Search results for "Union"
showing 10 items of 2069 documents
Bromide/bromate speciation by NTI-IDMS and ICP-MS coupled with ion exchange chromatography
1997
Two different mass spectrometric methods, negative thermal ionization isotope dilution mass spectrometry (NTI-IDMS) and inductively coupled plasma mass spectrometry (ICP-MS), off-line and on-line coupled with anion exchange chromatography, have been developed for simultaneous bromide and bromate determinations in water samples. The detection limits of these methods are in the range of 0.03–0.09 μg/L using a 50 mL sample.The results are independent of the content of other anions, which could be demonstrated by the analyses of six mineral waters containing chloride and sulfate of up to 160 mg/L and 1500 mg/L, respectively. Bromide has been analyzed by the NTI-IDMS method in the range of 10–50…
Optimization of Matrix Solid-Phase Dispersion method for simultaneous extraction of aflatoxins and OTA in cereals and its application to commercial s…
2010
Abstract A method based on Matrix Solid-Phase Dispersion (MSPD) has been developed for the determination of 5 mycotoxins (ochratoxin A and aflatoxins B and G) in different cereals. Several dispersants, eluents and ratios were tested during the optimization of the process in order to obtain the best results. Finally, samples were blended with C 18 and the mycotoxins were extracted with acetonitrile. Regarding to matrix effects, the results clearly demonstrated the necessity to use a matrix-matched calibration to validate the method. Analyses were performed by liquid chromatography–triple quadrupole-tandem mass spectrometry (LC–QqQ-MS/MS). The recoveries of the extraction process ranged from …
Extraction and analysis of ochratoxin A in bread using pressurised liquid extraction and liquid chromatography.
2005
A pressurised liquid extraction (PLE) method for the analysis of ochratoxin A (OTA) in bread samples is given. Parameters such as solvent, temperature, pressure and time were investigated thoroughly. The optimized PLE conditions were: methanol as extraction solvent, 80 degrees C, 2000 psi and a 5-min cycle. OTA was determined by liquid chromatography coupled with fluorescence detection and confirmed by methyl ester derivatization. Under these conditions OTA recovery is 92.3% with a RSD of 5%. Limits of detection and quantification were 0.02 and 0.06 microg/kg, respectively. The proposed method was applied to 20 bread samples, finding two positive samples with OTA levels below the maximum pe…
Multi-class determination of antimicrobials in meat by pressurized liquid extraction and liquid chromatography–tandem mass spectrometry
2008
A multi-residue method using pressurized liquid extraction (PLE) and liquid chromatography-tandem mass spectrometry (LC-MS/MS) has been developed for determining trace levels of 31 antimicrobials, including beta-lactams, lincosamides, macrolides, quinolones, sulfonamides, tetracyclines, nitroimidazoles and trimethoprim. The extraction method required pre-homogeneization of the meat with EDTA-washed sand and subsequent one-static-cycle extraction for 10 min with 40 ml of water at 1500 psi and 70 degrees C. The effect of operation temperature, pressure, flush volume, and static cycles on PLE performance was studied. Average recoveries ranged from 75 to 99% with relative standard deviations <1…
Peace as a Priority
2012
Chapter 9 underlines how since its inception the European Union has presented itself to the world as a great “peace project”. The European project consists in creating a “community of peace and democracy” based on the conviction that peace does not emerge from dissuasion but rather out of cooperation. Europe attempts to remodel the world by realising the Kantian dream of “perpetual peace”, which is not based on the balance of military powers (or the supremacy of one of them) but rather on the universal recognition of the dignity of the human being, on the universal guarantee of human rights, and on sustainable human development, which means superseding the current neoliberal model of global…
Differentiation, differentiated integration and disintegration in a ‘post-Brexit-era’
2019
In contrast to the ‘ever closer Union among the peoples of Europe’ invoked in the preamble of the Treaty of Rome, Frank Schimmelfennig and Thomas Winzen ponder whether the European Union (EU) is ‘growing ever looser’. Differentiation can take various forms which are often intertwined, such as functional, institutional, spatial/territorial as well as temporal differentiation. In 1998, Petersen studied Denmark’s integration policy in what he called a ‘dilemma’ between influence capability and stress sensitivity. With the Great Recession of 2007This introduction presents an overview of the key concepts discussed in the subsequent chapters of this book. The book 2008, the EU entered a new multi…
"L'effet direct des directives : la fin d'une résistance française", JCP éd. G, 2009, n° 50 du 7 décembre 2009, p. 542 et s.
2009
Le hasard dans le droit de l'Union européenne en matière d'accès au territoire de l'Union
2019
The article explores the question of "chance" in the European Union Law in the field of the admission of third States citizens and asylum seekers to the territory of the European Union. Le hasard fait son apparition dans le droit de l'Union européenne en matière de d'accès au territoire de l'Union pour les ressortissants des pays tiers, meme pour les demandeurs d'asile ou pour les personnes en besoin de protection. Dans ce contexte, le hasard perd les caractères habituels qui lui sont reconnus par les Etats membres de l'Union pour devenir un instrument de dissuasion au service de la priorité politique de reduire les mouvements migratoires.
Le associazioni e le società sportive dilettantistiche alla luce della normativa di fonte statale e federale: verifica della compatibilità con il det…
Il lavoro si pone lo scopo di analizzare nello specifico la tematica dei soggetti collettivi dilettantistici analizzando per iniziare la normativa che li concerne e valutando specificamente anche alcuni profili controversi che li riguardano, quali: a) la questione della rappresentanza apparente; b) il danno all'immagine dell’ente. In seguito ci si soffermerà sulle conseguenze funzionali del riconoscimento dell’autonomia dello sport e in particolare si analizzerà la natura aperta della sua struttura. Infatti, lo sport esercitato collettivamente a livello dilettantistico non tollera ingerenze statali per il tramite di controlli, autorizzazioni, registri e albi volti a creare differenziazioni …