Search results for "Tetraphene"

showing 3 items of 3 documents

Unexpected Scholl Reaction of 6,7,13,14-Tetraarylbenzo[k]tetraphene: Selective Formation of Five-Membered Rings in Polycyclic Aromatic Hydrocarbons

2016

Cyclodehydrogenation is a versatile reaction that has enabled the syntheses of numerous polycyclic aromatic hydrocarbons (PAHs). We now describe a unique Scholl reaction of 6,7,13,14-tetraarylbenzo[k]tetraphene, which "unexpectedly" forms five-membered rings accompanying highly selective 1,2-shift of aryl groups. The geometric and optoelectronic nature of the resulting bistetracene analogue with five-membered rings is comprehensively investigated by single-crystal X-ray, NMR, UV-vis absorption, and cyclic voltammetry analyses. Furthermore, a possible mechanism is proposed to account for the selective five-membered-ring formation with the rearrangement of the aryl groups, which can be ration…

010405 organic chemistryStereochemistryArylGeneral Chemistry010402 general chemistryHighly selective01 natural sciencesBiochemistryCatalysis0104 chemical sciencesScholl reactionchemistry.chemical_compoundColloid and Surface ChemistrychemistryComputational chemistryDensity functional theoryAbsorption (chemistry)Cyclic voltammetryTetrapheneJournal of the American Chemical Society
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CCDC 1427947: Experimental Crystal Structure Determination

2016

Related Article: Junzhi Liu, Akimitsu Narita, Silvio Osella, Wen Zhang, Dieter Schollmeyer, David Beljonne, Xinliang Feng, and Klaus Müllen|2016|J.Am.Chem.Soc.|138|2602|doi:10.1021/jacs.5b10399

671314-tetrakis(4-t-butylphenyl)-512-diiodobenzo[k]tetraphene dichloromethane solvateSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1542456: Experimental Crystal Structure Determination

2018

Related Article: Maude Desroches, Paula Mayorga Burrezo, Joël Boismenu-Lavoie, Miriam Peña Álvarez, Carlos J. Gómez-García, Jon M. Matxain, David Casanova, Jean-François Morin, Juan Casado|2017|Angew.Chem.,Int.Ed.|56|16212|doi:10.1002/anie.201708740

Space GroupCrystallography44'4''4'''-[(410-bis{[tris(propan-2-yl)silyl]ethynyl}naphtho[78123-nopqr]tetraphene-612-diylidene)dimethanediylylidene]tetrabenzonitrile chloroform solvateCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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