Search results for "aminocyclodextrin"

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Silver nanoparticles stabilized by a polyaminocyclodextrin as catalysts for the reduction of nitroaromatic compounds

2015

Abstract Silver nanoparticles stabilized by means of poly -(6- N , N -dimethyl-propylenediamino)-(6-deoxy)-β-cyclodextrin were synthesized, characterized by different techniques (UV–vis spectroscopy, Dynamic Light Scattering, High Resolution Transmission Electron Microscopy, Fourier-transform IR Spectroscopy) and used as catalysts for the reduction of various nitrobenzene derivatives with sodium borohydride. The nanocomposites obtained appear to have an organized structure, with a metal core surrounded by a layer-structured coating shell. Kinetic data, rationalized in terms of a modified Langmuir–Hinshelwood model, evidenced a non-linear dependence of the reaction rate on the concentration …

Process Chemistry and TechnologyInduction periodInorganic chemistryInfrared spectroscopySettore CHIM/06 - Chimica OrganicaCatalysisSilver nanoparticleCatalysisReaction rateSodium borohydridechemistry.chemical_compoundDynamic light scatteringchemistryPolyaminocyclodextrin Nitroarene reduction Silver nanocompositePhysical and Theoretical ChemistryHigh-resolution transmission electron microscopyJournal of Molecular Catalysis A: Chemical
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Binding abilities of polyaminocyclodextrins: polarimetric investigations and biological assays.

2017

Three polyaminocyclodextrin materials, obtained by direct reaction between heptakis(6-deoxy-6-iodo)-β-cyclodextrin and the proper linear polyamines, were investigated for their binding properties, in order to assess their potential applications in biological systems, such as vectors for simultaneous drug and gene cellular uptake or alternatively for the protection of macromolecules. In particular, we exploited polarimetry to test their interaction with some model p-nitroaniline derivatives, chosen as probe guests. The data obtained indicate that binding inside the host cavity is mainly affected by interplay between Coulomb interactions and conformational restraints. Moreover, simultaneous i…

nitroanilineaminocyclodextrins; binding properties; nitroanilines; pDNA; polarimetry; supramolecular chemistrySupramolecular chemistryaminocyclodextrins010402 general chemistry01 natural sciencesFull Research Papersupramolecular chemistryaminocyclodextrinlcsh:QD241-441lcsh:Organic chemistrypDNABioassaybinding propertielcsh:Sciencepolarimetry010405 organic chemistryChemistryBinding propertiesOrganic ChemistryCationic polymerizationnitroanilines0104 chemical sciencesChemistrybinding propertiesPolynucleotideBiophysicslcsh:QpUC19Direct reactionMacromoleculeBeilstein journal of organic chemistry
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