Search results for "Rotaxane"

showing 10 items of 41 documents

Directional Shuttling of a Stimuli-Responsive Cone-Like Macrocycle on a Single-State Symmetric Dumbbell Axle

2018

Rotaxane-based molecular shuttles are often operated using low-symmetry axles and changing the states of the binding stations. A molecular shuttle capable of directional shuttling of an acid-responsive cone-like macrocycle on a single-state symmetric dumbbell axle is now presented. The axle contains three binding stations: one symmetric di(quaternary ammonium) station and two nonsymmetric phenyl triazole stations arranged in opposite orientations. Upon addition of an acid, the protonated macrocycle shuttles from the di(quaternary ammonium) station to the phenyl triazole binding station closer to its butyl groups. This directional shuttling presumably originates from charge repulsion and an …

RotaxaneeducationTriazoleProtonation010402 general chemistry01 natural sciencessupramolecular chemistryCatalysischemistry.chemical_compoundbutyl groupssupramolekulaarinen kemiahost-guest chemistryrotaxanemoleculesta116Physicsmolecular machine010405 organic chemistrymolekyylitGeneral MedicineGeneral ChemistryMolecular machine0104 chemical sciencesMechanism (engineering)CrystallographyAxleMolecular shuttlechemistryDumbbellmacrocycleAngewandte Chemie International Edition
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Photoinduced Electron Transfer in Multiporphyrinic Interlocked Structures: The Effect of Copper(I) Coordination in the Central Site

2004

Photoinduced processes have been determined in a [2]catenane containing a zinc(II) porphyrin, a gold(III) porphyrin, and two free phenanthroline binding sites, Zn-Au(+), and in the corresponding copper(I) phenanthroline complex, Zn-Cu(+)-Au(+). In acetonitrile solution Zn-Au(+) is present in two different conformations: an extended one, L, which accounts for 40 % of the total, and a compact one, S. In the L conformation, the electron transfer from the excited state of the Zn porphyrin to the gold-porphyrin unit (k = 1.3x10(9) s(-1)) is followed by a slow recombination (k = 8.3x10(7) s(-1)) to the ground state. The processes in the S conformation cannot be clearly resolved but a charge-separ…

RotaxanesMetalloporphyrinsPhotochemistryPhenanthrolineCatenaneMolecular Conformationchemistry.chemical_elementElectronsPhotochemistryCatalysisPhotoinduced electron transferElectron Transportchemistry.chemical_compoundElectron transferChemistryOrganic ChemistryGeneral ChemistryPorphyrinCopperZincCrystallographyEnergy TransferSpectrophotometryExcited stateGoldGround stateCopperChemistry - A European Journal
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CCDC 781080: Experimental Crystal Structure Determination

2011

Related Article: J.-P.Collin, S.Durot, M.Keller, J.-S.Sauvage, Y.Trolez, M.Cetina, K.Rissanen|2011|Chem.-Eur.J.|17|947|doi:10.1002/chem.201002220

Space GroupCrystallography(3)-((mu2-38-bis(5-(2-(Trimethylsilyl)ethynyl)-2-pyridyl)-47-phenanthroline)-bis(29-(116-bis(41-phenylene)-147101316-hexaoxahexadecane)-110-phenanthroline)-di-zinc(ii)) pseudorotaxane tetrakis(trifluoromethanesulfonate) acetone solvate monohydrateCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 706838: Experimental Crystal Structure Determination

2009

Related Article: J.Frey, C.Tock, J.-P.Collins, V.Heitz, J.-P.Sauvage, K.Rissanen|2008|J.Am.Chem.Soc.|130|11013|doi:10.1021/ja801924y

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameters(4)-bis(mu~2~-38-bis(5-(4-Methoxyphenyl)-2-pyridyl)-47-phenanthroline-NN'N''N''') bis(mu~2~-161922252831515457606366-dodecaoxa-61037417174-hexa-azatridecacyclo-[44.24.4.2$811~2~1215~2~4750~2~6770!1^3236^1^3539^0^472^0^542^-0^740^0^938^0^4373^]-tetraoctaconta-1(71)24(72)5(42)6810121432(80)-3335(79)36384043(73)4446(74)4749676975778183-hexacosaene)-tetra-copper(i)-pseudorotaxane tetrakis(hexafluorophosphate) dichlo romethane tetrahydrofuran dichloromethane unspecified solvateExperimental 3D Coordinates
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CCDC 100241: Experimental Crystal Structure Determination

1997

Related Article: P.N.W.Baxter, H.Sleiman, J.-M.Lehn, K.Rissanen|1997|Angew.Chem.,Int.Ed.|36|1294|doi:10.1002/anie.199712941

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameters(mu~3~-(4)-(66'-bis(6-Methylpyridyl)-33'-bipyridazinyl)-tris(29-(44'-(36912-tetra-oxatetradecane-114-dioxy)diphenyl-110-phenanthroline))-pseudorotaxane)-tri-copper tris(hexafluorophosphate) benzene nitromethane solvate monohydrateExperimental 3D Coordinates
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CCDC 1575263: Experimental Crystal Structure Determination

2018

Related Article: Yan-Long Ma, Hua Ke, Arto Valkonen, Kari Rissanen, Wei Jiang|2018|Angew.Chem.,Int.Ed.|57|709|doi:10.1002/anie.201711077

Space GroupCrystallographyCrystal System[2]-(11'-(pentane-15-diyl)bis(14-diazabicyclo[2.2.2]octan-1-ium))-(10163642-tetrabutoxy-132839505456-hexaoxatridecacyclo[43.7.1.1351.12327.12529.027.0611.01520.01924.03237.03355.04146.04953]hexapentaconta-246810151719212329(55)30323436414345(53)4648-icosaene)-rotaxane bis(hexafluorophosphate) acetonitrile solvateCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1826426: Experimental Crystal Structure Determination

2018

Related Article: Jie‐Shun Cui, Qian‐Kai Ba, Hua Ke, Arto Valkonen, Kari Rissanen, Wei Jiang|2018|Angew.Chem.,Int.Ed.|57|7809|doi:10.1002/anie.201803349

Space GroupCrystallography[2]-(N1-((35-di-t-butylphenyl)methyl)-N6-((4-(1-((35-di-t-butylphenyl)methyl)-1H-123-triazol-4-yl)phenyl)methyl)-N1N1N6N6-tetramethylhexane-16-diaminium)-(10163642-tetrabutoxy-28505456-tetraoxa-1339-diazoniatridecacyclo[43.7.1.1351.12327.12529.027.0611.01520.01924.03237.03355.04146.04953]hexapentaconta-246810151719212329(55)30323436414345(53)4648-icosaene)-rotaxane trifluoroacetate tris(hexafluorophosphate) acetone methanol dichloromethane solvate monohydrateCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 733684: Experimental Crystal Structure Determination

2010

Related Article: J.-P.Collin, J.-P.Sauvage, Y.Trolez, K.Rissanen|2009|New J.Chem.|33|2148|doi:10.1039/b9nj00278b

Space GroupCrystallography[3]-((mu~2~-38-bis(5-[(triisopropylsilyl)ethynyl]pyridin-2-yl)-47-phenanthroline)-bis(691215182124-heptaoxa-3841-diazahexacyclo[27.8.4.2^25^.2^2528^.0^3240^.0^3539^]pentatetraconta-1(38)24252729(41)3032(40)3335(39)364244-tridecaene)-di-copper)-pseudorotaxane bis(hexafluorophosphate) acetone solvate hemihydrateCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1575262: Experimental Crystal Structure Determination

2018

Related Article: Yan-Long Ma, Hua Ke, Arto Valkonen, Kari Rissanen, Wei Jiang|2018|Angew.Chem.,Int.Ed.|57|709|doi:10.1002/anie.201711077

Space GroupCrystallography[3]-(11'-(decane-110-diyl)bis(14-diazabicyclo[2.2.2]octan-1-ium))-bis(10163642-tetrabutoxy-132839505456-hexaoxatridecacyclo[43.7.1.1351.12327.12529.027.0611.01520.01924.03237.03355.04146.04953]hexapentaconta-246810151719212329(55)30323436414345(53)4648-icosaene)-rotaxane bis(hexafluorophosphate) 12-dichloroethane acetonitrile solvateCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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Dual-stimuli pseudorotaxane switches under kinetic control

2021

A series of dumbbell-shaped sec-ammonium salts with bulky (pseudo)stoppers (‘speed bumps’) were tested for their ability to form pseudorotaxanes with a redox-switchable, tetrathiafulvalene (TTF)-decorated [24]crown-8 ether. Depending on the size of the pseudostoppers, fast (less than ten minutes), slow (hours to days) and very slow (no pseudorotaxanes observed) threading has been observed. NMR spectroscopy as well as tandem mass spectrometry indicate the formation of non-threaded face-to-face complexes prior to pseudorotaxanes formation. Both isomers can be distinguished by their substantially different stability in collision-induced dissociation (CID) experiments. Two external stimuli affe…

Steric effectsMechanical bond010405 organic chemistryOrganic ChemistryEtherNuclear magnetic resonance spectroscopy547010402 general chemistry01 natural sciencesDissociation (chemistry)pseudostoppers0104 chemical scienceschemistry.chemical_compoundCrystallographyDeprotonationchemistrysec-ammonium salts500 Naturwissenschaften und Mathematik::540 Chemie::547 Organische ChemieMoietyTetrathiafulvalenepseudorotaxanes
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