Search results for "SAGE"

Spectrophotometric determination of nalidixic and pipemidic acids in a flow injection assembly with a solid-phase reactor as a highly stable reagent …

2001

Abstract The flow-injection spectrophotometric determination of nalidixic (I) and pipemidic (II) acids were carried out by reaction with Fe(III) ions entrapped in a polymeric material and filling a packed-bed reactor; the released Fe(III) complexed with the quinolone is monitored at 426 nm. The method worked with a high reproducibility, even when using different reactors, days and solutions. Selectivity of the procedure was tested with different foreign compounds found in human urine as well as in pharmaceutical formulations containing both quinolones; no relevant interferences were observed. The calibration graph for (I) was linear over the range 1–250 μg ml −1 with a relative standard dev…

ORGANIZATION OF HIGHER-LEVEL CHROMATIN STRUCTURES (CHROMOMERE, CHROMONEMA AND CHROMATIN BLOCK) EXAMINED USING VISIBLE LIGHT-INDUCED CHROMATIN PHOTO-S…

2002

The method of chromatin photo-stabilization by the action of visible light in the presence of ethidium bromide was used for investigation of higher-level chromatin structures in isolated nuclei. As a model we used rat hepatocyte nuclei isolated in buffers which stabilized or destabilized nuclear matrix. Several higher-level chromatin structures were visualized: 100 nm globules—chromomeres, chains of chromomeres—chromonemata, aggregates of chromomeres—blocks of condensed chromatin. All these structures were completely destroyed by 2 M NaCl extraction independent of the matrix state, and DNA was extruded from the residual nuclei (nuclear matrices) into a halo. These results show that nuclear …

Usage assignment of the residence in the cases of familiar crises: commentary on the article 6 Valencian Law of familiar relations

2015

En este trabajo se analiza la regulación valenciana respecto a la atribución del uso de la vivienda familiar, tomando en consideración las sentencias dictadas en aplicación del art. 6 de la Ley de relaciones familiares. In this paper we study the Valencian regulation with regard to the assignment of the usage of the familiar residence, taking in consideration the judgments dictated in application of the article 6 law of familiar relations.

Towards Next Generation System Architecture for Emergency Services

2011

European Union has decided that all emergencies can be reported to authorities by European citizens by calling 112 or sending a text message to 112. Distributing warnings and alerts of authorities to citizens currently happens through national TV and radio channels, but telecom networks are also used now in some countries for this purpose. During the last ten years there have been attempts to develop new system architectures for various emergency service provision phases. Some of them are already deployed in special cases, like in ambulance services. Multimedia emergency alert messages can be delivered to citizens over fixed and mobile telecom networks and commercial systems are already in …

SAUCE: A Web-Based Automated Assessment Tool for Teaching Parallel Programming

2015

Many curricula for undergraduate studies in computer science provide a lecture on the fundamentals of parallel programming like multi-threaded computation on shared memory architectures using POSIX threads or OpenMP. The complex structure of parallel programs can be challenging, especially for inexperienced students. Thus, there is a latent need for software supporting the learning process. Subsequent lectures may cover more advanced parallelization techniques such as the Message Passing Interface (MPI) and the Compute Unified Device Architecture (CUDA) languages. Unfortunately, the majority of students cannot easily access MPI clusters or modern hardware accelerators in order to effectivel…

The socio-ecological and personal determinants of school performance and motivation of high school students

2022

For decades, and with the work of Moos (1979) and Walberg (1969), educational research has consistently demonstrated the importance of the personal characteristics of students and the socio-ecological characteristics of the classroom in determining the affective and cognitive development of students.Unfortunately, no research on this subject has been done in France with high school students. This is why we set ourselves the objective of studying the environmental and personal determinants of high school students' academic performance and motivation. Using the L.E.I (Walberg, 1969) and EMMAS (Ntamakiliro et al., 2000) measurement scales, as well as data collection from 405 students enrolled …

Comment favoriser le vivre ensemble à l'école ?

2019

International audience; Comment améliorer le climat scolaire et optimiser ainsi les apprentissages dans les cycles 2 et 3 ? Voici l'éclairage d'une expérimentation mise en place pour une durée de trois ans dans l'école Champgrenon de Charnay-Lès-Mâcon, en Saône-et-Loire.

Furosemide assay in pharmaceuticals by Micellar liquid chromatography: study of the stability of the drug.

2000

A simplified high-performance liquid chromatographic procedure is described for the determination of furosemide (4-chloro-N-furfuryl-5-sulphamoylanthranillic acid), which makes use of UV detection, a C18, reversed-phase column, and micellar mobile phases of sodium dodecyl sulphate (SDS) and 1-propanol at pH 3 buffered with phosphate system. The most adequate experimental conditions to handle furosemide solutions in the analytical laboratory are studied. The mixture of furosemide and its degradation products which are formed upon light exposition was resolved with a mobile phase of 0.04 M SDS-2% propanol. Separation of furosemide from its common impurities and the hydrolytic product, 4-chlor…

Rencontres du Clos-Vougeot 2009. Patrimoines et paysans viticoles

2010

Bayesian versus data driven model selection for microarray data

2014

Clustering is one of the most well known activities in scientific investigation and the object of research in many disciplines, ranging from Statistics to Computer Science. In this beautiful area, one of the most difficult challenges is a particular instance of the model selection problem, i.e., the identification of the correct number of clusters in a dataset. In what follows, for ease of reference, we refer to that instance still as model selection. It is an important part of any statistical analysis. The techniques used for solving it are mainly either Bayesian or data-driven, and are both based on internal knowledge. That is, they use information obtained by processing the input data. A…