel cells for APU in transportation application
2014
The fabrications of large area IT-SOFC planar cell by new simple and cost effective process were explained. The optimization of the new process with respect to pore formers, thickness of layers, sintering temperature were performed. The electrochemical results of 10cm2 performed in Fiaxell open flange set up were detailed with respect to different configuration. Long term ageing performance tests of single cells were conducted in Fiaxell device and results are discussed. Preparation of new test bench and stacking process performed till now were briefed.
LDR Image to HDR Image Mapping with Overexposure Preprocessing
2013
International audience; Due to the growing popularity of High Dynamic Range (HDR) images and HDR displays, a large amount of existing Low Dynamic Range (LDR) images are required to be converted to HDR format to benefit HDR advantages, which give rise to some LDR to HDR algorithms. Most of these algorithms especially tackle overexposed areas during expanding, which is the potential to make the image quality worse than that before processing and introduces artifacts. To dispel these problems, we . present a new,LDR to HDR approach, unlike the existing techniques, it focuses on avoiding sophisticated treatment to overexposed areas in dynamic range expansion step. Based on a separating principl…