Search results for "angle"

showing 10 items of 1921 documents

Through-bond versus through-space T1 energy transfers in organometallic compound-metalloporphyrin pigments

2009

The preparation and characterization of two d9−d9 M2-bonded Pt2(dppm)2(C≡CC6H4-M(P))2 complexes (where M = Zn or Pd, and P = diethylhexamethylporphyrin) were achieved. The central [Pt2(dppm)2(C≡CC6H4)2] organometallic unit appears to be an independent chromophore and is suspected to be luminescent at 77 K (in 2MeTHF) in the porphyrin-containing complexes, as this is the case for the unfunctionalized Pt2(dppm)2(C≡CPh)2 parent compound. However, when this spacer is connected (by a single C−C bond) to either M(P) (M = Zn, Pd), even in the absence of conjugation (as the computed dihedral angle between the C6H4 and porphyrin planes is ∼84.5°), total quenching of the luminescence of the [Pt2(dppm…

chemistry.chemical_elementDihedral angle010402 general chemistry01 natural sciencesInorganic Chemistrychemistry.chemical_compoundplatinumPhysical and Theoretical ChemistryComputingMilieux_MISCELLANEOUSQuenching (fluorescence)010405 organic chemistryChemistryOrganic ChemistryChromophoremetalloporphyrin pigmentpalladiumPorphyrin0104 chemical sciences[CHIM.THEO]Chemical Sciences/Theoretical and/or physical chemistryCrystallographytriplet energy transfer[ CHIM.THEO ] Chemical Sciences/Theoretical and/or physical chemistryAbsorption (chemistry)organometallic compoundPlatinumLuminescencePalladium
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CONSIDERAZIONI TEORICHE E PRATICHE SUL METODO DEL MASSIMO RETTANGOLO CIRCOSCRITTO PER LA VALUTAZIONE DELL’AMPIEZZA DELLA TENSIONE TANGENZIALE NEI CRI…

2012

The multiaxial fatigue criteria based on the approach of the critical plane require the determination of the amplitude of the alternating shear stress τ aacting on different planes passing through the point of the material analyzed. In the case of non-proportional stresses the shear stress vector varies both in modulus and direction and its tip describes a curvedefined loading path. In these cases τ ais identified and evaluated by means of special procedures the most recent, and apparently more effective, of which is that of the Maximum Circumscribed Rectangle (MCR) to the loading path itself. In particular τ ais equal to the length of the diagonal of the MCR. In this paper, the MCR method …

circumscribed circleSettore ING-IND/14 - Progettazione Meccanica E Costruzione Di Macchinecircumscribed rectanglemultiaxial fatiguerettangolo circoscrittoalternate shear strefatica multiassialetensione tangenziale alternatacerchio circoscritto
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R/C columns strengthened by means of steel angles and battens: testing, modeling and design

2010

columns angles battens confinement
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Linear ViscoElastic (LVE) Behaviour of Pure Bitumen via Fractional Model

2012

AbstractBy fitting experimental data from static creep/recovery carried out on pure bitumen, it is shown that the fractional model proposed enables the description of both creep and recovery behaviour with fewer parameters than those needed by other models in the literature. In particular, the model is fitted to experimental data of complex modulus |G*| and phase angle δ° obtained from Dynamic Mechanical Analysis. Lastly, it is demonstrated that when the fractional model is used, complex modulus isotherms for a range of frequencies can be created simply starting from isochronals at f = 1Hz.

complex modulubitumen.Materials scienceMathematical modelPhase angleThermodynamicsModulusDynamic mechanical analysisFractional modelViscoelasticityCreepAsphaltForensic engineeringRange (statistics)Settore ICAR/04 - Strade Ferrovie Ed AeroportiGeneral Materials ScienceCreep/recoverySettore ICAR/08 - Scienza Delle CostruzionibitumenComplex modulusProcedia - Social and Behavioral Sciences
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Crystal structure of (E)-4-methyl-N-{2-[2-(4-nitrobenzylidene)hydrazin-1-yl]-2-oxoethyl}benzenesulfonamideN,N-dimethylformamide monosolvate

2017

The molecule of the title Schiff base compound, C16H16N4O5S·C3H7NO, displays atransconformation with respect to the C=N double bond. The C—N and N—N bonds are relatively short compared to their normal bond lengths, indicating some degree of delocalization in the molecule. The molecule is bent at the S atom, with an S—N—C—C torsion angle of 164.48 (11)°. The dihedral angle between the two aromatic rings is 84.594 (7)°. Intermolecular N—H...O and C —H...O hydrogen bonds connect centrosymmetrically related molecules into dimers forming rings ofR33(11) andR22(10) graph-set motif stacked along theaaxis into a columnar arrangement. The molecular columns are further linked into a three-dimensional…

conformationchemistry.chemical_classificationcrystal structureSchiff baseDouble bondHydrogen bondAromaticityGeneral ChemistryCrystal structureDihedral angle010402 general chemistry010403 inorganic & nuclear chemistryCondensed Matter Physics01 natural sciences0104 chemical sciencesSulfonamidelcsh:ChemistryBond lengthSchiff basechemistry.chemical_compoundCrystallographylcsh:QD1-999chemistryGeneral Materials ScienceC—H...O hydrogen bondActa Crystallographica Section E Crystallographic Communications
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Naphthalene-2,6-diyl bis(4-methylbenzenesulfonate)

2018

The complete molecule of the title compound, C24H20O6S2, is generated by a crystallographic inversion centre at the middle of the naphthalene ring system. The dihedral angle between the naphthalene ring system and the pendant benzene ring is 10.23 (6)° and the C—S—O—C torsion angle is −172.05 (10)°. In the crystal, weak C—H...O interactions link the molecules into (10-1) sheets.

crystal structure010405 organic chemistryChemistryGeneral MedicineCrystal structureDihedral angle010402 general chemistryRing (chemistry)01 natural sciencesCoupling reactioncrosscoupling reactions0104 chemical sciencesCrystalCrystallographychemistry.chemical_compoundSulfonatecross-coupling reactionslcsh:QD901-999lcsh:CrystallographyPhysics::Chemical PhysicsBenzenetosylatesNaphthaleneIUCrData
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3,5-Dimethoxyphenyl 4-methylbenzenesulfonate

2017

Molecules of the title compound, C15H16O5S, are composed of a 3,5-dimethoxyphenyl moiety substituted with a toluene-4-sulfonate group. The dihedral angle between two aromatic rings is 57.23 (4)°. In the crystal, molecules are connected by weak C—H...O hydrogen bonds and S...O van der Waals interactions.

crystal structure010405 organic chemistryHydrogen bondStereochemistryChemistryAromaticityCrystal structuretosyl­atesDihedral angle010403 inorganic & nuclear chemistry01 natural sciencesMedicinal chemistryCoupling reaction0104 chemical sciencessymbols.namesakechemistry.chemical_compoundSulfonatecross-coupling reactionssymbolsMoietyvan der Waals forceIUCrData
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3,5-Bis(trifluoromethyl)phenyl 4-methylbenzenesulfonate

2017

Molecules of the title compound, C15H10F6O3S, are composed of 3,5-bis(trifluoromethyl)phenyl substituted with a toluene-4-sulfonate group. The dihedral angle between two aromatic moieties is 45.10 (5)°. In the crystal, molecules are connected by weak C—H...O and C—H...F contacts. One of the trifluoromethyl groups is disordered.

crystal structure010405 organic chemistryMeth-Crystal structuretosyl­atesDihedral angle010402 general chemistry01 natural sciencesCoupling reaction0104 chemical sciencesCrystalchemistry.chemical_compoundSulfonatecross-coupling reactionschemistryGroup (periodic table)Polymer chemistryMethyl benzeneIUCrData
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Crystal structure of 2-{[1-(2-methyl-5-nitro-1H-imidazol-1-yl)propan-2-yloxy]carbonyl}benzoic acid

2014

In the title compound, C15H15N3O6, the dihedral angle between the planes of the benzene and imidazole rings is 34.93 (10)°. An intramolecular C—H...O hydrogen bond is observed. In the crystal, O—H...N hydrogen bonds link the molecules into chains parallel to thecaxis.

crystal structureCrystal structurepharmaceuticalsDihedral angleBioinformaticsMedicinal chemistrynitro­imidazolesCrystalchemistry.chemical_compoundImidazoleGeneral Materials SciencePhysics::Chemical PhysicsO—H⋯N hydrogen bondsBenzeneBenzoic acidQuantitative Biology::BiomoleculesnitroimidazolesCrystallographyHydrogen bondGeneral ChemistryCondensed Matter PhysicsData ReportsO—H...N hydrogen bondschemistryQD901-999NitroActa Crystallographica Section E Structure Reports Online
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Crystal structure of 1-(2-fluoro­benzo­yl)-2,7-di­meth­oxy­naphthalene

2014

The asymmetric unit of the compound contains two independent conformers. Each conformer is stacked along the a axis to form columns through van der Waals inter­actions only.

crystal structureCrystallographyAromaticityGeneral ChemistryCrystal structureDihedral angleCondensed Matter PhysicsRing (chemistry)Bioinformatics1-aroyl­naphthalene compoundResearch Communicationschemistry.chemical_compoundsymbols.namesakeCrystallographynon-coplanarly accumulated aromatic rings structurechemistryQD901-999symbolsMoleculeGeneral Materials Sciencevan der Waals forceConformational isomerism1-aroylnaphthalene compoundNaphthalenespatial organizationActa Crystallographica Section E: Structure Reports Online
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