Search results for "Thermal"

Bio-predictive tablet disintegration: Effect of water diffusivity, fluid flow, food composition and test conditions

2013

Abstract Food intake may delay tablet disintegration. Current in vitro methods have little predictive potential to account for such effects. The effect of a variety of factors on the disintegration of immediate release tablets in the gastrointestinal tract has been identified. They include viscosity of the media, precipitation of food constituents on the surface of the tablet and reduction of water diffusivity in the media as well as changes in the hydrodynamics in the surrounding media of the solid dosage form. In order to improve the predictability of food affecting the disintegration of a dosage form, tablet disintegration in various types of a liquefied meal has been studied under stati…

Inactivation of dried spores of Bacillus subtilis 168 by a treatment combining high temperature and pressure

2019

International audience; Specific treatments combining high temperatures of up to 150 °C and moderate pressure of up to 0.6 MPa have been applied to Bacillus subtilis 168 spores conditioned at different aw levels (between 0.10 and 0.70) corresponding to different residual water contents within the spore core. The spores were treated as a dry powder in a pressurized nitrogen environment or in water/glycerol solutions.These thermodynamic conditions were intended to prevent any water evaporation from the spore core during time/temperature treatments.Our results clearly show that retaining liquid water in the core by applying pressure during the treatment resulted in greater spore destruction (b…

Impact of conventional and non-conventional processing on prickly pear ( Opuntia spp.) and their derived products: From preservation of beverages to …

2017

Abstract Background In recent years, both food researchers and food industry have shown growing interest in Opuntia fruits, as they constitute a good source of phytochemicals such as phenolics, vitamin C, vitamin E, polysaccharides and betalains. Many of these compounds have shown antioxidant, anti-cancer, antiatherosclerotic and/or hepatoprotective properties. Moreover, the fruit is also a source of dietary fibers, which promote bowel transit, thus preventing constipation. Scope and approach Due to these properties, Opuntia fruits are considered as functional products offering numerous health benefits when are consumed as fresh or processed product. However, these compounds can lose their …

Ab initiocomputational study on the lattice thermal conductivity of Zintl clathrates[Si19P4]Cl4andNa4[Al4Si19]

2016

The lattice thermal conductivity of silicon clathrate framework ${\mathrm{Si}}_{23}$ and two Zintl clathrates, $[{\mathrm{Si}}_{19}{\mathrm{P}}_{4}]{\mathrm{Cl}}_{4}$ and ${\mathrm{Na}}_{4}[{\mathrm{Al}}_{4}{\mathrm{Si}}_{19}]$, is investigated by using an iterative solution of the linearized Boltzmann transport equation in conjunction with ab initio lattice dynamical techniques. At 300 K, the lattice thermal conductivities for ${\mathrm{Si}}_{23}, [{\mathrm{Si}}_{19}{\mathrm{P}}_{4}]{\mathrm{Cl}}_{4}$, and ${\mathrm{Na}}_{4}[{\mathrm{Al}}_{4}{\mathrm{Si}}_{19}]$ were found to be 43 W/(m K), 25 W/(m K), and 2 W/(m K), respectively. In the case of ${\mathrm{Na}}_{4}[{\mathrm{Al}}_{4}{\mathrm…

Synthesis, characterization and thermal properties of new aromatic quaternary ammonium bromides

2004

Series of new aromatic R 2R′ 2N +Br - (R=benzyl, 4-methylbenzyl, 2-phenylethyl, 3-phenylpropyl; R′=ethyl, methyl, isopropyl) or RR′ 2NH +Br --type (R=benzyl, R′=isopropyl) quaternary ammonium bromides were prepared by using novel synthetic route in which a formamide (N,N-diethylformamide, N,N-dimethylformamide, N,N-diisopropylformamide) is treated with aralkyl halide in presence of a weak base. The compounds were characterized by 1H-NMR and 13C-NMR spectroscopy and mass spectrometry. Structures of the crystalline compounds were determined by X-ray single crystal diffraction, and in addition the powder diffraction method was used to study the structural similarities between the single crysta…

Catalytic hydrothermal liquefaction of municipal sludge assisted by formic acid for the production of next-generation fuels

2021

Abstract Hydrothermal liquefaction (HTL) of municipal sludge (MS) was studied at 325 °C and 30 min at 10 and 30% w/w concentration of MS using formic acid (FA) as a green liquid hydrogen donor both in the absence and in the presence of heterogeneous catalysts. Pellets of commercial NiMo/Al2O3, CoMo/Al2O3 and felt of activated carbon ACF 1600 were used as catalysts. The addition of FA at high MS loading allowed to increase the yields in BC from 41 to 62% and its H/C ratio from 1.80 to 2.01 leading to energy recovery (ER) higher than 100%.When heterogeneous catalysts were used together with FA, a marked improvement of BC yields and quality was obtained at 10% MS loading. This behavior was not…

Cogeneration from thermal treatment of selected municipal solid wastes. A stoichiometric model building for the case study on Palermo

2003

This paper aims to calculate the energetic and environmental effects of an integrated solid waste management system in Palermo, Italy. In particular, the thermal treatment of Municipal Solid Waste (MSW) with energy recovery is assessed. The current characterization at the local scale is taken into account. Two different options of collection are taken into account: (1) unselected wastes; and (2) sorted collection, according to the current Italian regulation. Combustion process is analyzed and the following features are calculated: (1) stoichiometric content of air and air excess; and (2) temperature and enthalpy of flue gases. Energy recovery is performed in the hypothesis of Hirn cycle bot…

Non-Local Thermoelasticity: The Fractional Heat conduction

2011

Thermal NDE of thick GRP panels by means of a Pulse Modulated Lock-In Thermography technique

2010

This work describes the development and implementation of an infrared thermal NDE procedure for the evaluation of subsurface defects. The approach is called Pulse-Modulated Lock-In Thermography (PMLT) and is based on the analysis of the frequency response of the measured temperature and comparison with the carrier frequencies launched by the external heat delivering source. The heat deposited on the object is in particular modulated as a train of square waves. This is easily achieved by periodically shuttering the heat source. The temperature is then sampled throughout the deposition of a few square waves. A lock-in algorithm is then implemented able to selectively filter out components at …

Friction Stir Processing: thermo-mechanical loads and consequent effects on the local material characteristics

2008

The present article is focused on the correlation between the applied thermal and mechanical loads and the consequent effects on the material in friction stir processing (FSP) operations. On one hand, the actions exerted in FSP are split compared to the results obtained with a tool without the pin at its end to a traditional one with a cylindrical pin. In this way, the thermal flux determined by the frictional forces at the tool—shoulder—workpiece interface is secluded from the mechanical stirring action made by the tool pin. On the other hand, the processed specimens are analysed in terms of residual stress state, microhardness, and average grain size values. An in-process heat treatment …