Search results for "Scanning"

Experiences from a wearable-mobile acquisition system for ambulatory assessment of diet and activity

2017

Public health trends are currently monitored and diagnosed based on large studies that often rely on pen-and-paper data methods that tend to require a large collection campaign. With the pervasiveness of smart-phones and -watches throughout the general population, we argue in this paper that such devices and their built-in sensors can be used to capture such data more accurately with less of an effort. We present a system that targets a pan-European and harmonised architecture, using smartphones and wrist-worn activity loggers to enable the collection of data to estimate sedentary behavior and physical activity, plus the consumption of sugar-sweetened beverages. We report on a unified pilot…

2015

AbstractWhile understanding the properties of materials under stress is fundamentally important, designing experiments to probe the effects of large tensile stress is difficult. Here tensile stress is created in thin films of potassium (up to 4 atomic layers) by epitaxial growth on a rigid support, graphite. We find that this “simple” metal shows a long-range, periodic “herringbone” reconstruction, observed in 2- and 3- (but not 1- and 4-) layer films by low-temperature scanning tunneling microscopy (STM). Such a pattern has never been observed in a simple metal. Density functional theory (DFT)simulations indicate that the reconstruction consists of self-aligned stripes of enhanced atom den…

On the synonymization of Acaulon longifolium Herrnst. & Heyn with Acaulon fontiquerianum Casas & Sérgio (Pottiaceae)

2021

During bryological work conducted in the Sharon plane region (Israel), a colony of Acaulon Müll. Hal. was discovered. The plants showed morphological affinities both to A. longifolium Herrnst. & Heyn and A. fontiquerianum Casas & Sérgio depending on the floras used for their identification which challenged their recognition as separate species. In order to solve this taxonomic dilemma, we conducted a detailed morphological characterization of the two species based on representative samples. The micromorphological study of vegetative, sporophytic and spore traits revealed the large overlap of range values between both species. Both species showed the characteristic combination of morphologic…

A positional scanning combinatorial library of peptoids as a source of biological active molecules: identification of antimicrobials

2003

9 pages, 4 figures, 2 schemes, 3 tables.-- PMID: 12959560 [PubMed].-- Printed version published in issue Sep-Oct 2003.-- Supporting information available at: http://pubs.acs.org/doi/suppl/10.1021/cc020075u

Mg2-xTixNi (x=0, 0.5) alloys prepared by mechanical alloying for electrochemical hydrogen storage: Experiments and first-principles calculations

2012

International audience; Mg2-xTixNi (x = 0, 0.5) electrode alloys have been prepared by mechanical alloying (MA) under argon atmosphere at room temperature using a planetary high-energy ball mill. The microstructures of synthesized alloys are characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The effects of substitutional doping of Ti in Mg2Ni phase have been investigated by first-principles density functional theory calculations. XRD analysis results indicate that Ti substitution for Mg in Mg2Ni-type alloys results in the formation of TiNi (Pm-3m) and TiNi3 intermetallics. With the increase of milling time, the TiNi phase…

Structural and Thermal Properties of Ethylene-Norbornene Copolymers Obtained Using Vanadium Homogeneous and SIL Catalysts

2020

The series of ethylene-norbornene (E-NB) copolymers was obtained using different vanadium homogeneous and supported ionic liquid (SIL) catalyst systems. The 13C and 1H NMR (carbon and proton nuclear magnetic resonance spectroscopy) together with differential scanning calorimetry (DSC) were applied to determine the composition of copolymers such as comonomer incorporation (CNB), monomer dispersity (MD), monomer reactivity ratio (re), sequence length of ethylene (le) and tetrad microblock distributions. The relation between the type of catalyst, reaction conditions and on the other hand, the copolymer microstructure, chain termination reaction analyzed by the type of unsaturation are discusse…

Unraveling the packing pattern leading to gelation using SS NMR and X-ray diffraction: direct observation of the evolution of self-assembled fibers

2010

A detailed understanding of the mode of packing patterns that leads to the gelation of low molecular mass gelators derived from bile acid esters was carried out using solid state NMR along with complementary techniques such as powder X-ray diffraction (PXRD), differential scanning calorimetry (DSC), thermogravimetric analysis (TGA) and polarizing optical microscopy (POM). Solid state 13C{1H} cross polarization (CP) magic angle spinning (MAS) NMR of the low molecular mass gel in its native state was recorded for the first time. A close resemblance in the packing patterns of the gel, xerogel and bulk solid states was revealed upon comparing their 13C{1H}CPMAS NMR spectral pattern. A doublet r…

Formation and Evolution of Nanoscale Metal Structures on ITO Surface by Nanosecond Laser Irradiations of Thin Au and Ag Films

2012

The effect of nanosecond laser irradiations on 5 nm thick sputter-deposited Au and Ag films on Indium-Tin-Oxide surface is investigated by atomic force microscopy (AFM) and scanning electron microscopy (SEM). After 500, 750, and 1000 mJ/cm 2 fluence irradiations, the breakup of the Au and Ag films into nanoscale islands is observed as a consequence of fast melting and solidification processes. The mean nanoparticles size and surface density are quantified, as a function of the laser fluence, by the AFM and SEM analyses. In particular, the comparison between the Au and Ag islands reveals the formation of larger islands in the case of Ag for each fixed fluence. The mechanism of the nanoscale …

Physical and biological properties of electrospun poly( d , l ‐lactide)/nanoclay and poly( d , l ‐lactide)/nanosilica nanofibrous scaffold for bone t…

2021

Electrospun scaffolds exhibiting high physical performances with the ability to support cell attachment and proliferation are attracting more and more scientific interest for tissue engineering applications. The inclusion of inorganic nanoparticles such as nanosilica and nanoclay into electrospun biopolymeric matrices can meet these challenging requirements. The silica and clay incorporation into polymeric nanofibers has been reported to enhance and improve the mechanical properties as well as the osteogenic properties of the scaffolds. In this work, for the first time, the physical and biological properties of polylactic acid (PLA) electrospun mats filled with different concentrations of n…

An advance Towards the Synthesis of Ag Nanorod Arrays with Controlled Surface Roughness for SERS Substrates

2016

An innovative approach to produce silver nanorod (NRs) arrays with controlled morphological parameters and surface roughness is presented. The Ag NRs were obtained using a three-stage fabrication process based on the electron beam exposure of a metal-polymer nanocomposite resist on a transparent substrate and development, a post bake and then a series of non-electrochemical metallization steps. After each step the evolution of the Ag NRs was characterized by scanning electron microscopy (SEM) for morphology and optical transmittance (T) measurements for Localized Surface Plasmon Resonance (LSPR). The transmittance measurements were interpreted using models based on the Finite Element Method…