Search results for "emissiospetrometria"

The determination of trace element concentrations in fly ash samples using ultrasound-assisted digestion followed with inductively coupled plasma opt…

2009

A method of ultrasound-assisted digestion followed by inductively coupled plasma optical emission spectrometry (ICP-OES) used for the determination of trace element (chromium, copper, lead, nickel, vanadium and zinc) concentrations in fly ash samples was developed. All the measurements were performed in robust plasma conditions. Ultrasound-assisted digestion procedures using digestion solutions of aqua regia and hydrofluoric acid (HF) resulted in recovery rates of over 80% for all the analyte elements. Ultrasound-assisted two-step digestion with digestion solutions of 6 mL of HNO₃(Step 1) and 3 mL of HNO₃+ 3 mL of HF (Step 2) resulted in recovery rates of over 92% for all the analyte elemen…