Search results for "extract"

showing 10 items of 2769 documents

Automatic Detection of Left Ventricular Contours from Cardiac Cine Magnetic Resonance Imaging Using Fuzzy Logic

1999

Gated cardiac cine magnetic resonance imaging provides accurate dynamic data of the left ventricular function. However, the manual extraction of important physiologic parameters such as myocardium wall thickness and left ventricular volumes is invariably time consuming and subjective. To reduce the variability and time constraints inherent in observer contour tracing, the authors developed an automatic left ventricle contour-detection method.The purpose was to apply fuzzy logic-based automatic contour detection to identification of endocardial and epicardial borders in short-axis magnetic resonance images. The automatic contouring was compared with manual tracing using the calculated ejecti…

Adultmedicine.diagnostic_testVentricular functionComputer scienceDynamic dataMyocardial InfarctionMagnetic Resonance Imaging CineStroke VolumeMagnetic resonance imagingGeneral MedicineMiddle AgedFuzzy logicManual extractionFuzzy LogicImage Processing Computer-Assistedcardiovascular systemmedicineHumansVentricular FunctionRadiology Nuclear Medicine and imagingcardiovascular diseasesWall thicknessAgedBiomedical engineeringInvestigative Radiology
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Capsular bag shrinkage after implantation of a capsular bending or capsular tension ring.

2005

To evaluate the influence of a capsular bending ring (CBR) or tension ring (CTR) on capsular bag shrinkage.Department of Ophthalmology, Johannes Gutenberg-University, and Department of Medical Biometry, Epidemiology and Informatics, University of Mainz, Mainz, Germany.In 92 eyes of 92 patients, a capsular measuring ring (CMR) was implanted after phacoemulsification to measure capsular bag size in vivo. Patients were randomized into 3 groups: The first received a CMR and CBR, the second received a CMR and CTR, and the third received a CMR alone. Measurements were performed preoperatively, intraoperatively, during the first 3 postoperative days, and after 1 and 3 months. Preoperative biometri…

Adultmedicine.medical_specialtyVisual acuityBiometrymedicine.medical_treatmentLens Capsule CrystallineCapsular tension ringIntraocular lensCataract ExtractionGroup differencesLens Implantation IntraocularOphthalmologymedicineHumansCapsulorhexisShrinkageAgedAged 80 and overPhacoemulsificationbusiness.industryPhacoemulsificationEquipment DesignProstheses and ImplantsMiddle AgedSensory SystemsSurgeryOphthalmologyCapsular bagMicroscopy Electron ScanningSurgerymedicine.symptombusinessJournal of cataract and refractive surgery
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Comparison of the effect of ginger and aloe vera mouthwashes on xerostomia in patients with type 2 diabetes: A clinical trial, triple-blind

2021

Background Ginger and aloe vera are two medicinal herbs mostly used to produce mouthwash. This study aimed to compare the effects of ginger and aloe vera mouthwashes on the xerostomia in patients referred to Bandar Abbas diabetes clinic (Iran). Material and Methods In this triple-blind clinical trial, three groups (n=35 patients in each group) were studied. One group was given aloe vera mouthwash, the other group used ginger mouthwash, and the control group was only given normal saline. All the mouthwashes were used 20 ccs three times daily for 14 consecutive days. The symptoms and severity of xerostomia were measured before and after the intervention by the questionnaire proposed by Fox et…

Adultmedicine.medical_specialtymedicine.medical_treatmentMouthwashesType 2 diabetesGingerIranXerostomiaAloe veralaw.inventionMcNemar's testbone regenerationstomatognathic systemRandomized controlled triallawInternal medicineDiabetes mellitusHumansMedicineIn patientthird molarxenograftAloeGeneral DentistrySalineUNESCO:CIENCIAS MÉDICASAgedtooth extractionOral Medicine and Pathologybiologybusiness.industryResearchMiddle Agedbiology.organism_classificationmedicine.diseaseClinical trialDiabetes Mellitus Type 2OtorhinolaryngologySurgerybusinessMedicina Oral Patología Oral y Cirugia Bucal
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Characterization of oligomeric compounds in secondary organic aerosol using liquid chromatography coupled to electrospray ionization Fourier transfor…

2009

The components of secondary organic aerosols (SOAs) generated from the gas-phase ozonolysis of two C(10)H(16)-terpenes (alpha-pinene; sabinene) and a cyclic C(6)H(10) alkene (cyclohexene) were characterized by the use of a Fourier transform ion cyclotron mass spectrometer equipped with an electrospray ionization source operated in the negative ion mode. Reversed-phase high-performance liquid chromatography was used to achieve chromatographic separation of highly oxidized organic compounds. In addition to the well-known group of low molecular weight oxidation products (monomers; e.g. dicarboxylic acids), higher molecular weight compounds (dimers) were also detected and their exact elemental …

AerosolsSpectrometry Mass Electrospray IonizationChromatographyChemistryElectrospray ionizationOrganic ChemistryAnalytical chemistryExtractive electrospray ionizationMass spectrometryTandem mass spectrometryFourier transform ion cyclotron resonanceIon sourceAnalytical ChemistryTandem Mass SpectrometryCyclohexenesSpectroscopy Fourier Transform InfraredMonoterpenesDirect electron ionization liquid chromatography–mass spectrometry interfaceChromatography High Pressure LiquidSpectroscopyBicyclic MonoterpenesAmbient ionizationRapid Communications in Mass Spectrometry
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Bimodal porous silica nanomaterials as sorbents for an efficient and inexpensive determination of aflatoxin M1 in milk and dairy products

2020

Abstract An extraction procedure was developed for the determination of aflatoxin M1 in milk and dairy products. A sorbent based on UVM-7 mesoporous silica was used as solid phase for the sample clean-up, and the analyte determination was carried out by HPLC coupled to a fluorescence detector. The material architecture was characterized by transmission electronic microscopy, X-ray diffraction, 29Si NMR and nitrogen adsorption-desorption. After the optimization of extraction parameters, the influence of the matrix has been evaluated, obtaining recoveries in the range 78–105% for whole and skimmed milk and yogurt matrix. The reusability of the material was also proved. The sensitivity of the …

AflatoxinAnalytefood.ingredientSorbentChromatographyMaterials science010401 analytical chemistryExtraction (chemistry)04 agricultural and veterinary sciencesGeneral MedicineMesoporous silica040401 food science01 natural sciences0104 chemical sciencesAnalytical ChemistryMatrix (chemical analysis)0404 agricultural biotechnologyfoodSkimmed milkSolid phase extractionFood ScienceFood Chemistry
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Occurrence of Aflatoxins in Tigernuts and Their Beverages Commercialized in Spain

2010

A method based on matrix solid phase dispersion extraction was applied to determine aflatoxins B(1), B(2), G(1), and G(2) from tigernuts and tigernut beverages. Recoveries of each aflatoxin from tigernut (spiked at 10 microg/kg level) and from tigernut beverages (spiked at 10 microg/L level) ranged from 72.3 to 82.1% and from 74.0 to 86.3%, respectively. The limits of quantification ranged from 0.21 to 1.49 microg/kg (for tigernuts) and from 0.13 to 0.57 microg/L (for tigernut beverages) studied using liquid chromatography with fluorescence detection. The proposed extraction method followed by liquid chromatography-fluorescence detection determination was applied to 37 and 25 samples of tig…

AflatoxinChromatographyRoot cropsExtraction (chemistry)Reproducibility of ResultsGeneral ChemistrySensitivity and SpecificityBeveragesMatrix (chemical analysis)chemistry.chemical_compoundSpectrometry FluorescenceAflatoxinschemistrySpainSolventsNutsUltrasonicsExtraction methodsFood scienceGeneral Agricultural and Biological SciencesMycotoxinControl methodsChromatography LiquidFood contaminantJournal of Agricultural and Food Chemistry
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Determination of aflatoxins in peanuts by matrix solid-phase dispersion and liquid chromatography

2003

A new method based on matrix solid-phase dispersion (MSPD) extraction was studied to determine aflatoxin B1, B2, G1 and G2 from peanuts. Optimization of different parameters, such as type of solid supports for matrix dispersion and elution solvents were carried out. The method used 2 g of peanut sample, 2 g of C18 bonded silica as MSPD sorbent and acetonitrile as eluting solvent. Recoveries of each aflatoxin spiked to peanut samples at 2.5 ng/g (5 ng/g for aflatoxin G2) level were between 78 and 86% with relative standard deviations ranging from 4 to 7%. The limits of quantification ranged from 0.125 to 2.5 ng/g for the four studied aflatoxins using liquid chromatography (LC) with fluoresce…

AflatoxinElectrosprayChromatographyArachisElutionChemistryOrganic ChemistryExtraction (chemistry)Enzyme-Linked Immunosorbent AssayGeneral MedicineSensitivity and SpecificityBiochemistryHigh-performance liquid chromatographyAnalytical ChemistryMatrix (chemical analysis)Spectrometry FluorescenceAflatoxinsSample preparationSolid phase extractionChromatography LiquidJournal of Chromatography A
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High Pressure Processing Impact on Alternariol and Aflatoxins of Grape Juice and Fruit Juice-Milk Based Beverages.

2021

High-pressure processing (HPP) has emerged over the last 2 decades as a good alternative to traditional thermal treatment for food safety and shelf-life extension, supplying foods with similar characteristics to those of fresh products. Currently, HPP has also been proposed as a useful tool to reduce food contaminants, such as pesticides and mycotoxins. The aim of the present study is to explore the effect of HPP technology at 600 MPa during 5 min at room temperature on alternariol (AOH) and aflatoxin B1 (AFB1) mycotoxins reduction in different juice models. The effect of HPP has also been compared with a thermal treatment performed at 90 °C during 21 s. For this, different juice models, or…

AflatoxinFood industryFood HandlingLiquid Phase MicroextractionAlternariolPharmaceutical ScienceOrganic chemistryFood Contamination01 natural sciencesArticlealternariolAnalytical ChemistryPascalizationBeverageschemistry.chemical_compoundLactones0404 agricultural biotechnologyQD241-441AflatoxinsTandem Mass Spectrometryjuice modelsDrug Discoverydispersive liquid–liquid microextractionAnimalsVitisFood sciencePhysical and Theoretical ChemistryMycotoxinChromatography High Pressure LiquidOrange juicehigh-pressure processingbusiness.industry010401 analytical chemistry04 agricultural and veterinary sciencesMycotoxinsFood safety040401 food science0104 chemical sciencesFruit and Vegetable JuicesMilkchemistryChemistry (miscellaneous)Fruitaflatoxin B1Molecular Medicinebusinessliquid chromatography coupled to tandem mass spectrometryFood contaminantMolecules (Basel, Switzerland)
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Occurrence of aflatoxins in feedstuff, sheep milk and dairy products in Western Sicily

2003

Samples of feedstuffs (15), milk (40), and cheese (30) coming from sheep and dairy farms (23) or market in WesternSicily were analyzed for their respective content of aflatoxin B1 (AFB1) and M1 (AFM1) to evidence any possible indirectmycotoxin contamination risk to the consumer. Analyses using HPLC and fluorescence detection were performed afterimmunoaffinity column sample extraction and cleanup; AFM1 was detected in 30% of the milk samples at levels rangingfrom 4 to 23 ng/l and in 13% of the cheeses from 21 to 101 ng/kg; in the feed the AFB1 ranged from None of the contaminated samples exceeded the legal limits set down by the European Union for milk (50 ng/l) and feed(5 μg/kg ), or tha…

AflatoxinMycotoxin contamination010405 organic chemistry010401 analytical chemistryContaminationBiology01 natural sciences0104 chemical sciencesmedia_common.cataloged_instanceAnimal Science and ZoologyFood sciencelcsh:Animal cultureSample extractionEuropean unionSheep milkAflatoxin M1 Sheep milk Sheep cheese Aflatoxin B1 Feedstuffmedia_commonlcsh:SF1-1100Italian Journal of Animal Science
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MYCOTOXINS | Detection and Analysis by Classical Techniques

2014

This article is a revision of the previous edition article by Imad Ali Ahmed, volume 2, pp. 1526–1532, © 1999, Elsevier Ltd.

Aflatoxinchemistry.chemical_compoundChromatographychemistryVolume (thermodynamics)Liquid–liquid extractionAnalytical chemistrySample preparationGas chromatographyHigh-performance liquid chromatographyOchratoxinThin-layer chromatography
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