Search results for "crossover"

showing 10 items of 658 documents

Stimuli responsive hybrid magnets : tuning the photoinduced spin-crossover in Fe(III) complexes inserted into layered magnets

2013

The insertion of a [Fe(sal_2 trien)]^+ complex cation into a 2D oxalate network in the presence of different solvents results in a family of hybrid magnets with coexistence of magnetic ordering and photoinduced spin crossover (LIESST effect) in compounds [Fe^{III}(sal_2 trien)][Mn^{II}Cr^{III}(ox)_3]·CHCl_3 (1·CHCl_{3}) [Fe^{III}(sal_{2} trien)][Mn^{II}Cr^{III}(ox)_{3}]·CHBr_{3} (1·CHBr_{3}) and [Fe^{III}(sal_{2} trien)][Mn^{II}Cr^{III}(ox)_{3}]·CH_{2}Br_{2} (1·CH_{2}Br_{2}). The three compounds crystallize in a 2D honeycomb anionic layer formed by Mn^{II} and Cr^{III} ions linked through oxalate ligands and a layer of [Fe(sal_{2} trien)]^{+} complexes and solvent molecules (CHCl_{3} CHBr_{…

MagnetismInorganic chemistry010402 general chemistry01 natural sciencesBiochemistryCatalysisOxalateLIESSTchemistry.chemical_compoundColloid and Surface ChemistrySpin crossoverFe(III)Mössbauer spectroscopyOrganometallic CompoundsMoleculeMolecular Structure010405 organic chemistryChemistryRelaxation (NMR)Complex cationMagnetismHybrid magnetsGeneral ChemistryOxalate network[CHIM.MATE]Chemical Sciences/Material chemistryPhotochemical Processes0104 chemical sciencesCrystallographyMagnetic FieldsFerromagnetismddc:540Solvents
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First Cobalt(II) Spin Crossover Compound with N4S2-Donorset

2020

Herein we report the synthesis and characterization of a novel bis-tridentate 1,3,4-thiadiazole ligand (L = 2,5-bis[(2-pyridylmethyl)thio]methyl-1,3,4-thiadiazole). Two new mononuclear complexes of the type [MII(L)2](ClO4)2 (with M = FeII (C1) and CoII (C2)) have been synthesized, containing the new ligand (L). In both complexes the metal centers are coordinated by an N4S2-donorset and each of the two ligands is donating to the metal ion with just one of the tridentate pockets. The iron(II) complex (C1) is in the low spin [LS] state below room temperature and shows an increase in the magnetic moment only above 300 K. In contrast, the cobalt(II) complex (C2) shows a gradual spin crossover (S…

MagnetismPharmaceutical Sciencechemistry.chemical_elementThio-n<sub>4</sub>s<sub>2</sub>-donorsetAnalytical Chemistrylcsh:QD241-441Metalspin crossoverlcsh:Organic chemistrySpin crossoverDrug DiscoveryPhysical and Theoretical ChemistrySpin (physics)134-thiadiazolecobalt(ii)Magnetic momentLigandOrganic Chemistryiron(ii)CrystallographychemistryChemistry (miscellaneous)magnetismvisual_artvisual_art.visual_art_mediumMolecular MedicineCobaltMolecules
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Prevention of Hereditary Angioedema Attacks with a Subcutaneous C1 Inhibitor

2017

Prevenció; Atac d'angioedema; Inhibidor C1 Prevención; Ataque de angioedema; Inhibidor C1 Prevention; Angioedema attack; C1 inhibitor BACKGROUND: Hereditary angioedema is a disabling, potentially fatal condition caused by deficiency (type I) or dysfunction (type II) of the C1 inhibitor protein. In a phase 2 trial, the use of CSL830, a nanofiltered C1 inhibitor preparation that is suitable for subcutaneous injection, resulted in functional levels of C1 inhibitor activity that would be expected to provide effective prophylaxis of attacks. METHODS: We conducted an international, prospective, multicenter, randomized, double-blind, placebo-controlled, dose-ranging, phase 3 trial to evaluate the …

Male:aminoácidos péptidos y proteínas::péptidos::serpinas::proteínas inactivadoras del complemento C1::proteína inhibidora del complemento C1 [COMPUESTOS QUÍMICOS Y DROGAS]0301 basic medicine:Otros calificadores::Otros calificadores::/prevención & control [Otros calificadores]Enzims proteolítics - InhibidorsSelf AdministrationSeverity of Illness Indexlaw.inventionC1-inhibitorSubcutaneous injection0302 clinical medicineRandomized controlled triallawCross-Over StudiesHereditary Angioedema Types I and IIbiologyEdema - PrevencióGeneral Medicine:Cardiovascular Diseases::Vascular Diseases::Angioedema::Angioedemas Hereditary [DISEASES]AnesthesiaHereditary angioedema:Other subheadings::Other subheadings::/administration & dosage [Other subheadings]Female:Amino Acids Peptides and Proteins::Peptides::Serpins::Complement C1 Inactivator Proteins::Complement C1 Inhibitor Protein [CHEMICALS AND DRUGS]medicine.symptomComplement C1 Inhibitor Protein:enfermedades cardiovasculares::enfermedades vasculares::angioedema::angioedemas hereditarios [ENFERMEDADES]AdultRiskmedicine.medical_specialtyInjections Subcutaneous:Aminoácidos Péptidos y Proteínas::Péptidos::Serpinas::Proteínas Inactivadoras del Complemento 1::Proteína Inhibidora del Complemento C1 [COMPUESTOS QUÍMICOS Y DROGAS]Placebo:Other subheadings::Other subheadings::/prevention & control [Other subheadings]03 medical and health sciencesDouble-Blind MethodInternal medicinemedicineHumans:Therapeutics::Drug Therapy::Drug Administration Routes::Injections::Injections Subcutaneous [ANALYTICAL DIAGNOSTIC AND THERAPEUTIC TECHNIQUES AND EQUIPMENT]:Otros calificadores::Otros calificadores::/administración & dosificación [Otros calificadores]Dose-Response Relationship DrugAngioedemabusiness.industry:Terapéutica::Tratamiento Farmacológico::Vías de Administración de Medicamentos::Inyecciones::Inyecciones Subcutáneas [TÉCNICAS Y EQUIPOS ANALÍTICOS DIAGNÓSTICOS Y TERAPÉUTICOS]Injeccions hipodèrmiquesmedicine.diseaseCrossover studyClinical trial:terapéutica::farmacoterapia::vías de administración de medicamentos::inyecciones::inyecciones subcutáneas [TÉCNICAS Y EQUIPOS ANALÍTICOS DIAGNÓSTICOS Y TERAPÉUTICOS]030104 developmental biology030228 respiratory systembiology.proteinbusinessNew England Journal of Medicine
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Shifts in Key Time Points and Strategies for a Multisegment Motor Task in Healthy Aging Subjects

2018

International audience; In this study, we compared key temporal points in the whole body pointing movement of healthy aging and young subjects. During this movement, subject leans forward from a standing position to reach a target. As it involves forward inclination of the trunk, the movement creates a risk for falling. We examined two strategic time points during the task-first, the crossover point where the velocity of the center of mass (CoM) in the vertical dimension outstripped the velocity in the anteroposterior dimension and secondly, the time to peak of the CoM velocity profile. Transitions to stabilizing postures occur at these time points. They both occurred earlier in aging subje…

MaleAgingmedicine.medical_specialtyEquilibriumMovementCrossoverWhole body pointingCenter of massKey (music)Cohort Studies03 medical and health sciences0302 clinical medicinePhysical medicine and rehabilitationReference ValuesTask Performance and AnalysisHumansMedicine[SDV.NEU] Life Sciences [q-bio]/Neurons and Cognition [q-bio.NC]Prospective StudiesHealthy agingPostural BalancepostureAged[SDV.MHEP.GEG] Life Sciences [q-bio]/Human health and pathology/Geriatry and gerontologybusiness.industryMovement (music)[SDV.MHEP.GEG]Life Sciences [q-bio]/Human health and pathology/Geriatry and gerontologyWork (physics)trunk structure030229 sport sciencesTrunkHealthy VolunteersBiomechanical PhenomenaOptimal controlvertical dimensionhealthy agingMotor SkillsDuration (music)Female[SDV.NEU]Life Sciences [q-bio]/Neurons and Cognition [q-bio.NC]Geriatrics and GerontologybusinessFalling (sensation)Psychomotor Performance030217 neurology & neurosurgeryThe Journals of Gerontology: Series A
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Amitriptyline in neuropathic cancer pain in patients on morphine therapy: A randomized placebo-controlled, double-blind crossover study

2002

Aims and Background Amitriptyline is the most common analgesic adjuvant used in cancer patients with neuropathic pain, even though no specific studies have demonstrated a benefit. A randomized placebo-controlled, double-blind crossover study was designed to evidence the effects of amitriptyline in patients with neuropathic cancer pain. Methods Sixteen advanced cancer patients with neuropathic pain on systemic morphine therapy, no longer receiving oncologic treatment, presenting moderate pain (about 4 or more, but less than 7, on a numerical scale of 0-10) in the last week, and given a stable morphine dose in the last 2 days were admitted to the study. During the first week of study, patient…

MaleCancer ResearchAmitriptylineAnalgesicPlaceboNeuropathic painDrug Administration Schedule03 medical and health sciences0302 clinical medicineDouble-Blind Method030502 gerontologyRandomized controlled studyNeoplasmsmedicineHumansAmitriptylineCancer painAgedPain MeasurementAged 80 and overCross-Over StudiesMorphinebusiness.industryGeneral MedicineAnalgesics Non-NarcoticMiddle AgedCrossover studyAnalgesics OpioidTreatment OutcomeOncologyOpioid030220 oncology & carcinogenesisAnesthesiaNeuropathic painQuality of LifeMorphineNeuralgiaDrug Therapy CombinationFemaleAnalgesic0305 other medical scienceCancer painbusinessmedicine.drug
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Directional Deep Brain Stimulation for Parkinson's Disease: Results of an International Crossover Study With Randomized, Double-Blind Primary Endpoin…

2022

Objective Published reports on directional deep brain stimulation (DBS) have been limited to small, single-center investigations. Therapeutic window (TW) is used to describe the range of stimulation amplitudes achieving symptom relief without side effects. This crossover study performed a randomized double-blind assessment of TW for directional and omnidirectional DBS in a large cohort of patients implanted with a DBS system in the subthalamic nucleus for Parkinson's disease. Materials and methods Participants received omnidirectional stimulation for the first three months after initial study programming, followed by directional DBS for the following three months. The primary endpoint was a…

MaleDeep brain stimulationParkinson's diseasemedicine.medical_treatmentParkinson's diseaseDeep Brain StimulationStimulation03 medical and health sciences0302 clinical medicinemedicineClinical endpointHumanstherapeutic windowNeurostimulationTherapeutic windowCross-Over Studiesbusiness.industrydirectional programmingParkinson DiseaseGeneral Medicinemedicine.diseaseCrossover studySubthalamic nucleusAnesthesiology and Pain MedicineTreatment OutcomeNeurologyAnesthesiaQuality of LifeFemaleNeurology (clinical)business030217 neurology & neurosurgery
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The impact of cortisol reactivity to acute stress on memory: Sex differences in middle-aged people

2010

Stress has been identified as a main factor involved in the cognitive changes that occur during the aging process. This study investigated sex differences in the relationship between the magnitude of the acute stress-induced salivary cortisol response and memory performance among middle-aged people. To this end, 16 men and 16 women (aged 54-72 years) were exposed to the Trier Social Stress Test and a control condition in a crossover design. Afterwards their memory performance was measured using a standardized memory test (Rey's Auditory Verbal Learning Test). Only among women, there was an acute impact of stress on memory performance and a significant relationship between a higher cortisol …

MaleHypothalamo-Hypophyseal SystemHydrocortisonePhysiologyPituitary-Adrenal SystemVerbal learningDevelopmental psychologylaw.inventionBehavioral NeuroscienceRandomized controlled trialMemorylawTrier social stress testHumansSalivaReactivity (psychology)AgedMemory DisordersSex CharacteristicsEndocrine and Autonomic SystemsStressorMiddle AgedCrossover studyPostmenopausePsychiatry and Mental healthNeuropsychology and Physiological PsychologyMenarcheFemalePsychologyStress PsychologicalClinical psychologySex characteristicsStress
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Comparison of the brainstem auditory evoked responses during sevoflurane or alfaxalone anaesthesia in adult cats.

2017

Abstract Objective To compare the effects of general anaesthesia using sevoflurane or alfaxalone on the brainstem auditory evoked response (BAER) test in adult healthy cats. Study design Prospective, clinical, ‘blinded’, crossover study. Animals Ten feral adult healthy cats. Methods Premedication consisted of dexmedetomidine (0.01 mg kg –1 ) intramuscularly (IM). The first general anaesthesia was induced and maintained with sevoflurane (treatment S) for physical examination, BAER test, complete blood tests, thoracic radiographs and abdominal ultrasound. The second general anaesthesia was induced with alfaxalone (treatment A) IM (2 mg kg –1 ) and maintained with alfaxalone (10 mg kg –1 hour …

MaleMethyl Ethers040301 veterinary sciencesSevofluranePregnanediones0403 veterinary science03 medical and health sciencesSevoflurane0302 clinical medicine030202 anesthesiologymedicineEvoked Potentials Auditory Brain StemReaction TimeAnimalsGeneral anaesthesiaDexmedetomidineAnestheticsCATSCross-Over StudiesGeneral Veterinarybusiness.industryAlfaxalone04 agricultural and veterinary sciencesCrossover studyAuditory brainstem responseAnesthesiaCatsPremedicationbusinessmedicine.drugVeterinary anaesthesia and analgesia
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Can Brief, Daily Training Using a Mobile App Help Change Maladaptive Beliefs? Crossover Randomized Controlled Trial

2019

BackgroundObsessive-compulsive disorder (OCD) is a disabling condition with a wide variety of clinical presentations including contamination fears, fear of harm, and relationship-related obsessions. Cognitive behavioral models of OCD suggest that OC symptoms result from catastrophic misinterpretations of commonly occurring intrusive experiences and associated dysfunctional strategies used to manage them. OCD-related maladaptive beliefs including inflated responsibility, importance and control of thoughts, perfectionism, and intolerance for uncertainty increase the likelihood of such misinterpretations. ObjectiveConsidering accumulating evidence suggesting that mobile health (mHealth) apps b…

MaleObsessive-Compulsive DisorderTime FactorsAdolescentmedicine.medical_treatmentHealth InformaticsFitness TrackersInformation technologymedicine.disease_causelaw.inventionYoung AdultRandomized controlled triallawobsessive compulsive disorderSurveys and Questionnairesmental disordersmedicineHumansStudentsExercisemobile appsOriginal PaperCross-Over Studiesbusiness.industryRepeated measures designmaladaptive beliefsPerfectionism (psychology)T58.5-58.64Mobile ApplicationsCrossover studyCognitive trainingMoodSpaincognitive therapyCognitive therapyFemalerelationshipsPublic aspects of medicineRA1-1270businessClinical psychologyPsychopathologyJMIR mHealth and uHealth
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Anodal transcranial direct current stimulation and intermittent theta-burst stimulation improve deglutition and swallowing reproducibility in elderly…

2019

Background: Dysphagia in the elderly, known as presbydysphagia, has become a relevant public health problem in several countries. Swallowing disorders may be a consequence of different neurological disorders (secondary presbydysphagia) or the expression of the aging process itself (primary presbydysphagia). We aimed to test the therapeutic potential of two different non-invasive brain stimulation (NIBS) techniques in subjects with primary or secondary presbydysphagia. Methods: A blinded randomized controlled trial with crossover design was carried out in 42 patients, randomly assigned to anodal transcranial direct current stimulation (tDCS) or intermittent theta-burst stimulation (TBS) grou…

MalePhysiologymedicine.medical_treatmentbrain stimulationStimulationTranscranial Direct Current StimulationtDCSlaw.invention030507 speech-language pathology & audiology03 medical and health sciences0302 clinical medicineSwallowingRandomized controlled trialDouble-Blind MethodlawmedicineHumansTBSProspective StudiesAgedCross-Over StudiesTranscranial direct-current stimulationEndocrine and Autonomic Systemsbusiness.industrySwallowing DisordersGastroenterologyMotor CortexCrossover studyDysphagiaDeglutitionTreatment OutcomepresbydysphagiaBrain stimulationAnesthesiaTMSFemalemedicine.symptom0305 other medical sciencebusinessDeglutition Disorders030217 neurology & neurosurgery
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