Search results for "Solid-Liquid"

Axial dispersion model for solid flow in liquid suspension in system of two mixers in total recycle

2006

The measurement of residence time distribution of solid particles in solid-liquid suspension is experimentally difficult. However, the twin system approach is particularly suited for the assessment of particle RTD in flow systems as it allows overcoming some of the usual difficulties generally encountered in this kind of measurement. Twin system consists of two vessels and external piping in total recycle. Experimental results from this system can be evaluated using Z-transforms to derive particle RTD for subsequent testing of alternative flow models. Recently, the axial dispersion model was applied using the "advection diffusion equation" (sometimes called the"diffusion with bulk flow equa…

On the Reduction of Power Consumption in Vortexing Unbaffled Bioslurry Reactors

2020

Bioremediation of polluted soils via bioslurry reactors is an interesting option among those available nowadays, especially when recalcitrant pollutants are present. Vortexing unbaffled stirred tanks may be a valuable choice to this purpose as they were recently found to be more efficient than baffled vessels for solid suspension processes where mixing time is not a controlling factor. When operated at sufficiently high agitation speeds, the central vortex bottom reaches the impeller and air bubbles start to be distributed throughout the system, thus avoiding any sparger and related clogging issues. In the present work, a vortexing unbaffled stirred tank with solid loadings ranging from 2.5…

Analysis of mycotoxins in barley using ultra high liquid chromatography high resolution mass spectrometry: comparison of efficiency and efficacy of d…

2012

The effectiveness of four extraction methods (modified QuEChERS, matrix solid-phase dispersion (MSPD), solid-liquid extraction (SLE) and solid-phase extraction (SPE) clean-up) were evaluated for simultaneous determination of 32 mycotoxins produced by the genus Fusarium, Claviceps, Aspergillus, Penicillium and Alternaria in barley by ultra high pressure liquid chromatography coupled to ultra-high resolution mass spectrometry (UHPLC-Orbitrap(®) MS). The efficiency and efficacy of extraction methods were evaluated and compared in number of extracted mycotoxins and obtained recoveries. From the one point of view, QuEChERS procedure was fast and easy, as well as it was able to successfully extra…

Residence Time Distribution of Solid Particles in a High-Aspect Ratio Multiple-Impeller Stirred Vessel

2003

Despite its importance, experimental information on the Residence Time Distribution (RTD) of solid particles in continuous-flow stirred vessels is still scant. In this work, experimental data on particle RTD in a high-aspect-ratio vessel stirred by three equally-spaced Rushton turbines, was obtained by means of a special technique named Twin System Approach (TSA). Quite surprisingly, results indicate that, among the various possibilities that could have been devised (e.g. 6, or 3, or 1 ideal tanks in series), the flow model closest to reality for the particle phase, at least in the experimental range here investigated, is that of a single perfectly stirred vessel.

Particle Suspension in Vortexing Unbaffled Stirred Tanks

2016

Three-phase processes in which particle suspension has to be achieved in conjunction with gas dispersion are traditionally carried out in sparged, baffled stirred tanks. The operation of such tanks can suffer, however, from particles tending to block the sparger holes. A viable alternative might be provided by uncovered unbaffled stirred tanks (UUSTs), where gas self-injection can occur when the free-surface vortex reaches the impeller blades and gas bubbles begin to be ingested by the liquid. In this work, the particle suspension and liquid aeration performances in three-phase UUSTs were experimentally investigated and compared with relevant literature correlations concerning baffled syste…

Modelling Turbulent Inter-Phase Drag in Mechanically Stirred Solid-Liquid Suspensions

2012

Dense Solid-Liquid Suspensions in Top-Covered Unbaffled Stirred Vessels

2011

In the present work solids suspension is investigated in an unbaffled tank stirred by a Rushton turbine and provided with a top-cover in order to avoid the formation of the well known central vortex. The data obtained are compared with those pertaining baffled stirred tanks via comparison with the well known Zwietering’s correlation. The dependence of Njs on particle concentration is found to be similar to that well established for baffled vessels, while, as a difference from the latter, Njs is found to decrease when liquid viscosity increases. Results also show that Njs is substantially independent of particle size, a feature that may advice the adoption of unbaffled tanks when large heavy…

CFD Simulation of Solid Liquid Suspensions in Baffled Stirred Vessels Below Complete Suspension Speed

2011

Suspension of solid particles into liquids within stirred vessels is a complex phenomenon encountered in several industrial applications. Most researchers have focused their attention on the assessment of the minimum impeller speed (Njs) able to guarantee the suspension of all particles. Actually, in a number of industrial cases an impeller speed N lower than Njs is chosen as typical operating condition (Oldshue, 1983) as the resulting energy savings well counterbalance the loss of active interfacial area. Therefore, the assessment of the amount of unsuspended particles at any given impeller speed represents the key to quantify the economical advantage/disadvantage of adopting an impeller s…

Measurements of Njs and Power Requirements in Unbaffled Bioslurry Reactors

2012

The remediation of urban/industrial polluted lands is a topic of crucial importance nowadays. Bioremediation techniques are widely employed to remove organic pollutants from contaminated soils because of their simplicity and cheapness. The bioslurry reactors mechanically agitated by stirrers represent one of the most promising bioremediation techniques. In the present work an unbaffled stirred vessel filled with solids and water is experimentally investigated from a fluid dynamic point of view. Air presence within the tank is guaranteed by the central vortex formation (typical occurrence concerning stirred vessels unprovided with baffles) instead of an intrinsically more expensive insufflat…

Power requirements for complete suspension and aeration in an unbaffled bioslurry reactor

2016

Remediation of contaminated soils is spreading as a matter of crucial importance nowadays. Bioremediation via bioslurry reactors of sites polluted by recalcitrant pollutants has been proved to be a valuable option, although optimization is needed to reduce process costs. Free-surface unbaffled stirred tanks (with central air vortex) have been recently proposed as a promising alternative to the more common systems provided with baffles. In a bioslurry reactor solid-liquid interfacial area, oxygen supply, solid loading per reactor unit volume should be maximized, and, at the same time, operation costs have to be kept low. In this regard, the minimum impeller speeds for complete suspension Njs…