Search results for "emulsion"
showing 10 items of 344 documents
Microwave-assisted synthesis of anhydrous CdS nanoparticles in a water-oil microemulsion.
2006
Abstract Microwave irradiation at a frequency of 2.45 GHz and a power ranging between 22 and 30 W was used, in a water–oil microemulsion at 35 ± 2 ° C , to obtain stable, small, crystalline, anhydrous CdS nanoparticles exhibiting enhanced luminescence properties. The process of nanoparticles growth at different irradiation times was followed by UV–vis spectroscopy. It was observed that irradiated nanoparticles grew faster and their size reached a constant value. The final mean nanoparticle diameter was 2.7 nm, smaller than that observed in a non-irradiated sample, in which particle dimensions slowly increased even after 10 h. This finding was confirmed by high resolution transmission electr…
Photonic Crystals from Core-Shell Colloids with Incorporated Highly Fluorescent Quantum Dots
2005
We report the preparation of nanoscaled PS/PMMA core-shell spheres with highly fluorescent CdS/ZnS coated CdSe quantum dots (QDs) integrated in the core. Core-shell spheres of different diameters have been self-assembled to colloidal photonic crystals (PCs) with photonic stop bands located in the visible range of the electromagnetic spectrum. For the synthesis of the core, a modified miniemulsion polymerization has been used; the shell was prepared by a newly developed core-shell polymerization. The CdSe QDs embedded in the core were coated with the higher band gap semiconductor materials CdS and ZnS in a successive ion layer adsorption reaction (SILAR) keeping up the light-emitting propert…
Microwave radiation effect on the synthesis of cadmium sulphide nanoparticles in water in oil microemulsion: a preliminary study at different frequen…
2004
AbstractCadmium sulphide nanoparticles have been synthesised in water/sodium bis (2-ethylhexyl) sulfosuccinate (AOT)/n- heptane microemulsions kept at 30 °C by microwave irradiation coupled with water-cooling and in conventional thermostatic conditions at the same temperature. The study has been performed exposing the reaction media to microwave radiation at five different frequencies (2.45, 2.85, 8, 12 and 18 GHz). For each frequency, a suitable microwave exposure set-up has been assembled. During the growth process, the dimensions of the nanoparticles have been characterised by means of UV-Vis spectroscopy. At the end of the growth process, the surface morphology of the nanoparticles has …
Synthesis of low density foam shells for inertial confinement fusion experiments
2011
This work deals with the fabrication process of low density foam shells and the sharp control of their shape (diameter, thickness, density, sphericity, non-concentricity). During this PhD we focused on the non-concentricity criterion which has to be lower than 1%. The shells are synthesized using a microencapsulation process leading to a double emulsion and followed by a thermal polymerization at 60°C. According to the literature, three major parameters, the density of the three phases, the deformations of the shells along the process and the kinetics of the polymerization have a direct influence on the shells non-concentricity. The results obtained showed that when the density gap between …
Measurement of charmed-particle lifetimes and decay branching ratios
1987
The lifetimes of charmed hadrons photoproduced in nuclear emulsion have been computed from a practically background-free sample of 44 neutral particle decays and 42 charged-particle decays including 27D±, 11Λc+, 1Ds+ and 3 ambiguous decays. The values obtained are τ(D0, bar D0) = (3.6-0.8+1.2 ± 0.7) 10-13 s, τ(D±) = (5.0-1.0+1.5 ± 1.9) 10-13 s, τ(Λc+) = = (2.3-0.6+0.9 ± 0.4) 10-13 s. Branching ratios of various decay topologies were also obtained.
Configurational entropy of microemulsions : The fundamental length scale
1993
Phenomenological models have been quite successful in characterizing both the various complex phases and the corresponding phase diagrams of microemulsions. In some approaches, e.g., the random mixing model (RMM), the lattice parameter is of the order of the dimension of an oil or water domain and has been used as a length scale for computing a configurational entropy, the so‐called entropy of mixing, of the microemulsion. In the central and material section of this paper (Sec. III), we show that the fundamental length scale for the calculation of the entropy of mixing is of the order of the cube root of the volume per molecule—orders of magnitude smaller than the dimension of such a domain…
Nuclear Interactions of 400 GeV Protons in Emulsion
1978
Abstract We report on 400 GeV proton-emulsion nucleus reactions and compare the results to hadron-nucleus reactions at smaller energies. In particular we present results on the emission of fast target protons (essentially grey track particles) and on their correlation with the number of collisions inside the nucleus, ν, with the number of charged evaporated particles (essentially black track particles) and with the number of pions produced (essentially shower particles). We observe that the main features of the 200–400 GeV data are very similar. However, we find that the mean shower-particle multiplicity at 400 GeV is essentially higher than expected from the simple independent particle mod…
Search for νμ(νe) ↔ ντ oscillations with a detector based on a emulsion-silicon target
1996
We discuss the performance of a next generation νμ(νe)↔ ντ oscillation experiment, based on a target consisting of a sandwich of nuclear emulsion layers and silicon detectors. The target would be followed by a full spectrometer for energy-momentum measurement and particle identification. A τ-enriched sample is selected in terms of vertex and kinematical criteria using the electronic spectrometer, with very high efficiency, while at the same time reducing the load of background events to be scanned by up to two orders of magnitude. Events fulfilling the selection criteria are very efficiently located and scanned in the emulsion, thanks to the very good resolution allowed by the silicon track…
Status of J-PARC E07: Systematic study of double strangeness nuclei with hybrid emulsion method
2019
J-PARC E07 is the most complex emulsion experiment to date investigating double hypernuclei with a hybrid emulsion method. This experiment aims to detect 104 Ξ− stop events, ten times more events than the past experiments. Thus, an unequivocal identification of several new double hypernuclei is expected. The beam exposure has been completed at the K1.8 beam line of the J-PARC hadron facility in June 2017. The photographic development of all emulsion sheets has also been completed in February 2018. The emulsion sheets are presently being analyzed with dedicated optical microscopes. Current statistics is comparable to that of E373 and so far 10 events of 3-vertices topology have been detected…
Status of the J-PARC E07, Systematic Study of Double Strangeness Nuclei with the Hybrid Emulsion Method
2019
The current status of the J-PARC E07 experiment and two typical events, a _ΛΛBe hypernuclear event named “MINO” and \(_{\Xi }^{15}\text{C}\) hypernuclear event named “IBUKI”, are presented. J-PARC E07 is the most complex emulsion experiment so far to investigate double hypernuclei. The physics run at the K1.8 beam line in the J-PARC hadron facility and photographic development of all emulsion sheets have been completed. The emulsion sheets are presently being analyzed with dedicated optical microscopes. Current statistics are estimated to be about twice that of KEK-PS E373. Quantitative data on ΔB_ΛΛ of double Λ hypernucleus and \(B_{\Xi ^{ - }}\) of Ξ hypernucleus are being accumulated suc…