Search results for "Synthesis"
showing 10 items of 2844 documents
Fabrication and characterization of Metal and Metal Oxide Nanostructures Grown by metal displacement deposition into anodic alumina membranes
2011
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Nickel-Indium Sulphide Core-Shell Nanostructures Obtained by Spray-ILGAR Deposition
2013
Ni nanowires (NWs) of different lengths were fabricated by pulsed potentiostatic deposition within pores of polycarbonate membranes. After template dissolution, substrates underwent sequential Spray-ILGAR (R) depositions of thin indium sulphide films. The effect of deposition temperature was also investigated. For low number of deposition cycles, results showed complete and uniform covering of metal over the entire length of NWs, with formation of Ni - In2S3 core-shell structures. However, with increasing number of deposition cycles films became uneven and crusty, especially at higher temperatures, owing to the simultaneous formation of nickel sulfide. This drawback was almost eliminated do…
Nanostructured anode material for Li-ion battery obtained by galvanic process
2016
This work focused on the synthesis and characterization of nanostructured lead hydroxide chloride (PbOHCl) that is an innovative anode material for lithium-ion batteries (LIBs). In particular, we have obtained nanostructures of mixed PbOHCl and lead metal, directly into the pores of a commercially available alumina membrane, acting as template. The process was based on galvanic displacement reaction that was carried out in a two-compartment electrochemical cell without the use of an external power supply. This simple and cheap procedure gives regular array of Pb/PbOHCl composite nanowires. To obtain nanostructured electrodes is a significant result because, it’s well known that nanostructur…
Analogia e omologia: la questione della filogenesi delle emozioni
2013
Aim of this paper is to outline a new evolutionary interpretation of aesthetic emotions, in the light of the most recent developments in Evolutionary Biology, in particular the so-called “Extended Synthesis of Evolution” (Pigliucci-Müller 2010). Focussing on the biological concept of homology, the Author argues that, in order to effectively understand role and evolutionary value of aesthetic emotions, it should be asked not “what aesthetic emotions are for?”, rather “what kind of constraints and homologies influence the specific “shape” of human aesthetic emotions?”. In a few words, we should move from a functionalist approach to human aesthetic emotions towards a morphological one.
Arte da Linguagem na Era da Panofonia
2018
This article calls attention to the hybrid genre of voice-based performances and its blending of the supposed binaries of human and machinic speech. Using the concept of panophonia, the author refers to the animatronic sculptures of speaking figures created by Ken Feingold and to Mark Böhlen’s talking robots. Through their comparative analysis, the author explores different poetic metalanguages both artists create to deconstruct communicative structures that demarcate post-human era.
From Overstoichiometric to Substoichiometric Enantioselective Protonation with 2-Sulfinyl Alcohols: A View in Perspective
2005
A general study of the enantioselective protonation of prochiral enolates with 2-sulfinyl alcohols is reported. The modification of reaction conditions to reduce drastically the amount of chiral proton source needed to obtain a good enantiomeric excess is reported. The effects of the different factors controlling the stereoselectivity are clearly established. Different protocols for enolate generation are compared.
Cytoplasmic 5′-3′ exonuclease Xrn1p is also a genome-wide transcription factor in yeast
2014
The 5′ to 3′ exoribonuclease Xrn1 is a large protein involved in cytoplasmatic mRNA degradation as a critical component of the major decaysome. Its deletion in the yeast Saccharomyces cerevisiae is not lethal, but it has multiple physiological effects. In a previous study, our group showed that deletion of all tested components of the yeast major decaysome, including XRN1, results in a decrease in the synthetic rate and an increase in half-life of most mRNAs in a compensatory manner. Furthermore, the same study showed that the all tested decaysome components are also nuclear proteins that bind to the 5′ region of a number of genes. In the present work, we show that disruption of Xrn1 activi…
Growth and Electrochemical Performance of Lead and Lead Oxide Nanowire Arrays as Electrodes for Lead-Acid Batteries
2013
n this work, we present the growth and electrochemical performance of nanostructured lead and lead oxide electrodes for lead-acid batteries. The electrodes were obtained by template electrodeposition in polycarbonate membranes, acting as template. Electrochemical tests were conducted at constant current in 5M aqueous solution of sulphuric acid, after assembling nanostructured lead and lead oxide electrodes in a zero-gap configuration using a commercially available separator. The main advantages of these electrodes are the high specific energy and power density, and the wide surface area, about 70 times higher than the geometrical one. These features allowed high discharge rates, up to 20C. …
One-dimensional nanostructures of lead and lead dioxide for application in lead-acid batteries
2010
Fabrication of Pb and PbO2 nanostructures was undertaken with the aim of building low cost lead acid micro-batteries with high performance. Despite environmental problems and the relatively low specific energy in comparison with other galvanic generators, lead acid batteries are still extensively used in the field of energy accumulation, owing to a well known and reliable technology. Thus, it is of high technological interest to develop procedures for fabricating these devices at a micrometer scale or less. PbO2 nanowires were grown in different electrochemical deposition conditions leading to pure -PbO2, pure -PbO2 and mixture [1-2]. Several parameters, like temperature, electrolyte…
Perceptions of learning and teaching human movement in physiotherapy : A systematic review and metasynthesis of qualitative studies
2023
Purpose: Human movement is essential for health and well-being. Understanding human movement is pivotal in physiotherapy, but also an important element of physiotherapy education. This review identified, critically appraised, and synthesized the available evidence on learning and teaching human movement in physiotherapy as perceived by students, therapists, and instructors. Methods: The databases MEDLINE, CINAHL, ERIC, PsycINFO, MEDIC and FINNA, were searched. The search was conducted in March/April 2020 and updated in March 2022. The systematic review followed the JBI methodology for systematic reviews of qualitative evidence and was conducted in accordance with an a priori protocol. Resul…